CN204768721U - Pure looks cobaltosic oxide's of synthetic preparation of liquid phase apparatus for producing - Google Patents
Pure looks cobaltosic oxide's of synthetic preparation of liquid phase apparatus for producing Download PDFInfo
- Publication number
- CN204768721U CN204768721U CN201520501698.5U CN201520501698U CN204768721U CN 204768721 U CN204768721 U CN 204768721U CN 201520501698 U CN201520501698 U CN 201520501698U CN 204768721 U CN204768721 U CN 204768721U
- Authority
- CN
- China
- Prior art keywords
- feed pipe
- inlet pipe
- pipe
- alkali lye
- oxidant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Abstract
The utility model relates to a pure looks cobaltosic oxide's of synthetic preparation of liquid phase apparatus for producing, the oxidant inlet pipe, cobalt liquid inlet pipe and alkali lye inlet pipe all are on a parallel with reation kettle axon line and are vertical direction height -adjustable to stretch into reation kettle internal, the oxidant inlet pipe, cobalt liquid inlet pipe and alkali lye inlet pipe are apart from the internal wall 5 -50 of reation kettle centimetre, the lower mouth of pipe of cobalt liquid inlet pipe and the lower mouth of pipe of alkali lye inlet pipe are higher than the lower mouth of pipe of oxidant inlet pipe, the oxidant inlet pipe, 0 -60 degree contained angle is personally submitted with the level in the plane that the low tube degree of lip -rounding of cobalt liquid inlet pipe and alkali lye inlet pipe tee pipe becomes, the height of stirring rake is in the oxidant inlet pipe, in the lower mouth of pipe of cobalt liquid inlet pipe and alkali lye inlet pipe tee pipe between the high and minimum mouth of pipe horizontal plane. Its simple structure, the simple operation obtains pure nature cobaltosic oxide because of reaction rate change product changes thereupon at cobaltosic oxide in process of production.
Description
Technical field
The utility model relates to a kind of cobaltosic oxide production equipment, is the process units that a kind of liquid phase synthesis prepares pure phase cobaltosic oxide specifically.
Background technology
In the generative process of cobaltosic oxide, in the reaction that preparation cobalt liquid and preparation alkali lye are oxidized at blowing air, because the intensity of reactive site oxidation is different, the cobalt oxide generated forms difference: a kind of shaping loose, the jolt ramming and the pine that affect particle fill on the low side, and specific surface is higher, and these material are as made lithium battery, battery compacting will be affected, thus reduce battery containing electricity.Another kind of shaping crystallization, comprises during this grain forming or the more sodium of crystallization, by XRD analysis still containing hydroxy cobalt oxide, does not meet customer requirement.
Summary of the invention
The utility model is intended providing a kind of structure simple, and simple operation, at cobaltosic oxide, because of reaction rate change, product changes the process units obtaining pure property cobaltosic oxide thereupon in process of production
The technical solution adopted in the utility model is: a kind of liquid phase synthesis prepares the process units of pure phase cobaltosic oxide, comprise reaction kettle body, oxidant feed pipe, cobalt liquid feed pipe, alkali lye feed pipe and paddle, reaction kettle body is provided with overfall, described oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe are all parallel to reaction kettle body axis and stretch in reaction kettle body, oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe distance reaction kettle body inwall 5-50 centimetre, the lower nozzle of cobalt liquid feed pipe and the lower nozzle of alkali lye feed pipe are higher than the lower nozzle of oxidant feed pipe, oxidant feed pipe, the plane of the lower nozzle formation of cobalt liquid feed pipe and alkali lye feed pipe three pipe is horizontal by 0-60 degree angle, the height of paddle is in oxidant feed pipe, between mouth of pipe horizontal plane high and minimum in the lower nozzle of cobalt liquid feed pipe and alkali lye feed pipe three pipe.
Further, described oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe three are managed and are projected as equilateral triangle in the horizontal plane.
Further, the described equilateral triangle length of side is the 0.5-0.8 of reactor diameter.
Further, the 0.35-0.45 of described paddle blade length and reactor radius.
Again further, the lower nozzle of described cobalt liquid feed pipe is positioned at 0-25cm on stirring, and the lower nozzle of alkali lye feed pipe is positioned at 0-40cm on stirring, and air feed pipe is positioned at 0-60cm under stirring.
