CN204727824U - A kind of polymeric amide polycondensation reaction device - Google Patents
A kind of polymeric amide polycondensation reaction device Download PDFInfo
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- CN204727824U CN204727824U CN201520445379.7U CN201520445379U CN204727824U CN 204727824 U CN204727824 U CN 204727824U CN 201520445379 U CN201520445379 U CN 201520445379U CN 204727824 U CN204727824 U CN 204727824U
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Abstract
The utility model discloses a kind of polymeric amide polycondensation reaction device, and described polycondensation device comprises polycondensation vessel, Dropping feeder, the first pipe bundle condenser and the first airway; Described first pipe bundle condenser is connected with the internal cavities of described polycondensation vessel by described first airway, and described Dropping feeder comprises container for storing liquid, catheter and valve.Be provided with the first traverse baffle in described first pipe bundle condenser, described first traverse baffle is connected with the prolong in described first pipe bundle condenser.Described polycondensation vessel comprises polycondensation kettle and polycondensation kettle cover, and described polycondensation kettle comprises interior tank body and outer tank body.The utility model has the advantage automatically controlling temperature of reaction, improve processing safety and auto-alarm function.
Description
Technical field
The utility model relates to the preparation field of polymeric amide, particularly relates to a kind of polymeric amide polycondensation reaction device.
Background technology
Polyamide resin, is called for short PA, for main chain having the polymer of amido linkage.Can be obtained by diamine and diprotic acid polycondensation, lactan ring-opening polymerization.Multiple polyamide resin is obtained because diprotic acid used is different with the kind of diamine.High-molecular polyamide resin and low molecule pa resin is roughly divided into by the size of relative molecular weight.
High-molecular polyamide resin, namely the nylon known of people or polyamide fibre, be made up of straight-chain aliphatic diprotic acid and diamine, mainly for the preparation of synthon and engineering plastics, the class polyamide resin that R and D technics comparing is complete.Low molecule pa resin obtains, also known as dimer acid polyamide resin after carrying out polycondensation by dimeracid and diamine or polyamine.Two large classes can be divided into: non-reacted or neutral polyamide and reactive polyamide by its character.Neutral polyamide synthesizes, for the production of ink, hot melt adhesive and coating primarily of dimeracid and quadrol.
At present, its heating system of batch condensation polymerization reactor producing polymeric amide use is mostly electrically heated, because heating and temperature control is poor, causes Heating temperature too high or too low, thus has a strong impact on quality product.By heat-conducting oil heating if publication No. is a kind of heat-conducting oil heating reactor system as described in the patent application of CN103100361A, by adopting circulating heat conduction, ensure the constant temperature of reactor.But this heating means need the recycle system to be in working order all the time, guarantee temperature of reaction kettle constant, level of automation is low.And, though heat conduction chuck peripheral hardware has thermal insulation layer can play certain effect of heat insulation in the technical scheme of this patent application, but, because partial reaction requires that temperature is higher, heat can be made to penetrate thermofin come out, also can there is the harm of the staff that burns, lack the function near rear warning.
Utility model content
The utility model, for the deficiency of present technology, provides a kind of automatic control temperature of reaction, improves processing safety and has the polymeric amide polycondensation reaction device of auto-alarm function.
The utility model adopts following technique means to solve the problems of the technologies described above: a kind of polymeric amide polycondensation reaction device comprises polycondensation vessel, Dropping feeder, the first pipe bundle condenser and the first airway; Described first pipe bundle condenser is connected with the internal cavities of described polycondensation vessel by described first airway, and described Dropping feeder comprises container for storing liquid, catheter and valve; One end of described catheter is connected with the discharge port of described container for storing liquid, and the other end of described catheter extends in the internal cavities of described polycondensation vessel, and described valve is arranged on described catheter; Be provided with the first traverse baffle in described first pipe bundle condenser, described first traverse baffle is connected with the prolong in described first pipe bundle condenser; Described polycondensation vessel comprises polycondensation kettle and polycondensation kettle cover, and described polycondensation kettle comprises interior tank body and outer tank body, described outer tank body offers the first oil-in and the first oil outlet; Cavity place between described interior tank body and described outer tank body stores fluid, described kettle cover offers the 4th opening for feed; Described polycondensation device also comprises automatic temp controller, and described automatic temp controller comprises temperature sensor, circulating pipe, recycle pump, electrovalve and fuel reserve tank; Described temperature sensor is arranged in described outer tank body, and described recycle pump and described electrovalve are all arranged on described circulating pipe; Described fuel reserve tank offers the second oil-in and the second oil outlet, described circulating pipe comprises oil inlet pipe and oil outlet pipe; Described first oil-in is connected by described oil inlet pipe with described second oil outlet, and described first oil outlet is connected by described oil outlet pipe with described second oil-in.
