CN204582595U - A kind of separator of fusel oil - Google Patents

A kind of separator of fusel oil Download PDF

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Publication number
CN204582595U
CN204582595U CN201520285898.1U CN201520285898U CN204582595U CN 204582595 U CN204582595 U CN 204582595U CN 201520285898 U CN201520285898 U CN 201520285898U CN 204582595 U CN204582595 U CN 204582595U
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CN
China
Prior art keywords
tank body
column plate
plate
separator
separator according
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Expired - Fee Related
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CN201520285898.1U
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Chinese (zh)
Inventor
邹刚
王伦
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Individual
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Individual
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Priority to CN201520285898.1U priority Critical patent/CN204582595U/en
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Abstract

The utility model discloses a kind of separator of fusel oil, comprise: tank body, be arranged at multiple material inlets of tank body sidepiece, be arranged at light fraction outlet and the outlet of multiple heavy constituent of tank body top and bottom, this separator also comprises the multiple column plates being arranged at tank interior, and being arranged at multiple draining plates of tank body madial wall, column plate partly overlaps along the axial bearing of trend of tank body.By arranging multiple column plate and multiple draining plate in tank body, achieving the effect of the component of different boiling being carried out efficient Separation & Purification, improve the separating effect to fusel oil significantly; Be convenient to cleaning, structure is simple, and security is higher simultaneously.