React and sent into by oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe, stir, kettle diameter relatively concrete, take into account the adjustment of reaction key element simultaneously, produce the product met.Cobalt chloride solution first carries out degree of depth oil removal treatment, is configured to the cobalt liquor needing concentration, adds additive in proportion, react in special reactor with liquid caustic soda, pass into air and be oxidized, by controlling reaction rate, control particles generation environment, thus produce the cobaltosic oxide of pure phase.
The plane formed by regulating the lower nozzle of three feed pipes and horizontal plane angle, in conjunction with the adjustment of the relative distance of control three feed pipes distance and still wall, preparation pure phase obtains cobaltosic oxide, oxidation completely, grain forming is better, and particle jolt ramming >=2.8g/ ㎝ 3, pine dress >=1.7g/ ㎝ 3, sodium≤0.030%, cobalt content >=69.5%, particle are spherical.The utility model operating process is easy, production efficiency is high, labor strength is little.
Accompanying drawing explanation
Fig. 1 is the utility model structural representation.
In figure: reaction kettle body 1, oxidant feed pipe 2, cobalt liquid feed pipe 3, alkali lye feed pipe 4, overfall 5, paddle 6.
Detailed description of the invention
Be described further below in conjunction with drawings and Examples.
Shown in Fig. 1: the process units that a kind of liquid phase synthesis prepares pure phase cobaltosic oxide comprises reaction kettle body 1, oxidant feed pipe 2, cobalt liquid feed pipe 3, alkali lye feed pipe 4 and paddle 6, reaction kettle body 1 is provided with overfall 5, oxidant feed pipe 2, cobalt liquid feed pipe 3 and alkali lye feed pipe 4 are all parallel to reaction kettle body 1 axis and stretch in reaction kettle body 1, oxidant feed pipe 2, cobalt liquid feed pipe 3 and alkali lye feed pipe 4 are apart from reaction kettle body 1 inwall 5-50 centimetre, the lower nozzle of cobalt liquid feed pipe 3 and the lower nozzle of alkali lye feed pipe 4 are higher than the lower nozzle of oxidant feed pipe 2, oxidant feed pipe 2, the plane of the lower nozzle formation of cobalt liquid feed pipe 3 and alkali lye feed pipe 4 three pipe is horizontal by 0-60 degree angle, the height of paddle 6 is in oxidant feed pipe 2, between mouth of pipe horizontal plane high and minimum in the lower nozzle of cobalt liquid feed pipe 3 and alkali lye feed pipe 4 three pipe.Oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe three are managed and are projected as equilateral triangle in the horizontal plane.The equilateral triangle length of side is the 0.5-0.8 of reactor diameter.The 0.35-0.45 of paddle blade length and reactor radius.The lower nozzle of cobalt liquid feed pipe is positioned at 0-25cm on paddle, and the lower nozzle of alkali lye feed pipe is positioned at 0-40cm on paddle, and air feed pipe is positioned at 0-60cm under paddle.
The inwall of reaction kettle body 1 can be evenly equipped with multiple vertically disposed baffle plate, for corresponding stirring arm wake turbulence, improve reaction efficiency.
Claims (5)
1. a liquid phase synthesis prepares the process units of pure phase cobaltosic oxide, comprise reaction kettle body, oxidant feed pipe, cobalt liquid feed pipe, alkali lye feed pipe and paddle, reaction kettle body is provided with overfall, it is characterized in that: described oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe be all parallel to reaction kettle body axis in vertical direction height adjustable stretch in reaction kettle body, oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe distance reaction kettle body inwall 5-50 centimetre, the lower nozzle of cobalt liquid feed pipe and the lower nozzle of alkali lye feed pipe are higher than the lower nozzle of oxidant feed pipe, oxidant feed pipe, the plane of the lower nozzle formation of cobalt liquid feed pipe and alkali lye feed pipe three pipe is horizontal by 0-60 degree angle, the height of paddle is in oxidant feed pipe, between mouth of pipe horizontal plane high and minimum in the lower nozzle of cobalt liquid feed pipe and alkali lye feed pipe three pipe.
2. a kind of liquid phase synthesis according to claim 1 prepares the process units of pure phase cobaltosic oxide, it is characterized in that: described oxidant feed pipe, cobalt liquid feed pipe and alkali lye feed pipe three are managed and be projected as equilateral triangle in the horizontal plane.
3. a kind of liquid phase synthesis according to claim 2 prepares the process units of pure phase cobaltosic oxide, it is characterized in that: the described equilateral triangle length of side is the 0.5-0.8 of reactor diameter.