Preferably: described polycondensation device also comprises thermal insulation protection cover, described polycondensation vessel is set in described thermal insulation protection cover.
Preferably: described recycle pump is arranged on described oil inlet pipe, and described electrovalve is arranged on described oil outlet pipe.
Preferably: described recycle pump is also provided with power regulator.
Preferably: the arranged outside of described thermal insulation protection cover has non-contact inductive warning device.
Preferably: described non-contact inductive warning device comprises infrared sensor, treater and acoustic-optic alarm; The output terminal of described infrared sensor is connected with the input terminus of described treater, and the output terminal of described treater is connected with the input terminus of described acoustic-optic alarm.
The utility model has the advantage of: in polycondensation device, arrange automatic temp controller, the signal sent by temperature sensor controls unlatching or the closedown of electrovalve, realizes the circulation of fluid in fluid in polycondensation vessel and fuel reserve tank, reaches the effect of automatic heat preserving.By arranging power regulator on recycle pump, regulate the speed of circulation.By arranging infrared sensor on thermal insulation protection cover, when there being staff near kettle, infrared sensor sends signal, after treated device process, drives acoustic-optic alarm to report to the police, improves the security of staff.
Accompanying drawing explanation
Fig. 1 is the structured flowchart of the utility model embodiment.
Fig. 2 is the structural representation of poly-unit in the utility model embodiment.
Fig. 3 is the structural representation of transfer still in the utility model embodiment.
Fig. 4 is the structural representation of centrifugal separating device in the utility model embodiment.
Fig. 5 is the structural representation of pipeline switch filtering device in the utility model embodiment.
Fig. 6 is the structural representation of flange in the utility model embodiment.
Fig. 7 is the structural representation of polycondensation device in the utility model embodiment.
Fig. 8 is the structural representation of filtration unit in the utility model embodiment.
Fig. 9 is the structural representation of distributor in the utility model embodiment.
Figure 10 is the structural representation of granulation transfer mechanism in the utility model embodiment.
Figure 11 is the structural representation of automatic spraying device in the utility model embodiment.
Figure 12 is the partial perspective view of granulation grading discharge mechanism in the utility model embodiment.
Figure 13 is the structural representation of granulation grading discharge mechanism in the utility model embodiment.
Embodiment
Below in conjunction with accompanying drawing, the utility model is described in detail.
As shown in Figure 1, the present embodiment comprises poly-unit, acidifying still, plate-and-frame filter press, transfer still, centrifugal separating device, thin-film evaporator, molecular distillation apparatus, pipeline switch filtering device, polycondensation device, filtration unit and granulating system from front to back successively by technical process.
Described acidifying still, described plate-and-frame filter press, described thin-film evaporator and described molecular distillation apparatus are existing installation.
As shown in Figure 2, poly-unit comprises polymeric kettle 101 and carries materials device 102, and described polymeric kettle 101 comprises polymerization kettle 1011 and polymerization kettle cover 1012, described polymerization kettle cover 1012 offers the first opening for feed 1013.Described materials device 102 of carrying comprises storage tank 1021, first lift pump 1022 and the first material guiding pipe 1023.One end of described first material guiding pipe 1023 is connected with described first opening for feed 1013, and the other end of described first material guiding pipe 1023 is connected with the discharge port of described storage tank 1021, and described first lift pump 1022 is arranged on described first material guiding pipe 1023.
As shown in Figure 3, described transfer still comprises transfer still shell body 401 and contact automatic alarm system 402, described transfer still shell body 401 offers the second opening for feed 403, and described contact autoalarm 402 comprises the first liquid level sensor 4021 and warning 4022.Described first liquid level sensor 402 is suspended in the internal cavities of described transfer still shell body 401, and described first liquid level sensor 4021 sends induced signal and drives described warning 4022 to send guard signal.
