CN204816164U - Novel ammonia is retrieved device - Google Patents
Novel ammonia is retrieved device Download PDFInfo
- Publication number
- CN204816164U CN204816164U CN201520621777.XU CN201520621777U CN204816164U CN 204816164 U CN204816164 U CN 204816164U CN 201520621777 U CN201520621777 U CN 201520621777U CN 204816164 U CN204816164 U CN 204816164U
- Authority
- CN
- China
- Prior art keywords
- ammonia
- absorption tower
- pipe
- water
- seal head
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims abstract description 123
- 229910021529 ammonia Inorganic materials 0.000 title claims abstract description 58
- 238000010521 absorption reaction Methods 0.000 claims abstract description 72
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 68
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims abstract description 36
- 238000011084 recovery Methods 0.000 claims abstract description 16
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 61
- 239000004744 fabric Substances 0.000 claims description 9
- 238000004064 recycling Methods 0.000 claims description 9
- 239000007921 spray Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000008400 supply water Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Landscapes
- Treating Waste Gases (AREA)
- Gas Separation By Absorption (AREA)
Abstract
The utility model belongs to the technical field of the ammonia is retrieved, specifically disclose a novel ammonia is retrieved device, include water tank, aqueous ammonia case, aqueous ammonia collecting box, absorption tower and the ammonia pipe that communicates with the absorption tower, the water tank leads to pipe and absorption tower intercommunication, is equipped with the water seal head on the absorption tower, and the ammonia pipe passes the water seal head and stretches into in the absorption tower, be equipped with the ammonia recovery tube in the water seal head, ammonia recovery tube one end and absorption tower intercommunication, the other end is established in the water seal head and is buckled downwards, the water pipe has two branch pipes, and a branch pipe is connected with the shower nozzle of establishing in the absorption tower, and another branch pipe is connected with the water seal head, be equipped with absorption tower aqueous ammonia pipe and head aqueous ammonia pipe on the aqueous ammonia collecting box, aqueous ammonia pipe in absorption tower is connected with the absorption tower bottom, and head aqueous ammonia pipe is connected with the water seal head. The utility model discloses simple structure, rate of recovery height and with low costs.
Description
Technical field
The utility model belongs to Ammonia recovery technical field, particularly the novel ammonia recycling device of one.
Background technology
Ammonia is very easily water-soluble, can prepare ammoniacal liquor with water absorbing ammonia.Ammonia is water-soluble, volume-diminished, can increase the solubility of ammonia in water, thus obtain the ammoniacal liquor of high concentration by increasing pressure or reducing temperature.Namely the main task in ammonia job shop ammoniacal liquor post is unnecessary ammonia is generated ammoniacal liquor and processes the weak aqua ammonia sent here in synthesis workshop, plays the effect that balance ammonia is produced.
In actual production, the absorption tower in ammoniacal liquor post is ordinary-pressure absorption, is packing layer in the middle part of absorption tower, and top is spray equipment, and top blow-down pipe removes liquid layer built with filler.Ammoniacal liquor requires that certified products concentration is at 18%-20%, and it is between 13%-25% that weak aqua ammonia concentration is sent in synthesis workshop here, and carry not the melting property gas such as a small amount of methane secretly, pressure is 1.5MP.Synthesizing after the weak aqua ammonia sent here enters receiving slit beats to absorption tower bottom pressure relief with pump, enters ammonia vessel after most of ammoniacal liquor decompression bottom absorption tower, and another part ammoniacal liquor resolves volatilization for ammonia.The ammonia of resolving volatilization also enters 1# ammonia vessel after packing layer is absorbed into ammoniacal liquor by the clear water sprayed bottom absorption tower.The emptying after remove liquid except liquid layer of gas after absorption.Because weak aqua ammonia concentration instability is sent in synthesis here, pressure is higher, and excessive pressure reduction causes ammonia absorption pressure oscillation, and the ammonia that ammoniacal liquor resolves volatilization can not absorb completely in absorption tower, and part ammonia is overflowed from blow-down pipe, causes adverse effect to surrounding enviroment.