4. a kind of liquid phase synthesis according to claim 1 prepares the process units of pure phase cobaltosic oxide, it is characterized in that: the 0.35-0.45 of described paddle blade length and reactor radius.
5. a kind of liquid phase synthesis according to claim 1 prepares the process units of pure phase cobaltosic oxide, it is characterized in that: the lower nozzle of described cobalt liquid feed pipe is positioned at 0-25cm on stirring, the lower nozzle of alkali lye feed pipe is positioned at 0-40cm on stirring, and air feed pipe is positioned at 0-60cm under stirring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520501698.5U CN204768721U (en) | 2015-07-13 | 2015-07-13 | Pure looks cobaltosic oxide's of synthetic preparation of liquid phase apparatus for producing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520501698.5U CN204768721U (en) | 2015-07-13 | 2015-07-13 | Pure looks cobaltosic oxide's of synthetic preparation of liquid phase apparatus for producing |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204768721U true CN204768721U (en) | 2015-11-18 |
Family
ID=54508852
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520501698.5U Active CN204768721U (en) | 2015-07-13 | 2015-07-13 | Pure looks cobaltosic oxide's of synthetic preparation of liquid phase apparatus for producing |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204768721U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107128980A (en) * | 2017-06-27 | 2017-09-05 | 荆门市格林美新材料有限公司 | The fast preparation method and system of a kind of cobaltosic oxide |
-
2015
- 2015-07-13 CN CN201520501698.5U patent/CN204768721U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107128980A (en) * | 2017-06-27 | 2017-09-05 | 荆门市格林美新材料有限公司 | The fast preparation method and system of a kind of cobaltosic oxide |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206285902U (en) | Slurry is set at the uniform velocity to flow out the device of agitator tank | |
| CN105417566A (en) | Method for preparing nano calcium carbonate through full-automatic rotating pressure jet-carbonation technology | |
| CN203577796U (en) | Circular reaction device of spherical cobalt hydroxide | |
| CN104556174B (en) | A kind of impact flow reactor | |
| CN204768721U (en) | Pure looks cobaltosic oxide's of synthetic preparation of liquid phase apparatus for producing | |
| CN206027682U (en) | Novel ludox reaction device | |
| CN107416888A (en) | A kind of preparation method of nano cupric oxide | |
| CN106698444A (en) | Hypergravity liquid precipitation method of preparing silicone dioxide nanometer granule based on rice hull ash | |
| CN208894199U (en) | A kind of precipitated silica generating device | |
| CN113788501B (en) | Method for preparing cobalt oxyhydroxide | |
| CN203754439U (en) | Conic bottom perturbation plug flow aluminum hydroxide crystal reactor | |
| CN104998596A (en) | Production device for preparing pure-phase cobalt tetraoxide through liquid-phase synthesis | |
| CN205575669U (en) | Preparation nano calcium carbonate's device | |
| CN204958493U (en) | Wadding machine is separated to dense media powder flco | |
| CN210973907U (en) | Micro-reaction device for preparing nano calcium carbonate | |
| CN201783631U (en) | Thermal insulating exothermic riser molding device | |
| CN103395807A (en) | Impinging stream-rotating disc coupling reaction device and ultrafine magnesium hydroxide fire retardant synthesis method using impinging stream-rotating disc coupling reaction device | |
| CN209836096U (en) | Improved VCM production equipment | |
| CN106629755A (en) | Supergravity gas-liquid precipitation method for preparing silica nanoparticles based on rice hull ash | |
| CN208454515U (en) | A kind of reaction unit of negative pressure cobalt chloride carbonate synthesis cobalt | |
| CN207102398U (en) | Alkaline brine filter cellulose batch tank | |
| CN106629791B (en) | The device and technique of a kind of hypergravity-crystal seed method synthesizing superfine flame retardant of magnesium hydroxide | |
| CN203440102U (en) | Impinging stream-rotating disc coupling reaction device | |
| CN203636971U (en) | Brick making machine | |
| CN106735302B (en) | A kind of preparation method of Pt nanowires |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 225400 No. 8 Binjiang North Road, Taixing Economic Development Zone, Jiangsu Patentee after: Grammy (Jiangsu) cobalt industry Limited by Share Ltd Address before: 225400 Taixing Economic Development Zone, Jiangsu, Binjiang, North Road, No. 8, No. Patentee before: Jiangsu Cobalt Nickel Metal Co., Ltd. |
|
| CP03 | Change of name, title or address |