As shown in Figure 4, described centrifugal separating device comprises whizzer, separator tank and water shoot 503.Described whizzer comprises housing 5011, upper cover 5012, rotary drum 5013, light phase weir 5014, heavy phase weir 5015.Described rotary drum 5013 is arranged on the center of described housing 5011, and described light phase weir 5014 is arranged on the open area at described rotary drum 5013 top, and described heavy phase weir 5015 is arranged on the bottom of described upper cover 5012.Described housing 5011 offers the 3rd opening for feed 5016, first water-in 5017, light phase export 5018 and heavy out 5019.Described 3rd opening for feed 5016 and described first water-in 5017 are positioned at the below of described light phase export 5018 and described heavy out 5019.Described upper cover 5012 offers the first row mouth of a river 50110, and the described first row mouth of a river 50110 connects with described water shoot 503, described water shoot 503 is provided with the second lift pump 504.Described separator tank 502 is arranged on the below of described heavy out 5019, is provided with baffle plate 5023 in described separator tank 502, and the bottom of described baffle plate 5023 and the bottom of described separator tank 502 inwall exist gap.
The inwall of described rotary drum 5013 is offered and is equipped with temperature-control device 5021, described temperature-control device comprises temperature detector 50211, electronic heater 50212 and heating tube 50213, and the temperature test scope of described temperature detector 50211 is (50-100) DEG C.Its temperature range of water flowed into through described first water-in 5017 is (85-95) DEG C, and described baffle plate 5023 is welded on the sidewall of described separator tank 502 internal cavities, described separator tank is divided into the first cavity 5021 and the second cavity 5022.Described gap is (1-5) cm, described centrifugal separating device 5 also comprises heavy phase vent pipe 505, described heavy phase vent pipe 505 is provided with the 3rd lift pump 506, described heavy phase vent pipe 505 one end be connected with described heavy out 5019, the other end of described heavy phase vent pipe 5023 extends in described first cavity 5021 and (can extend in described second cavity 5022).Described heavy phase vent pipe 505 is connected with described heavy out 5019, and described separator tank is provided with the universal wheel 5024 that dynamic device stayed by band.
As seen in figs. 5-6, described pipeline switch filtering device comprises the first feed-pipe 701, surge tank 702, siphunculus more than first 703, several hay tanks 704, pipe connecting 705 and return line 706.Described return line 706 is provided with the 4th lift pump 707.Described siphunculus more than first 703 is Y-tube, and described Y-tube is made up of vertical tube 7031 and transverse tube 7032.Described hay tank 704 comprises the first hay tank 7041 and the second hay tank 7042.Described vertical tube 7031 is connected with the discharge port of described surge tank 702, one end of described transverse tube 7032 is connected with described first hay tank 7041 by the first flange 708, and the other end of described transverse tube 7031 is connected with described second hay tank 7042 by the second flange 709.The feeding mouth of described pipe connecting 705 is connected with the discharge port of described first hay tank 7041 (also can be connected with the discharge port of the second hay tank 7042) by three-flange 7010, and the discharge port of described pipe connecting 705 is connected with described return line 706 by the 4th flange 7011.Described vertical tube 7031 is also provided with main valve 7033, is provided with point valve 7034 at the two ends of described transverse tube 7031, all flanges include fixed flange 7015, mounting flange 7016 and fastening piece 7017.Described fixed flange 7015 connects into entirety by described fastening piece 7017 with described mounting flange 7016, also be provided with gasket 7018 between described fixed flange 7015 and mounting flange 7016, the surface-coated of described gasket 7018 has waterproof, preservative coat (not shown in FIG.).
