CN204737729U - Device of diamond is retrieved to chlorine - Google Patents
Device of diamond is retrieved to chlorine Download PDFInfo
- Publication number
- CN204737729U CN204737729U CN201520381662.8U CN201520381662U CN204737729U CN 204737729 U CN204737729 U CN 204737729U CN 201520381662 U CN201520381662 U CN 201520381662U CN 204737729 U CN204737729 U CN 204737729U
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- China
- Prior art keywords
- chlorine
- pipeline
- valve
- reactor
- absorption column
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- Expired - Fee Related
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Abstract
The utility model discloses a device of diamond is retrieved to chlorine, its characterized in that: add gaseous absorption and pressed devices such as warning with the accuse on reation kettle, gaseous absorbing device comprises the absorption column, pump, converter and the pipeline that link to each other with reation kettle with gas pipeline through the back bending pipe and arrange its top in, and the inlet piping of pump inserts the accumulator still bottom, and its exit end is continuous with absorption column top shower nozzle, and it is continuous with the liquid seal groove that the pipeline is passed through on the absorption column top, the accuse presses alarm device mainly to comprise accumulator still, the alarm of taking the floater, intercommunication valve and pipeline, sets up to be connected with the accumulator still bottom of being equipped with the alarm in the communicating pipe of reation kettle tail band flowing back valve and intercommunication valve. Above -mentioned device can make diamond waste product recovery process not have wastewater discharge.
Description
One, technical field
The present invention relates to the recycling of waste, particularly a kind of chlorine reclaims adamantine device.
Two, background technology
Diamond and graphite belong to the simple substance of carbon.Diamond is the hardest material of occurring in nature, is therefore also just provided with many important industrial uses, as fine grinding material, high hard parting tool, all kinds of drill bits etc.During present man-made diamond has been widely used in and has produced and live.China is diamond and diamond tool production and application big country, the diamond that annual consumption is a large amount of, also produces a large amount of diamond waste products.Except containing except expensive diamond particles in diamond waste product, also containing some, there is the very high material (as wolfram varbide, copper, cobalt, nickel etc.) recycling value.Therefore, be very significant to the recycling of diamond waste product.
The recovery of existing diamond waste product mainly adopts liquid-solid phase reaction method, namely uses acid dissolve metallic bond, filters to obtain diamond particles.But liquid-solid phase reaction method produces a large amount of brine wastes.If directly discharge, meeting severe contamination water body, if evaporation concentration extracts metal-salt, can produce a large amount of evaporative condenser waste water, also can produce pollution to environment.
Three, summary of the invention
The purpose of this utility model is the shortcoming for existing in existing diamond recovery method, provides a kind of chlorine not discharging evaporative condenser waste water to reclaim adamantine device.
Described chlorine reclaims adamantine device, it is characterized in that: on reactor, set up gas absorbing device, pressure control warning device and chlorine feedway.Described gas absorbing device is by be connected with reactor by return bent pipe and gas pipeline and the absorption column of side placed on it, pump, frequency transformer and pipeline form, the inlet pipeline of pump inserts bottom accumulator still, its exit end is connected with absorption column top shower nozzle, and absorption column top is connected with liquid seal trough by pipeline; Described pressure control warning device, primarily of accumulator still, the warning howler being with ball float, communicating valve and pipeline composition, is arranged on reactor tail band tapping valve and is connected with bottom the accumulator still that warning howler is housed the communicating pipe of communicating valve; Described chlorine feedway by being arranged on the weigher of placement chlorine cylinder of reactor side, the pipeline of band chlorine valve that reactor top is connected and chlorine distribution pipe form, the entrance end of chlorine valve is connected with the chlorine cylinder be placed on weigher, and exit end is connected with chlorine distribution pipe.
The invention has the beneficial effects as follows: due on the basis of original liquid-solid phase reaction method acid dissolve diamond waste product production equipment, gas absorbing device, pressure control warning device and chlorine feedway are set up, just can under tiny structure, adopt gas-liquid-solid method and chlorine to add water and produce acid fluid dissolves diamond waste product, avoid original technique purchase acid solution and bring a large amount of water, water in production process can be recycled, non-wastewater discharge.
Below in conjunction with accompanying drawing, the invention will be further described.
Four, accompanying drawing illustrates:
Fig. 1 is structural representation of the present invention.
In figure: 1 is kettle cover, 2 is gas pipeline, and 3 is return bent pipe, and 4 is filler, 5 is absorption column, and 6 is shower nozzle, and 7 is charging valve, 8 is pump, and 9 is frequency transformer, and 10 is warning howler, 11 is liquid seal trough, and 12 is ball float, and 13 is accumulator still, 14 is tapping valve, and 15 is reactor, and 16 is chlorine distribution pipe, 17 is weigher, and 18 is chlorine valve, and 19 is communicating valve.