Utility model content
The purpose of this utility model is to provide that a kind of structure is simple, the rate of recovery is high and the novel ammonia recycling device that cost is low.
For achieving the above object, the utility model is by the following technical solutions: novel ammonia recycling device, the ammonia pipe comprising water tank, ammoniacal liquor case, ammoniacal liquor collecting box, absorption tower and be communicated with absorption tower, water tank is communicated with absorption tower by water pipe, absorption tower is provided with water seal head, and ammonia pipe stretches in absorption tower through water seal head; Be provided with Ammonia recovery pipe in water seal head, Ammonia recovery pipe one end is communicated with absorption tower, and the other end to be located in water seal head and to bend downwards; Water pipe is with two arms, and an arm is connected with the shower nozzle be located in absorption tower, and another arm is connected with water seal head; Ammoniacal liquor collecting box is provided with absorption tower ammonia water pipe and end socket ammonia water pipe, and absorption tower ammonia water pipe is connected with bottom absorption tower, and end socket ammonia water pipe is connected with water seal head.
Further, ammoniacal liquor case passes through to be connected into ammonia water pipe with bottom absorption tower.
Further, in absorption tower, be provided with shower nozzle fabric swatch, described shower nozzle fabric swatch is evenly distributed with shower nozzle.
Further, water pipe is connected with water pump.
Compared with prior art, the beneficial effects of the utility model are as follows: absorption tower is provided with water seal head, and ammonia pipe stretches in absorption tower through water seal head, effectively enhances the sealing of device, prevent ammonia leakage from improving security; Be provided with Ammonia recovery pipe in water seal head, Ammonia recovery pipe one end is communicated with absorption tower, and the other end to be located in water seal head and to bend downwards, arranges bending place, can effectively increase ammonia and contact with water body, strengthens the absorptivity of ammonia, avoids the situation occurring ammonia leakage; Water pipe is with two arms, and an arm is connected with the shower nozzle be located in absorption tower, and another arm is connected with water seal head, adopts a water tank to supply water to water seal head and absorption tower simultaneously, reduces the quantity of parts, cost-saving; Ammoniacal liquor collecting box is provided with absorption tower ammonia water pipe and end socket ammonia water pipe, absorption tower ammonia water pipe is connected with bottom absorption tower, and end socket ammonia water pipe is connected with water seal head, and the ammoniacal liquor absorbed in absorption tower and water seal head enters ammoniacal liquor collecting box by pipeline, layout designs is reasonable, is conducive to the recovery of ammoniacal liquor; Ammoniacal liquor case passes through to be connected into ammonia water pipe with bottom absorption tower, arranges ammoniacal liquor case passing in ammonia forward direction absorption tower and passes into ammoniacal liquor, be conducive to the absorption of ammonia, increases Ammonia recovery rate; Be provided with shower nozzle fabric swatch in absorption tower, shower nozzle fabric swatch is evenly distributed with shower nozzle, shower nozzle is evenly arranged on shower nozzle fabric swatch, makes water body spray evenly, increases the absorptivity of ammonia.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
Novel ammonia recycling device, as shown in Figure 1, the ammonia pipe 6 comprising water tank 3, ammoniacal liquor case 1, ammoniacal liquor collecting box 12, absorption tower 5 and be communicated with absorption tower 5, water tank 3 is communicated with absorption tower 5 by water pipe 4, absorption tower 5 is provided with water seal head 7, and ammonia pipe 6 stretches in absorption tower 5 through water seal head 7; Be provided with Ammonia recovery pipe 8 in water seal head 7, Ammonia recovery pipe 8 one end is communicated with absorption tower 5, and the other end to be located in water seal head 7 and to bend downwards; Water pipe 4 is with two arms, and an arm is connected with the shower nozzle 10 be located in absorption tower 5, and another arm is connected with water seal head 7; Ammoniacal liquor collecting box 12 is provided with absorption tower ammonia water pipe 13 and end socket ammonia water pipe 11, and absorption tower ammonia water pipe 13 is connected with bottom absorption tower 5, and end socket ammonia water pipe 11 is connected with water seal head 7.Ammoniacal liquor case 1 passes through to be connected into ammonia water pipe 14 with bottom absorption tower 5.Be provided with shower nozzle fabric swatch 9 in absorption tower 5, shower nozzle fabric swatch 9 be evenly distributed with shower nozzle 10.Water pipe 4 is connected with water pump 2.