As shown in Figure 7, described polycondensation device comprises polycondensation vessel 801, Dropping feeder 802, first pipe bundle condenser 803 and the first airway 804.Described first pipe bundle condenser 803 is connected with the internal cavities of described polycondensation vessel 801 by described first airway 804, and described Dropping feeder 802 comprises container for storing liquid 8021, catheter 8022 and valve 8023.One end of described catheter 8022 is connected with the discharge port of described container for storing liquid 8021, and the other end of described catheter 8022 extends in the internal cavities of described polycondensation vessel 801, and described valve 8023 is arranged on described catheter 8022.Be provided with the first traverse baffle 805 in described first pipe bundle condenser 803, described first traverse baffle 805 is connected with the prolong in described first pipe bundle condenser 803; Described polycondensation vessel 801 comprises polycondensation kettle 8011 and polycondensation kettle cover 8012, and described polycondensation kettle 8011 comprises interior tank body 80111 and outer tank body 80112, described outer tank body 80112 offers the first oil-in and the first oil outlet.Cavity place between described interior tank body 80111 and described outer tank body 80112 stores fluid, described kettle cover 8012 offers the 4th opening for feed.Described polycondensation device 8 also comprises automatic temp controller 805, and described automatic temp controller 805 comprises temperature sensor 8051, circulating pipe, recycle pump 8053, electrovalve 8054 and fuel reserve tank 8055.Described temperature sensor 8051 is arranged in described outer tank body 80112, and described recycle pump 8053 and described electrovalve 8054 are all arranged on described circulating pipe.Described fuel reserve tank 8055 offers the second oil-in and the second oil outlet, described circulating pipe 8055 comprises oil inlet pipe 80551 and oil outlet pipe 80552.Described first oil-in is connected by described oil inlet pipe 80551 with described second oil outlet, and described first oil outlet is connected by described oil outlet pipe 80552 with described second oil-in.
Described polycondensation device also comprises thermal insulation protection cover 806, and described polycondensation vessel 801 is set in described thermal insulation protection cover 806.Described recycle pump 8053 is arranged on described oil inlet pipe 80551, and described electrovalve 8054 is arranged on described oil outlet pipe 80552.Described recycle pump 8053 is also provided with power regulator 8058.The arranged outside of described thermal insulation protection cover 806 has non-contact inductive warning device 807, and described non-contact inductive warning device 807 comprises infrared sensor, treater and acoustic-optic alarm.The output terminal of described infrared sensor is connected with the input terminus of described treater, and the output terminal of described treater is connected with the input terminus of described acoustic-optic alarm.
As shown in Figure 8, described filtration unit comprises strainer 901, second feed-pipe 902, first discharge nozzle 903 and oil pipe 904.Described second feed-pipe 902 comprises pipe 9021 and the second charging outer tube 9022 in the second charging, and described first discharge nozzle 903 comprises pipe 9031 and the first discharging outer tube 9032 in the first discharging, and the cavity place between interior pipe outer tube corresponding thereto stores fluid.Described second charging outer tube 9022 is connected with one end of described oil pipe 904, and described first discharging outer tube 9032 is connected with the other end of described oil pipe 904.In described first discharging, in pipe 9031 and described second charging, pipe 9021 all communicates with the internal cavities of described strainer 901.
Described filtration unit also comprises the 5th flange 905 and the 6th flange 906, described second charging outer tube 9022 is connected by described 5th flange 905 with one end of described oil pipe 904, and described first discharging outer tube 9032 is connected by the 6th flange 907 with the other end of described oil pipe 904.Described oil pipe 904 is also provided with automatic heating device 907, and described heating unit 907 comprises temperature regulator and well heater, and described well heater is also provided with portable power source interface 908.Described temperature regulator comprises display screen and control device, described control device is provided with USB interface 909.Described strainer 901 comprises protective housing 9011 and is arranged on the filter assemblies 9012 of described protective housing inside.
As shown in Figure 1, described granulating system comprises granulating mechanism, granulation transfer mechanism and granulation grading discharge mechanism from front to back successively according to technical process.
As shown in figs. 9-10, described granulating mechanism comprises distributor and transmission mechanism, and described distributor comprises granulating cylinder 100111 and pellet device 100112.Described pellet device 100112 comprises grain-cutter 1001121 and transmission shaft 1001122, described grain-cutter 1001121 is set in described transmission shaft 1001122, the main part of described transmission shaft 1001122 is housed in the cavity of described granulating cylinder 100111, and the two ends of described transmission shaft 1001122 are all extended outside the cavity of described granulating cylinder 100111.The bottom of described granulating cylinder 100111 offers several regularly arranged material holes 100113, and the top of described granulating cylinder 100111 offers spout 100114, described material hole 100113, described spout 100114 and described cavity intercommunication.Described transmission mechanism comprises motor 100122, first gear 100121, second gear 100123 and chain 100124, described chain 100124 is set on described first gear 100121 and the second gear 100123, the output shaft of described motor 100122 is connected with described first gear 100121, and described second gear 100123 is connected with the end of described transmission shaft 1001122.