Description

A kind of separator of fusel oil
Technical field
The utility model relates to fusel oil separation equipment field, particularly relates to a kind of separator of fusel oil.
Background technology
Fusel oil is cereal crops through the Main By product of preparing ethanol by fermentation and beer, comprises methyl alcohol, ethanol, normal propyl alcohol, isobutanol, isoamyl alcohol etc.Usually rectifier unit is adopted to carry out Separation & Purification to fusel oil by the different boiling of various component at present.After being separated by knockout tower heating after fusel oil flows into raw material tank, utilize condenser that the component of different boiling is completed Separation & Purification.
In the prior art, the knockout tower (i.e. packed tower) of built-in filler is usually adopted to be separated fusel oil.But packed tower opereating specification is less, the change for liquid load is responsive especially.When liquid load is less, filling surface can not soak well, and mass transfer effect sharply declines; When liquid load is excessive, easily produce liquid flooding.Meanwhile, the separative efficiency of packed tower is not high, especially undesirable to the extraction efficiency of ethanol, these light component materials of propyl alcohol.In addition, meanwhile, packed tower should not process the material containing solid suspension; Finally, packed tower cleaning is inconvenient, and complex structure, security is not high.
In view of this, be necessary to be improved the separator for fusel oil Extraction and isolation of the prior art, to solve the problem.
Utility model content
The purpose of this utility model is openly a kind of separator for fusel oil, in order to improve the separating effect to fusel oil, is convenient to cleaning, simplifies structure, and improve security.
For achieving the above object, the utility model provides a kind of separator of fusel oil, comprise: tank body, be arranged at multiple material inlets of tank body sidepiece, be arranged at light fraction outlet and the outlet of multiple heavy constituent of tank body top and bottom, this separator also comprises the multiple column plates being arranged at tank interior, and is arranged at multiple draining plates of tank body madial wall, and column plate partly overlaps along the axial bearing of trend of tank body.
In some embodiments, multiple column plate is set in parallel in tank body.
In some embodiments, draining plate is arranged at the both sides up and down of column plate, and encloses formation arc-shaped gaps with tank body.
In some embodiments, column plate comprises column plate and lower column plate, and upper column plate and lower column plate arrange along the axisymmetrical of tank body and partly overlap.
In some embodiments, upper column plate and lower column plate lap undulate or zigzag.
In some embodiments, draining plate is symmetricly set in the both sides of column plate along the axis at intervals of tank body.
In some embodiments, the end of the downward bearing of trend of draining plate is provided with a bending part.
In some embodiments, tank interior is provided with at least ten five column plates.
In some embodiments, the bottom of tank body is also provided with waste gate.
Compared with prior art, the beneficial effects of the utility model are: by arranging multiple column plate and multiple draining plate in tank body, achieving the effect of the component of different boiling being carried out efficient Separation & Purification, improve the separating effect to fusel oil significantly; Be convenient to cleaning, structure is simple, and security is higher simultaneously.
Accompanying drawing explanation
Fig. 1 is the structural representation of the separator of a kind of fusel oil of the utility model;
The schematic diagram of adjacent two layers column plate when being separated different component in the separator that Fig. 2 is a kind of fusel oil shown in Fig. 1;
Fig. 3 is the sectional view along A-A direction in Fig. 2.
Detailed description of the invention
Below in conjunction with each embodiment shown in the drawings, the utility model is described in detail; but should be noted that; these embodiments are not limitation of the utility model; those of ordinary skill in the art are according to these embodiment institute work energy, method or structural equivalent transformations or substitute, and all belong within protection domain of the present utility model.
Embodiment one:
A kind of detailed description of the invention of the separator of please refer to the drawing 1 and a kind of fusel oil of the utility model shown in Fig. 2.
In the utility model, the separator 100 of this fusel oil comprises tank body 10, and multiple material inlets 20, the light fraction outlet 30 being arranged at tank body 10 sidepiece is arranged at the top of tank body 10, multiple heavy constituent outlets 40 are arranged at the bottom of tank body 10, and are specially the sidepiece near bottom; And the waste gate 70 be arranged at bottom tank body 10, such as, to be discharged the high boiling substance of trace by this waste gate 70, the impurity of class sapropelitic shape.
After fusel oil is heated by heater in this separator 100, some light component such as methyl alcohol, ethanol are vaporized flowing from bottom to top, some heavy constituent such as isopropyl alcohol, butanols, isoamyl alcohol flow from top to bottom, and the heavy constituent outlet 40 set by the middle and lower part of whole separator is assembled and gets rid of, and carries out condensation thus realize utilizing the different boiling of different component to carry out the effect of Separation & Purification to the various components in fusel oil by the condenser (not shown) be connected with the separator 100 of this fusel oil.It should be noted that, in this description, described in each embodiment, light component and heavy constituent are comparatively speaking.Such as, the boiling point of isopropyl alcohol is 82.45 degrees Celsius, and the boiling point of normal propyl alcohol is 97.1 degrees Celsius, and therefore isopropyl alcohol is exactly light component for normal propyl alcohol, and normal propyl alcohol is exactly heavy constituent for isopropyl alcohol.
Therefore, the separator 100 of multiple fusel oil can be coordinated with condenser, form a continuous print purification & isolation device, utilize the different boiling of component in fusel oil to realize the separation of different component.Isoamyl alcohol is higher in the ratio of fusel oil, and economic worth is higher, can realize the high efficiency extraction to isoamyl alcohol by the separator 100 of the fusel oil shown by embodiment each in the utility model, and the isoamyl alcohol high purity more than 99.8% extracted.
In the present embodiment, the centre position of the sidewall of the separator 100 of this fusel oil is provided with two material inlets 20, and the quantity of heavy constituent outlet 40 is set to two.The quantity that material inlet 20 and heavy constituent export 40 can be adjusted to one or three or four or more according to the demand needing to be separated different component in whole fusel oil piece-rate system.
Shown in reference Fig. 2 and Fig. 3, in the present embodiment, the separator 100 of this fusel oil also comprises 15 column plates 50 being arranged at tank body 10 inside and the multiple draining plates 60 being arranged at tank body madial wall, and this column plate 50 partly overlaps along the axial bearing of trend of tank body 10.Concrete, multiple column plate 50 is set in parallel in tank body 10, and draining plate 60 is arranged at the both sides up and down of column plate 50.Concrete, draining plate 60 interval is symmetricly set in the both sides of column plate 50, and encloses with tank body 10 and form arc-shaped gaps 601.The quantity of draining plate 60 can be equal with the quantity of column plate 50, also can be less than the draining plate 60 of column plate 50 by magnitude setting.
Column plate 50 comprises column plate 51 and lower column plate 52, and upper column plate 51 is symmetrical arranged with the axis 110 of lower column plate 52 along tank body 10 and partly overlaps.Concrete, upper column plate 51 comprises plate-like portion 511 and pleated portions 501, and lower column plate 52 comprises plate-like portion 512 and pleated portions 502, and overlapping to realize partly overlapping of upper column plate 51 and lower column plate 52 by pleated portions 501 and pleated portions 502.Plate-like portion 511 is fixedly connected with tank body 10.Further, between upper column plate 51 and lower column plate 52, be provided with certain gap, thus the light-component gas be convenient in fusel oil after heat vaporized by this gap by column plate 50, and make light-component gas continue flow to last layer column plate 50.Concrete, the gap between pleated portions 501 and pleated portions 502 is specially 200-300mm, and more preferably 200mm.In the present embodiment, this pleated portions 501 and pleated portions 502 indention.
Entered into the internal cavity 101 of tank body 10 via material inlet 20 by pump in the fusel oil the produced input head tank of cereal crops after preparing ethanol by fermentation and beer.By vaporization after the heating of heater (not shown).To heat and fusel oil after vaporizing upwards flows along the direction of arrow 521, and upwards flowed by the direction of the gap between pleated portions 501 and pleated portions 502 according to arrow 521, carry out heat exchange with the liquid in each fold groove, the gas after the light component vaporization in liquid is continued to move to lastblock column plate 50; The liquid (i.e. the alcohols material of heavy constituent) be not vaporized is assembled and one block of column plate 50 is carried out said process repeatedly below being dropped onto by the direction of arrow 531 by plate-like portion 512 and draining plate 60 in pleated portions 501, thus realizes the separation and acquisition to different component.Because the column plate 50 in this separator does not need to use filler, therefore use cost is low, and temperature fluctuation interval is little, is easy to control reaction process.
In the present embodiment, the end of the downward bearing of trend of this draining plate 60 is also provided with a bending part 61, and forms the less arc-shaped gaps 611 of a cross-sectional area by this bending part 61 with tank body 10.Arc-shaped gaps 601,611 by being formed between draining plate 60 and tank body 10 between every layer of column plate 50 forms (the i.e. heavy constituent alcohols material) communicating passage that flows downward for liquid.
Embodiment two:
The main distinction of the present embodiment and embodiment one is, axis 110 side that the pleated portions 501 that upper column plate 51 is overlapped with lower column plate 52 and pleated portions 502 are partial to tank body 10 is arranged, and other detailed description of the invention please be joined shown in embodiment one, do not repeat them here.
Embodiment three:
The difference of the present embodiment and first two embodiment is, in the present embodiment, adjacent two column plates 50 are in " splayed ", and other detailed description of the invention please be joined shown in embodiment one, do not repeat them here.
Embodiment four:
The present embodiment and the difference that first three plants embodiment are, in the present embodiment, upper column plate 51 and lower column plate 52 lap undulate, other detailed description of the invention please be joined shown in embodiment one to three, do not repeat them here.
A series of detailed description listed is above only illustrating for feasibility embodiment of the present utility model; they are also not used to limit protection domain of the present utility model, all do not depart from the utility model skill equivalent implementations of doing of spirit or change all should be included within protection domain of the present utility model.
To those skilled in the art, obvious the utility model is not limited to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present utility model or essential characteristic, can realize the utility model in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present utility model is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the utility model.Any Reference numeral in claim should be considered as the claim involved by limiting.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should by description integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.