During work, first the water in water tank 3 is passed in absorption tower 5 and water seal head 7 by water pipe 4, shower nozzle 10 starts water spray, again the weak aqua ammonia in ammoniacal liquor case 1 is passed through to pass in absorption tower 5 into ammonia water pipe 14, then ammonia to be entered in absorption tower 5 by ammonia pipe 6 and is absorbed by the water that shower nozzle 10 sprays, the unabsorbed ammonia of part to be entered in water seal head 7 by Ammonia recovery pipe 8 and is absorbed by water wherein and forms weak aqua ammonia, and the ammoniacal liquor formed after reaction is entered in ammoniacal liquor collecting box 12 by end socket ammonia water pipe 11 and absorption tower ammonia water pipe 13.
Claims (4)
1. novel ammonia recycling device, the ammonia pipe comprising water tank, ammoniacal liquor case, ammoniacal liquor collecting box, absorption tower and be communicated with absorption tower, water tank is communicated with absorption tower by water pipe, it is characterized in that: described absorption tower is provided with water seal head, and ammonia pipe stretches in absorption tower through water seal head; Be provided with Ammonia recovery pipe in described water seal head, Ammonia recovery pipe one end is communicated with absorption tower, and the other end to be located in water seal head and to bend downwards; Described water pipe is with two arms, and an arm is connected with the shower nozzle be located in absorption tower, and another arm is connected with water seal head; Described ammoniacal liquor collecting box is provided with absorption tower ammonia water pipe and end socket ammonia water pipe, and absorption tower ammonia water pipe is connected with bottom absorption tower, and end socket ammonia water pipe is connected with water seal head.
2. ammonia recycling device as claimed in claim 1, is characterized in that: described ammoniacal liquor case passes through to be connected into ammonia water pipe with bottom absorption tower.
3. ammonia recycling device as claimed in claim 1 or 2, is characterized in that: be provided with shower nozzle fabric swatch in described absorption tower, described shower nozzle fabric swatch is evenly distributed with shower nozzle.
4. ammonia recycling device as claimed in claim 3, is characterized in that: described water pipe is connected with water pump.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201520621777.XU CN204816164U (en) | 2015-08-18 | 2015-08-18 | Novel ammonia is retrieved device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201520621777.XU CN204816164U (en) | 2015-08-18 | 2015-08-18 | Novel ammonia is retrieved device |
Publications (1)
Publication Number | Publication Date |
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CN204816164U true CN204816164U (en) | 2015-12-02 |
Family
ID=54673807
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201520621777.XU Expired - Fee Related CN204816164U (en) | 2015-08-18 | 2015-08-18 | Novel ammonia is retrieved device |
Country Status (1)
Country | Link |
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CN (1) | CN204816164U (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107303458A (en) * | 2016-04-19 | 2017-10-31 | 五冶集团上海有限公司 | Pressure Vessels Ammonia Leak Testing residual gas recycling device |
CN108332458A (en) * | 2018-03-26 | 2018-07-27 | 河南开祥精细化工有限公司 | The ammonia recycling device of ammonia refrigeration system |
CN109482058A (en) * | 2018-11-13 | 2019-03-19 | 段美军 | A kind of efficient acid mist adsorption tower reducing poisonous gas leakage |
-
2015
- 2015-08-18 CN CN201520621777.XU patent/CN204816164U/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107303458A (en) * | 2016-04-19 | 2017-10-31 | 五冶集团上海有限公司 | Pressure Vessels Ammonia Leak Testing residual gas recycling device |
CN108332458A (en) * | 2018-03-26 | 2018-07-27 | 河南开祥精细化工有限公司 | The ammonia recycling device of ammonia refrigeration system |
CN109482058A (en) * | 2018-11-13 | 2019-03-19 | 段美军 | A kind of efficient acid mist adsorption tower reducing poisonous gas leakage |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151202 |