Described transmission mechanism also comprises Tension gear 100125, and described Tension gear 100125 is between described first gear 100122 and described second gear 100123 and be arranged on the inner side of described chain 100124.The diameter in described material hole 100113 is 0.8mm, and the arranged outside of described spout 100114 has sealing cover 100115, and described sealing cover 100115 adopts with described spout 100114 and is threaded.Described granulating mechanism also comprises two secondary bracing frames 10013; described two secondary bracing frames 10013 are oppositely arranged; two ends of described granulating cylinder 100111 are arranged on corresponding bracing frame 10013, and described grain-cutter 1001121 is set in described transmission shaft 1001122 in the shape of a spiral.
As shown in figs. 10-11, described granulation transfer mechanism comprises e Foerderanlage, and the particle flowed out through granulating cylinder 100111 transmits by described e Foerderanlage.Described e Foerderanlage comprises motion-work wheel 100211, follow-up pulley 100212 and drapery panel 100213, and described drapery panel 100213 is set on described motion-work wheel 100211 and follow-up pulley 100212.Described e Foerderanlage also comprises some pieces and pats plate 100214, the described plate 100214 that pats is fixed on lower layer mix feeding plate 100213 perpendicular to the throughput direction of described drapery panel, and the length direction patting plate 100214 described in ensureing parallels with the width of described drapery panel 100213.Several automatic spraying devices 10022 are also provided with in the side of described e Foerderanlage.The top of described e Foerderanlage is also provided with waste gas collection device, and described waste gas collection device comprises extractor fan 100231 and ventilator trunk 100232.Described extractor fan 100231 is arranged on the top of described granulating cylinder 100111, one end of described ventilator trunk 100232 is connected with described extractor fan 100231, and the length direction that the other end of described ventilator trunk 100231 is parallel to described e Foerderanlage extends to the top of described delivery device tip.The bottom of described ventilator trunk 100232 is provided with some row's ventilation holes 100233.
The described length patting plate 100214 is not shorter than the width of described drapery panel 100213, described in pat plate 100214 bottom be coated with smooth layer (not shown in FIG.).The described two ends patting plate 100214 length direction are welded with fixed link (not shown in FIG.) respectively, and the bottom of described fixed link fixes on the ground.Described automatic spraying device 10022 comprises shower nozzle 100221, heat inductor block, receiver, electric controller, water pump 100222 and water tank 100223.Described shower nozzle 100221 is fixed on the top of described drapery panel 100213, and described heat inductor block is distributed in order to test the heat that on drapery panel 100213, particle distributes.The signal that described receiver sends in order to accept described heat inductor block, described pneumoelectric controller accepts information that described receiver sends and drives described water pump 100222 to draw water by motor.
As illustrated by figs. 12-13, described granulation grading discharge mechanism comprise scraper 10031, sieve 10032, lower funnel 10033, blower 10034, tripping device 10035, second discharge nozzle 10036, floss collection device 10037 and siphunculus more than second 10038.The edge of a knife of described scraper 10031 abuts on the drapery panel 100213 of described delivery device tip, described sieving 10032 is arranged on the below of described scraper 10031 and is fixed on the opening end of described lower funnel 10033, the bottom of described lower funnel 10033 with described siphunculus more than second 10038 to being communicated with.The inlet end of described siphunculus more than second 10038 is provided with described blower 10034, the outlet of described porous pipe line is connected with the entrance of described tripping device 10035, described tripping device 10035 offers floss outlet, the bottom of described tripping device 10035 offers discharge port.Described floss outlet 10035 is connected with described floss collection device 10037 by described second material guiding pipe 10036.Described second discharge nozzle 10036 is connected with the discharge port of described tripping device 10035.The discharge outlet of described tripping device 10035 is provided with side tool lock 100310, and described second material guiding pipe 10036 is provided with the 5th lift pump 100311.
