CN204705529U - The extraction element of acid non-soluble substance in carbonatite - Google Patents
The extraction element of acid non-soluble substance in carbonatite Download PDFInfo
- Publication number
- CN204705529U CN204705529U CN201520383139.9U CN201520383139U CN204705529U CN 204705529 U CN204705529 U CN 204705529U CN 201520383139 U CN201520383139 U CN 201520383139U CN 204705529 U CN204705529 U CN 204705529U
- Authority
- CN
- China
- Prior art keywords
- reactor
- filter membrane
- filter plate
- extraction element
- soluble substance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model discloses the extraction element of acid non-soluble substance in a kind of carbonatite, this extraction element comprises reactor and filtrator, reactor is made by the PVC material of acid corrosion-resistant, the bottom of reactor offers the opening that can stretch into stirrer, opening part is provided with cock body with matching, filter bits is in the top of reactor, and form seamless link between its outer edge and outer peripheral face of reactor head, filtrator comprises filter membrane one, for supporting the filter plate of described filter membrane one and the hold assembly for fixing described filter membrane one and filter plate, the middle part of described hold assembly is cylindricality, inward at both ends extends into annular.The extraction element that the utility model provides and method, make whole reaction, filtration, cleaning process carry out all in the reactor, changing filtration into simultaneously, greatly saving leaving standstill the sample preparation time, decreasing the loss preparing acid non-soluble substance in sample.
Description
Technical field
The utility model relates to carbonatite mineral extraction and analysis technical field, is specifically related to the extraction element of acid non-soluble substance in a kind of carbonatite.
Background technology
Often need to pay close attention to the secondary mineral except carbonate mineral (kalzit, rauhkalk etc.) in carbonatite research, the ground of these secondary mineral changes into point, combination form, composition and content etc. have great importance for research sedimentary environment, Diagn, and therefore how extraction acid non-soluble substance more rapidly and efficiently has just become the problem needing to solve.
Extraction at present for mineral secondary in carbonatite adopts acid extracting often, namely in reaction vessel, adds sample and excess acid makes it react, and gets acid non-soluble substance research after precipitation cleaning.And in this process, often react thoroughly, part mineral be also removed with supernatant when removing supernatant after precipitation, simultaneously because mineral grain is tiny, precipitation process needs the plenty of time, if sample size is many, the time of needs will be longer.
Utility model content
The purpose of this utility model is the extraction element providing acid non-soluble substance in a kind of carbonatite, this extraction element can save the time that acid non-soluble substance extracts greatly, thus raising extraction efficiency, and the situation that the mineral owing to causing when toppling over supernatant fluid run off can be avoided.
The extraction element of acid non-soluble substance in a kind of carbonatite, comprise reactor and filtrator, described reactor is made by the PVC material of acid corrosion-resistant, the bottom of described reactor offers the opening that can stretch into stirrer, described opening part is provided with cock body with matching, described filter bits is in the top of reactor, and form seamless link between the outer peripheral face of its outer edge and described reactor head, described filtrator comprises filter membrane one, for supporting the filter plate one of described filter membrane one, for fixing hold assembly and the filter plate two of described filter membrane one and filter plate one, described hold assembly is quality of rubber materials, the middle part of described hold assembly is cylindricality, inward at both ends extends into annular, be respectively the annular one being positioned at top and the annular two being positioned at bottom, described filter plate one is fastened in described annular one, described filter membrane one is laid on towards on the filter plate one of described inside reactor side, the inwall of described hold assembly is provided with the packing ring preventing described filter membrane one slide downward, described filter plate two is arranged on the below of filter membrane one.
This extraction element comprises reactor and filtrator, reaction can be guaranteed and filter in same container, avoid the loss of mineral matter, and opening is set in the bottom of reactor, this opening is sealed condition in the stage of reaction, extraction element can be inverted at later stage filtration stage, in this opening, put into stirrer stir, to prevent problem that the filter membrane of filtrator blocks in filter process.
Above-mentioned filtrator, by the back up pad of filter plate one as filter membrane one, filter membrane one is laid and is fitted on filter plate, the filter membrane one of filtration condition fits tightly on filter plate one, and the inwall of hold assembly is provided with packing ring, this packing ring is quality of rubber materials, can prevent filter membrane one from gliding in filtration condition, avoid the loss of acid non-soluble substance; Be hollow cylindrical in the middle part of hold assembly, the annular one that its inward at both ends extends and annular two, closely can be fastened on the periphery of filter plate and reactor head, filter plate two plays the effect of filtration.