Claims (9)

1. the separator (100) of a fusel oil, comprise: tank body (10), be arranged at multiple material inlets (20) of tank body sidepiece, be arranged at light fraction outlet (30) and multiple heavy constituent outlet (40) of tank body top and bottom, it is characterized in that, also comprise the multiple column plates (50) being arranged at tank interior, and being arranged at multiple draining plates (60) of tank body madial wall, described column plate (50) partly overlaps along the axial bearing of trend of tank body.
2. separator according to claim 1, is characterized in that, multiple column plate (50) is set in parallel in tank body (10).
3. separator according to claim 1, is characterized in that, described draining plate (60) is arranged at the both sides up and down of column plate (50), and encloses formation arc-shaped gaps with tank body (10).
4. separator according to claim 3, it is characterized in that, described column plate (50) comprises column plate (51) and lower column plate (52), and described upper column plate (51) is symmetrical arranged with the axis (110) of lower column plate (52) along tank body and partly overlaps.
5. separator according to claim 4, is characterized in that, described upper column plate (51) and lower column plate (52) lap undulate or zigzag.
6. separator according to claim 3, is characterized in that, described draining plate (60) is symmetricly set in the both sides of column plate (50) along axis (110) interval of tank body.
7. separator according to claim 6, is characterized in that, the end of the downward bearing of trend of described draining plate (60) is provided with a bending part (61).
8. separator according to claim 1, is characterized in that, described tank body (10) inside is provided with at least ten five column plates (50).
9. separator according to claim 8, is characterized in that, the bottom of described tank body (10) is also provided with waste gate (70).
CN201520285898.1U 2015-05-05 2015-05-05 A kind of separator of fusel oil Expired - Fee Related CN204582595U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520285898.1U CN204582595U (en) 2015-05-05 2015-05-05 A kind of separator of fusel oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520285898.1U CN204582595U (en) 2015-05-05 2015-05-05 A kind of separator of fusel oil

Publications (1)

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CN204582595U true CN204582595U (en) 2015-08-26

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108815874A (en) * 2018-08-30 2018-11-16 安徽顺恒信新材料有限公司 A kind of rectifying still self-flow device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108815874A (en) * 2018-08-30 2018-11-16 安徽顺恒信新材料有限公司 A kind of rectifying still self-flow device

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150826

Termination date: 20180505

CF01 Termination of patent right due to non-payment of annual fee