Described sieve 10032 mesh diameter be (0.6-1.1) mm, the opening end bore of described lower funnel 10033 and described sieve 10032 equal and opposite in direction.Described side tool lock 100310 comprises blocking material plate 1003101 and handle of a knife 1003102, one end of described blocking material plate 1003101 and the discharge port of described tripping device 10035 hinged, the other end of described blocking material plate 1003101 is provided with described handle of a knife 1003102.Described blower fan 10034 is also provided with Power Conditioning Unit 100341, and described Power Conditioning Unit 100341 is transformer.Described granulation grading discharge mechanism also comprises two pieces of retaining plates 10039, and described two pieces of retaining plates 10039 are oppositely arranged on the both sides of the end of described e Foerderanlage.Every block fixed block 10039 is provided with groove 100391, the two ends of described scraper 10031 are welded with screw rod 100311 respectively, described screw rod 100311 adopts with described groove 100391 and is slidably connected, every root screw rod 100311 is also arranged with two nuts 100312, nut is close to the both sides of corresponding groove respectively.
The production method of the present embodiment comprises the following steps:
1) vegetable oil acid, carclazyte, Quilonum Retard and water are added in polymeric kettle, carry out polyreaction;
2) acidifying is carried out by the product press-in acidifying still after polymerization;
3) by plate-and-frame filter press, the product after acidifying is filtered, obtain rough dimeracid;
4) keep in rough dimeracid press-in transfer still;
5) rough dimeracid is fed in centrifugal separating device, and mix with hot water, carry out centrifugation;
6), in the product feeding thin-film evaporator after centrifugation, distill, removing steam;
7) product after thin-film evaporator process is fed in molecular distillation apparatus, be separated;
8) surge tank and pre-filtering is entered by the smart dimeracid feeding pipeline switch filtering device obtained after separation;
9) product press-in polycondensation vessel pre-filtering obtained, drips quadrol simultaneously and carries out polycondensation;
10) by filtration unit, the product after polycondensation is filtered;
11) carry out granulation by the product feeding granulating system after filtration, obtain product.
Described step 1) in the vegetable oil acid that the uses one that is behenic acid or cotton oil acid, the mass ratio of described vegetable oil acid, described carclazyte, described Quilonum Retard and described water is 100:10:0.5:1.5; The temperature of reaction of described polyreaction is 230 DEG C, and the reaction times of polyreaction is (3-4) h;
Described step 2) in the souring agent that uses be phosphoric acid, described phosphoric acid and product quality after described polymerization are than being 3:100; Reaction process is: acidificatoin time is 1h, and temperature of reaction is (150-180) DEG C;
Described step 5) in add water temperature be (85-95) DEG C;
Described step 6) vaporization temperature be 160 DEG C;
Described step 7) separation temperature be 230 DEG C, vacuum tightness is below 30Pa;
Described step 9) in dimeracid after pre-filtering be 1:1 with the mol ratio of quadrol, react and comprise following several stages:
8.1) the dimeracid heating phase, Heating temperature is (125-133) DEG C;
8.2) the dropping stage of quadrol, time for adding is (25-35) min;
8.3) intensification polycondensation phase, temperature rises to (190-205) DEG C;
8.4) the constant temperature stage, temperature controls as (215-225) DEG C; The isothermal reaction time is (3-4) h;
8.5) decompression phase, reduces pressure under 5mmHg.
The present embodiment, by being added in polymeric kettle 101 by vegetable oil acid, carclazyte, Quilonum Retard and water, carries out polyreaction, and the heavy metal ion in absorption reaction thing, then carry out acidifying by the product press-in acidifying still after polymerization; By plate-and-frame filter press, the product after acidifying is filtered, obtain rough dimeracid, keep in rough dimeracid press-in transfer still.By feeding rough dimeracid in centrifugal separating device, and mix with hot water, carry out centrifugation, the product after centrifugation feeds in thin-film evaporator and molecular distillation apparatus successively, carries out distilling, being separated, obtains smart dimeracid.The smart dimeracid feeding obtained after distillation is entered people's surge tank 702 and pre-filtering tank 704 to pipeline switch filtering device; The product press-in polycondensation vessel 801 pre-filtering obtained, drips quadrol simultaneously and carries out polycondensation; By filtration unit, the product after polycondensation is filtered again; Carry out granulation by the product feeding granulating system after filtration, obtain product.