As a preferred version of the present utility model, above-mentioned annular one is provided with the pillar supporting reactor.
When filtering, reactor need be inverted, arranging pillar is to make the reactor after inversion stablize on the one hand, can facilitate the outflow of liquid in reactor on the one hand, is convenient to collect.
As another preferred version of the present utility model, the outer peripheral face of above-mentioned reactor head is provided with screw thread, and above-mentioned annular two entirety is nested with on above-mentioned screw thread.
Annular two is quality of rubber materials, reactor is PVC material, and when the screw thread of reactor head outer peripheral face and annular two fasten, the existence due to screw thread increases friction force therebetween, make to fasten more tight therebetween, during to guarantee that reactor is inverted, liquid can not seepage.
Further, above-mentioned filtrator also comprises filter membrane two, and above-mentioned filter membrane two is arranged on the bottom surface of filter plate two, and the below of above-mentioned hold assembly inwall packing ring is provided with draw-in groove, and above-mentioned filter membrane two and filter plate two are fastened in above-mentioned draw-in groove.
The aperture of filter membrane two can be greater than the aperture of filter membrane one, is equivalent to carry out double medium filtration to the mixed liquor in reactor.
Further, the outer wall of reactor is provided with scale.
First powder and acid join in reactor to mix and react by the utility model, after having reacted, do not need secondary transferring, reactor is inverted and can filtration be completed by beating action, compared with traditional method, the utility model single stage method can complete the extraction of acid non-soluble substance, and in same reactor, the loss of acid non-soluble substance can be avoided, improve its yield.
The extraction element that the utility model provides, makes whole reaction, filtration, cleaning process carry out all in the reactor, changing filtration into simultaneously, greatly saving leaving standstill the sample preparation time, decreasing the loss preparing acid non-soluble substance in sample.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the utility model is described in further details:
Fig. 1 is the diagrammatic cross-section of the utility model extraction element;
Fig. 2 is the utility model filtration condition schematic diagram;
Fig. 3 is the side view of the utility model extraction element;
In figure, 1, reactor, 2, scale, 3, hold assembly, 4, filter membrane two, 5, filter membrane one, 6, filter plate one, 7, pillar, 8, opening, 9, motor, 10, shaft, 11, helical-blade oar.
Embodiment
Elaborate below in conjunction with specific embodiment.
As shown in Figure 1, the utility model, the extraction element of acid non-soluble substance in carbonatite, it is mainly used for extracting the acid non-soluble substance in carbonatite, this extraction element comprises reactor 1, filtrator and stirrer three parts, the reaction of carbonatite powder and acid is there is in reactor 1, therefore, the material of reactor 1 is the PVC material of anti-acid corrosion, the capacity of reactor 1 can be determined according to actual conditions, the utility model preferred reactor 1 is column, the periphery wall of reactor 1 is carved with scale 2, scale 2 mark has 0ml, the printed words such as 500ml and 1000ml, this reactor head does not have lid, centre position bottom it is provided with opening, opening 8 is opened for installing stirrer sometimes with cock body shutoff sometimes.
Under normal circumstances, by after carbonatite and acid reaction in prior art, then transfer in another filtration unit and filter, collect acid non-soluble substance, the utility model arranges filtrator at the top of reactor, filtrator is by hold assembly, filter membrane one, filter membrane two and filter plate form, wherein, filter plate is provided with two, be respectively the filter plate one being positioned at hold assembly top and the filter plate two be positioned in the middle part of hold assembly, the filter plate one at top is for supporting filter membrane one, the filter plate two at middle part plays the effect of filtration, as shown in Figure 3, hold assembly 3 is column in the middle part of it, the inward at both ends of column extends to form annular, the annular being positioned at top is defined as annular one, the annular being positioned at bottom is defined as annular two, because annular one has the part extended internally, its extended spot can block establishes filter plate 1, filter plate 1 one side down lays filter membrane 1, filter membrane one is also that the extended spot being located at annular one by its edge card fixes, in order to when preventing from filtering, filter membrane one occurs glide thus cause acid non-soluble substance to flow out from filter, packing ring can be laid at the inwall of the inwall of hold assembly and column, packing ring is also select quality of rubber materials, can prevent filter membrane one from moving down, in order to ensure the collecting amount of acid non-soluble substance, the utility model, preferably by two-layer filtration, namely arranges filter membrane 24 at the hold assembly inwall of side near reactor further, filter membrane 24 filter bores can be greater than the filter bores of filter membrane 1.