Five, embodiment
As shown in Figure 1, it is on reactor 15, set up gas absorbing device, pressure control warning device and chlorine feedway.Described gas absorbing device is by be connected with reactor 15 by return bent pipe 3 and gas pipeline 2 and the absorption column 5 of side placed on it, pump 8, frequency transformer 9 and pipeline form, the inlet pipeline of pump 8 inserts bottom accumulator still 13, its exit end is connected with absorption column 5 top shower nozzle 6, and absorption column 5 top is connected with liquid seal trough 11 by pipeline; Described pressure control warning device, primarily of accumulator still 13, the warning howler 10 being with ball float 12, communicating valve 19 and pipeline composition, is arranged on reactor 15 tail band tapping valve 14 and is connected with bottom the accumulator still 13 that warning howler 10 is housed the communicating pipe of communicating valve 19; Described chlorine feedway by being arranged on the weigher 17 of placement chlorine cylinder of reactor 15 side, the pipeline of band chlorine valve 18 that reactor 15 top is connected and chlorine distribution pipe 16 form, the entrance end of chlorine valve 18 is connected with the chlorine cylinder be placed on weigher 17, and exit end is connected with chlorine distribution pipe 16.
When implementing the utility model, a certain amount of diamond waste product is dropped in reactor 15, covers kettle cover 1, open charging valve 7, be greater than the ratio of 1:3.15 according to diamond waste product and the mass ratio of water, add water in reactor, finish closedown charging valve 7.Ejector priming 8, close communicating valve 19, in reactor 15, rare gas element is discharged through liquid seal trough 11, and when three ball floats 12 all leave liquid level, pump 8 cuts out automatically.Open communicating valve 19, open chlorine valve 18 and pass into chlorine, reactor 15 liquid level declines, and accumulator still 11 liquid level rises.Instantly and in two ball floats 12 when being all submerged, pump 8 starts automatically, still liquid is delivered to absorption column 5 top, be sprayed onto filler 4 surface through shower nozzle 6, gas and liquid phase contact area is increased, chlorine absorption speed increases, cause reactor 15 pressure to decline rapidly, reactor 15 liquid level rises, and accumulator still 11 liquid level declines, instantly, when ball float 12 leaves liquid level, pump 8 cuts out automatically.Regulate chlorine valve 18, chlorine flowrate is controlled be in half work half resting state at pump 8.Along with the carrying out of reaction, in reactor 15, indifferent gas knows from experience constantly accumulation.Make lower ball float 12 leave liquid level when rare gas element is increased to, when pump 8 cannot be in half working order, slightly turn chlorine valve 18 down; Make down when rare gas element runs up to, in, lower three ball floats 12 are all submerged, and when warning howler 10 sends out a warning and reports to the police, close chlorine valve 18, after 5-10 minute, close communicating valve 19, repeat above-mentioned row's rare gas element and pass into chlorine operation, until when scrap metal all dissolves in reactor 15.Then, open kettle cover 1, cleaning reaction still 15.Process still liquid and scavenging solution, the water obtaining silicon carbide, tantalum, gold, copper, iron trichloride and can be recycled.
Claims (1)
1. a chlorine reclaims adamantine device, it is characterized in that having set up gas absorbing device on reactor (15), pressure control warning device and chlorine feedway, described gas absorbing device is connected and the absorption column (5) of side placed on it with reactor (15) with gas pipeline (2) by by return bent pipe (3), pump (8), frequency transformer (9) and pipeline composition, the inlet pipeline of pump (8) inserts accumulator still (13) bottom, its exit end is connected with absorption column (5) top shower nozzle (6), absorption column (5) top is connected with liquid seal trough (11) by pipeline, described pressure control warning device is primarily of accumulator still (13), the warning howler (10) being with ball float (12), communicating valve (19) and pipeline composition, and the communicating pipe being arranged on reactor (15) tail band tapping valve (14) and communicating valve (19) is connected with accumulator still (13) bottom that warning howler (10) are housed, described chlorine feedway by being arranged on the weigher (17) of placement chlorine cylinder of reactor (15) side, the pipeline of band chlorine valve (18) that reactor (15) top is connected and chlorine distribution pipe (16) form, the entrance end of chlorine valve (18) is connected with the chlorine cylinder be placed on weigher (17), and exit end is connected with chlorine distribution pipe (16).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520381662.8U CN204737729U (en) | 2015-06-06 | 2015-06-06 | Device of diamond is retrieved to chlorine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201520381662.8U CN204737729U (en) | 2015-06-06 | 2015-06-06 | Device of diamond is retrieved to chlorine |
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CN204737729U true CN204737729U (en) | 2015-11-04 |
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CN201520381662.8U Expired - Fee Related CN204737729U (en) | 2015-06-06 | 2015-06-06 | Device of diamond is retrieved to chlorine |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108786419A (en) * | 2018-06-23 | 2018-11-13 | 台州帆环保设备科技有限公司 | A variety of exhaust gas total systems |
-
2015
- 2015-06-06 CN CN201520381662.8U patent/CN204737729U/en not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108786419A (en) * | 2018-06-23 | 2018-11-13 | 台州帆环保设备科技有限公司 | A variety of exhaust gas total systems |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151104 Termination date: 20160606 |
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CF01 | Termination of patent right due to non-payment of annual fee |