The foregoing is only the preferred embodiment that the utility model is created; do not create in order to limit the utility model; the any amendment done within all spirit of creating at the utility model and principle, equivalent to replace and improvement etc., all should be included within protection domain that the utility model creates.
Claims (6)
1. a polymeric amide polycondensation reaction device, comprise polycondensation vessel, Dropping feeder and the first pipe bundle condenser, it is characterized in that: described first pipe bundle condenser is connected by the internal cavities of the first airway with described polycondensation vessel, and described Dropping feeder comprises container for storing liquid, catheter and valve; One end of described catheter is connected with the discharge port of described container for storing liquid, and the other end of described catheter extends in the internal cavities of described polycondensation vessel, and described valve is arranged on described catheter; Be provided with the first traverse baffle in described first pipe bundle condenser, described first traverse baffle is connected with the prolong in described first pipe bundle condenser; Described polycondensation vessel comprises polycondensation kettle and polycondensation kettle cover, and described polycondensation kettle comprises interior tank body and outer tank body, described outer tank body offers the first oil-in and the first oil outlet; Cavity place between described interior tank body and described outer tank body stores fluid, described kettle cover offers the 4th opening for feed; Described polycondensation device also comprises automatic temp controller, and described automatic temp controller comprises temperature sensor, circulating pipe, recycle pump, electrovalve and fuel reserve tank; Described temperature sensor is arranged in described outer tank body, and described recycle pump and described electrovalve are all arranged on described circulating pipe; Described fuel reserve tank offers the second oil-in and the second oil outlet, described circulating pipe comprises oil inlet pipe and oil outlet pipe; Described first oil-in is connected by described oil inlet pipe with described second oil outlet, and described first oil outlet is connected by described oil outlet pipe with described second oil-in.
2. a kind of polymeric amide polycondensation reaction device according to claim 1, is characterized in that: described polycondensation device also comprises thermal insulation protection cover, and described polycondensation vessel is set in described thermal insulation protection cover.
3. a kind of polymeric amide polycondensation reaction device according to claim 1, is characterized in that: described recycle pump is arranged on described oil inlet pipe, and described electrovalve is arranged on described oil outlet pipe.
4. a kind of polymeric amide polycondensation reaction device according to claim 1, is characterized in that: described recycle pump is also provided with power regulator.
5. a kind of polymeric amide polycondensation reaction device according to claim 2, is characterized in that: the arranged outside of described thermal insulation protection cover has non-contact inductive warning device.
6. a kind of polymeric amide polycondensation reaction device according to claim 5, is characterized in that: described non-contact inductive warning device comprises infrared sensor, treater and acoustic-optic alarm; The output terminal of described infrared sensor is connected with the input terminus of described treater, and the output terminal of described treater is connected with the input terminus of described acoustic-optic alarm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520445379.7U CN204727824U (en) | 2015-06-25 | 2015-06-25 | A kind of polymeric amide polycondensation reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520445379.7U CN204727824U (en) | 2015-06-25 | 2015-06-25 | A kind of polymeric amide polycondensation reaction device |
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| CN204727824U true CN204727824U (en) | 2015-10-28 |
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| CN201520445379.7U Withdrawn - After Issue CN204727824U (en) | 2015-06-25 | 2015-06-25 | A kind of polymeric amide polycondensation reaction device |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104910375A (en) * | 2015-06-25 | 2015-09-16 | 安庆市虹泰新材料有限责任公司 | Polyamide polycondensation reactor |
| CN109806828A (en) * | 2019-02-27 | 2019-05-28 | 黄山天马新材料科技有限公司 | A kind of organo silane coupling agent reaction kettle |
-
2015
- 2015-06-25 CN CN201520445379.7U patent/CN204727824U/en not_active Withdrawn - After Issue
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104910375A (en) * | 2015-06-25 | 2015-09-16 | 安庆市虹泰新材料有限责任公司 | Polyamide polycondensation reactor |
| CN109806828A (en) * | 2019-02-27 | 2019-05-28 | 黄山天马新材料科技有限公司 | A kind of organo silane coupling agent reaction kettle |
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