Above-mentioned hold assembly also can be two parts separately, namely be positioned at the hold assembly one of top and be positioned at the hold assembly two of below, hold assembly two is nested with in hold assembly one, namely the top of hold assembly two is provided with screw thread, inserted in hold assembly one by rotating hold assembly two, and filter membrane 24 can be fixed on the junction of hold assembly one and hold assembly two, this structure is convenient to be changed filter membrane one, filter membrane two, filter membrane one and the position of filter plate one and the identical of foregoing description.
Preferably, filtrator also comprises filter membrane two, and filter membrane two is arranged on the bottom surface of filter plate two, and the below of hold assembly inwall packing ring is provided with draw-in groove, and filter membrane two and filter plate two are fastened in draw-in groove.
This extraction element needs to be inverted at later stage filtration stage, therefore, sealing is guaranteed in junction between above-mentioned filtrator and reactor, the outer peripheral face of reactor head is laid the screw thread of some, then filtrator is by being fastened on the screw thread of reactor head by annular two, friction between screw thread and annular two strengthens, and annular two is quality of rubber materials, the seamless link completely namely formed between filtrator and reactor can be sealed, the conveniently outflow of supernatant, the top of filtrator and annular one are provided with three pillars 7, three pillars 7 are triangularly arranged.
As shown in Figure 2, after carbonatite in reactor 1 and acid reaction complete, reactor 1 need be inverted, three root posts 7 are positioned at bottom, support this reactor 1, after inversion, the cock body being used for sealed open 8 is opened, stirrer is laid from this opening part, stirrer is identical with conventional whisk structure of the prior art, respectively by shaft 10, the motor 9 driving shaft 10 to rotate and the helical-blade oar 11 be positioned at bottom shaft 9 form, the large I of motor 9 covers this opening 8 completely, shaft 10 stretches into the correct position in reactor 1, namely the position that supernatant is discharged is not stopped, specifically stretch into the degree of depth can according to the mixed liquor of the volume of reactor and carbonatite and acid number decide, when need filter, can by electrical power, thus drive shaft and helical-blade oar 11 to rotate, prevent mixed liquor by plugged filter.
Introduce the extracting method of the utility model extraction element below in detail, comprise the following steps successively:
Choosing and pulverizing of step 1, rock sample: choose clean, unpolluted carbonatite rock sample, is crushed to floury in vibromill, gets 10g and is placed in sample sack for subsequent use;
Step 2, keep the cock body of reactor bottom be sealing state, above-mentioned powder joined in reactor, then in reactor, adds 1L acid, reaction a period of time, question response no longer bubbling time stop reacting;
After step 3, mounting filter, reactor is inverted, opens cock body, load stirrer and start stirring;
Dynamic filtration process is in step 4, whipping process, solid matter and mineral matter are stayed in reactor, liquid substance and supernatant are through filtrator, after filtration completes, cock body is installed, reaction vessel is just come, open filtration unit, and clear up, the acid non-soluble substance of collection is rejoined in reaction vessel, filtration unit is installed after rejoining acid reaction and repeats above-mentioned steps.Acid dissolution will be in triplicate;
Step 5, filtered washing and by supernatant discharge, by reactor acid non-soluble substance take out, get final product deployment analysis after natural drying.
It should be noted that; the shape of above-mentioned reactor also can be transformed to taper, irregular cylindricality etc. according to actual needs; those skilled in the art are under enlightenment of the present utility model, and the replacement that can also make, simple deformation all should within protection domains of the present utility model.
Claims (5)
1. the extraction element of acid non-soluble substance in a carbonatite, comprise reactor and filtrator, described reactor is made by the PVC material of acid corrosion-resistant, it is characterized in that: the bottom of described reactor offers the opening that can stretch into stirrer, described opening part is provided with cock body with matching, described filter bits is in the top of reactor, and form seamless link between the outer peripheral face of its outer edge and described reactor head, described filtrator comprises filter membrane one, for supporting the filter plate one of described filter membrane one, for fixing hold assembly and the filter plate two of described filter membrane one and filter plate one, described hold assembly is quality of rubber materials, the middle part of described hold assembly is cylindricality, inward at both ends extends into annular, be respectively the annular one being positioned at top and the annular two being positioned at bottom, described filter plate one is fastened in described annular one, described filter membrane one is laid on towards on the filter plate one of described inside reactor side, the inwall of described hold assembly is provided with the packing ring preventing described filter membrane one slide downward, described filter plate two is arranged on the below of filter membrane one.
2. the extraction element of acid non-soluble substance in carbonatite according to claim 1, is characterized in that: described annular one is provided with the pillar supporting described reactor.
3. the extraction element of acid non-soluble substance in carbonatite according to claim 1, it is characterized in that: the outer peripheral face of described reactor head is provided with screw thread, described annular two entirety is nested with on described screw thread.
4. the extraction element of acid non-soluble substance in carbonatite according to claim 1, it is characterized in that: described filtrator also comprises filter membrane two, described filter membrane two is arranged on the bottom surface of filter plate two, the below of described hold assembly inwall packing ring is provided with draw-in groove, and described filter membrane two and filter plate two are fastened in described draw-in groove.
5. the extraction element of acid non-soluble substance in carbonatite according to claim 1, is characterized in that: the outer wall of described reactor is provided with scale.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520383139.9U CN204705529U (en) | 2015-06-04 | 2015-06-04 | The extraction element of acid non-soluble substance in carbonatite |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520383139.9U CN204705529U (en) | 2015-06-04 | 2015-06-04 | The extraction element of acid non-soluble substance in carbonatite |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204705529U true CN204705529U (en) | 2015-10-14 |
Family
ID=54285134
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520383139.9U Active CN204705529U (en) | 2015-06-04 | 2015-06-04 | The extraction element of acid non-soluble substance in carbonatite |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204705529U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104880352A (en) * | 2015-06-04 | 2015-09-02 | 山东科技大学 | Extraction device and extraction method for acid non-soluble substances in carbonatite |
-
2015
- 2015-06-04 CN CN201520383139.9U patent/CN204705529U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104880352A (en) * | 2015-06-04 | 2015-09-02 | 山东科技大学 | Extraction device and extraction method for acid non-soluble substances in carbonatite |
| CN104880352B (en) * | 2015-06-04 | 2017-09-01 | 山东科技大学 | The extraction element and extracting method of acid non-soluble substance in carbonate rock |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN204705529U (en) | The extraction element of acid non-soluble substance in carbonatite | |
| CN210079002U (en) | High-efficiency processor for swill | |
| CN104880352A (en) | Extraction device and extraction method for acid non-soluble substances in carbonatite | |
| CN203816550U (en) | Stirring device of silicon slice grinding fluid | |
| CN209500877U (en) | A kind of active skull cap components extraction element | |
| CN106984216A (en) | A kind of new preliming tank agitating device | |
| CN105833761B (en) | A kind of agitating device prepared by biological medicine | |
| CN205413022U (en) | Stirring device of reaction kettle | |
| CN211864098U (en) | Filter equipment is used in sour milk drink fermentation preparation | |
| CN210057973U (en) | Mixing arrangement is used in ferment processing | |
| CN208553202U (en) | A kind of supercritical carbon dioxide extraction apparatus | |
| CN205907254U (en) | Straw fermentation preparation marsh gas and fertilizer all -in -one | |
| CN218553945U (en) | Cubic crystallization cleaning device of mixed acid stirred tank | |
| CN204746322U (en) | High -efficient electrolyte reation kettle of convenient sample | |
| CN215743207U (en) | Medicinal material evaporates and glues thick cream liquid agitating unit | |
| CN205850839U (en) | A kind of organosilicon produces uses chemical reaction still | |
| CN210729252U (en) | Agitator of collapsible type | |
| CN204933355U (en) | A kind of pesticide producing agitating device | |
| CN217773826U (en) | Lithium manganate battery production is with mixing thick liquid device of selecting separately lithium from fluorite tailing | |
| CN214599421U (en) | Coal slime pulper | |
| CN207632813U (en) | A kind of barley beta-amylase extraction system | |
| CN212974251U (en) | Soil screen filter | |
| CN220176102U (en) | Plant juice composition extraction element | |
| CN213738692U (en) | A aeration mechanism for kitchen garbage oil extraction device | |
| CN214553295U (en) | Low-concentration slurry material stirring barrel convenient for discharging |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |