CN204543581U - A kind of efficient chemical industry evaporating kettle - Google Patents

A kind of efficient chemical industry evaporating kettle Download PDF

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Publication number
CN204543581U
CN204543581U CN201520061749.7U CN201520061749U CN204543581U CN 204543581 U CN204543581 U CN 204543581U CN 201520061749 U CN201520061749 U CN 201520061749U CN 204543581 U CN204543581 U CN 204543581U
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China
Prior art keywords
kettle
sample tap
valve
liquid
probe tube
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Expired - Fee Related
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CN201520061749.7U
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Chinese (zh)
Inventor
翁增琦
刘进军
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Ningbo University
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Ningbo University
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Priority to CN201520061749.7U priority Critical patent/CN204543581U/en
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Publication of CN204543581U publication Critical patent/CN204543581U/en
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Abstract

The utility model discloses a kind of efficient chemical industry evaporating kettle, comprise kettle, described kettle top is provided with charging aperture and steam (vapor) outlet, and autoclave body bottom is provided with discharge nozzle, and discharge nozzle is provided with gravimetry instrument and outlet valve; Liquid circulating apparatus is provided with on the left of described kettle, sampler is provided with on the right side of kettle, liquid circulating apparatus comprises shower nozzle, circulating line and liquid delivery pump, and shower nozzle stretches in kettle by kettle top, and liquid delivery pump is connected with autoclave body bottom and shower nozzle respectively by circulating line; Described sampler comprises probe tube, the first sample tap and the second sample tap, probe tube two ends are communicated with kettle, probe tube is provided with the first sample tap and the second sample tap from top to bottom successively, helical heating pipe is provided with in described kettle, helical heating pipe lower end is connected with motor, the utility model energy homogeneous heating needs the feed liquid of evaporation, can accelerate the heat trnasfer of feed liquid, improves evaporation efficiency; It is convenient to sample, and have multiple sample tap, sampling precision is high, effectively ensures discharging quality.

Description

A kind of efficient chemical industry evaporating kettle
Technical field
The utility model relates to a kind of chemical industry equipment, specifically a kind of efficient chemical industry evaporating kettle.
Background technology
Usually need in Chemical Manufacture to use evaporating kettle, but existing evaporating kettle is realize heating evaporation by arranging tube heater at its outer wall mostly, this heating means can only be heated to the liquid of evaporating kettle periphery of inner wall, cause heating uneven, affect evaporation rate, in evaporating kettle, feed liquid flows little relatively, affect heat-transfer effect, agitating device is set in kettle and can alleviates above problem, but be the increase in manufacturing cost, improve energy consumption, and effectively can not realize the flowing between the upper and lower layer of feed liquid; Evaporating kettle is in sampling process, often the character of upper strata feed liquid and lower floor's feed liquid differs greatly, traditional sampler can only realize the sampling to the feed liquid on a horizontal plane, whether qualified with this sample detection product, deviation is existed to the detection of Total Product quality, effectively can not ensure product quality; Based on above problem, need to carry out design improvement to the evaporating kettle of prior art.
Utility model content
The purpose of this utility model is to provide a kind of energy homogeneous heating to need the feed liquid of evaporation, can accelerate the heat trnasfer of feed liquid, improve evaporation efficiency; It is convenient to sample, and have multiple sample tap, sampling precision is high, effectively ensures the efficient chemical industry evaporating kettle of discharging quality, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the utility model provides following technical scheme:
A kind of efficient chemical industry evaporating kettle, comprise kettle, liquid circulating apparatus and sampler, described kettle top is provided with charging aperture and steam (vapor) outlet, and autoclave body bottom is provided with discharge nozzle, and described discharge nozzle is provided with gravimetry instrument and outlet valve; The left side of described kettle is provided with liquid circulating apparatus, sampler is provided with on the right side of kettle, described liquid circulating apparatus comprises shower nozzle, circulating line and liquid delivery pump, and shower nozzle stretches in kettle by kettle top, and liquid delivery pump is connected with autoclave body bottom and shower nozzle respectively by circulating line; Described sampler comprises probe tube, the first sample tap and the second sample tap, the two ends of probe tube are communicated with kettle, probe tube is provided with the first sample tap and the second sample tap from top to bottom successively, described first sample tap top, between the first sample tap and the second sample tap and on the probe tube of the second sample tap bottom, be respectively equipped with the first valve, the second valve and the 3rd valve, described kettle inside is provided with helical heating pipe, and the lower end of helical heating pipe is stretched out autoclave body bottom and is connected with motor.
As further program of the utility model: described steam (vapor) outlet is connected with liquefaction recycling can by pipeline.
As the utility model further scheme: described pipeline is provided with aspiration pump.
As the utility model further scheme: described gravimetry instrument controls outlet valve and opens and closes.
As the utility model further scheme: described first sample tap place is provided with the 4th valve, and the second sample tap place is provided with the 5th valve.
Compared with prior art, the beneficial effects of the utility model are: the utility model structure is simple, reasonable in design, and by arranging helical heating pipe in kettle, energy homogeneous heating needs the feed liquid of evaporation; Liquid circulating apparatus makes feed liquid realize the flowing of in the vertical direction, accelerates the heat trnasfer of feed liquid, improves evaporation efficiency; Sampler has been provided with multiple sample tap, can realize sampling the feed liquid of liquid level multiple in kettle, and it is convenient to sample, and sampling precision is high, product quality more accurately can be provided to detect, be convenient to the control to evaporation process; The gravimetry instrument that discharge outlet is arranged, can the density of the real time measure discharging feed liquid, and its density range with qualified products contrast, when discharging feed liquid density is not in the density range of qualified products, namely control closes outlet valve, effectively ensure that discharging quality.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
Be described in more detail below in conjunction with the technical scheme of detailed description of the invention to this patent.
Refer to Fig. 1, a kind of efficient chemical industry evaporating kettle, comprise kettle 1, liquid circulating apparatus 2 and sampler 3, described kettle 1 top is provided with charging aperture 4 and steam (vapor) outlet 5, steam (vapor) outlet 5 is connected with liquefaction recycling can 21 by pipeline 20, and pipeline 20 is provided with aspiration pump 22; Be provided with discharge nozzle 6 bottom described kettle 1, discharge nozzle 6 is provided with gravimetry instrument 7 and outlet valve 8, and gravimetry instrument 7 controls outlet valve 8 and opens and closes; The left side of described kettle 1 is provided with liquid circulating apparatus 2, sampler 3 is provided with on the right side of kettle 1, described liquid circulating apparatus 2 comprises shower nozzle 9, circulating line 10 and liquid delivery pump 11, shower nozzle 9 stretches in kettle 1 by kettle 1 top, and liquid delivery pump 11 is connected with shower nozzle 9 respectively with bottom kettle 1 by circulating line 10; Described sampler 3 comprises probe tube 12, first sample tap 13 and the second sample tap 14, the two ends of probe tube 12 are communicated with kettle 1, probe tube 12 is provided with successively the first sample tap 13 and the second sample tap 14 from top to bottom, described first sample tap 13 top, between the first sample tap 13 and the second sample tap 14 and on the probe tube 12 of the second sample tap 14 bottom, be respectively equipped with the first valve 15, second valve 16 and the 3rd valve 17, described first sample tap 13 place is provided with the 4th valve 23, second sample tap 14 place and is provided with the 5th valve 24; Described kettle 1 inside is provided with helical heating pipe 18, and the lower end of helical heating pipe 18 is stretched out bottom kettle 1 and is connected with motor 19.
Operation principle of the present utility model is: need the feed liquid of evaporation to enter in kettle 1 by charging aperture 4, heating evaporation is carried out by helical heating pipe 18, feed liquid is promoted to kettle 1 top by being recycled pipeline 10 bottom kettle 1 under the effect of liquid delivery pump 11, be sprayed in kettle 1 by shower nozzle 9, improve the relative flowing of feed liquid, add heat-transfer effect, shorten evaporation time, when equipment runs, first valve 15 of sampler 3, second valve 16 and the 3rd valve 17 are in folding condition, 4th valve 23 and the 5th valve 24 are in closure state, due to law of connected vessels, feed liquid distribution in probe tube 12 is identical with the feed liquid distribution situation in kettle 1, by locating the sampling of different liquid level to the first sample tap 13 and the second sample tap 14 liang, feed liquid evaporation situation in the clearer understanding kettle 1 of energy, when needs sample the first sample tap 13, only need close the second valve 16, open the 4th valve 23, when needs sample the second sample tap 14, only need close the second valve 16 and the 3rd valve 17, open the 5th valve 24, gravimetry instrument 7 on discharge nozzle 6 can detect the density of discharging feed liquid in real time, and when the density of discharging feed liquid is not in the density range of the qualified feed liquid preset, density tester 7 controls outlet valve 8 and closes, and effectively ensure that the quality of discharging feed liquid.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art possesses, various change can also be made under the prerequisite not departing from this patent aim.

Claims (5)

1. an efficient chemical industry evaporating kettle, comprise kettle (1), liquid circulating apparatus (2) and sampler (3), described kettle (1) top is provided with charging aperture (4) and steam (vapor) outlet (5), kettle (1) bottom is provided with discharge nozzle (6), it is characterized in that: described discharge nozzle (6) is provided with gravimetry instrument (7) and outlet valve (8), the left side of described kettle (1) is provided with liquid circulating apparatus (2), kettle (1) right side is provided with sampler (3), described liquid circulating apparatus (2) comprises shower nozzle (9), circulating line (10) and liquid delivery pump (11), shower nozzle (9) stretches in kettle (1) by kettle (1) top, and liquid delivery pump (11) is connected with kettle (1) bottom and shower nozzle (9) respectively by circulating line (10), described sampler (3) comprises probe tube (12), first sample tap (13) and the second sample tap (14), the two ends of probe tube (12) are communicated with kettle (1), probe tube (12) is provided with successively the first sample tap (13) and the second sample tap (14) from top to bottom, described first sample tap (13) top, the probe tube (12) of between the first sample tap (13) and the second sample tap (14) and the second sample tap (14) bottom is respectively equipped with the first valve (15), second valve (16) and the 3rd valve (17), described kettle (1) inside is provided with helical heating pipe (18), the lower end of helical heating pipe (18) is stretched out kettle (1) bottom and is connected with motor (19).
2. efficient chemical industry evaporating kettle according to claim 1, is characterized in that, described steam (vapor) outlet (5) is connected with liquefaction recycling can (21) by pipeline (20).
3. efficient chemical industry evaporating kettle according to claim 2, is characterized in that, described pipeline (20) is provided with aspiration pump (22).
4. efficient chemical industry evaporating kettle according to claim 1, is characterized in that, described gravimetry instrument (7) controls outlet valve (8) and opens and closes.
5. efficient chemical industry evaporating kettle according to claim 1, is characterized in that, described first sample tap (13) place is provided with the 4th valve (23), and the second sample tap (14) place is provided with the 5th valve (24).
CN201520061749.7U 2015-01-23 2015-01-23 A kind of efficient chemical industry evaporating kettle Expired - Fee Related CN204543581U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520061749.7U CN204543581U (en) 2015-01-23 2015-01-23 A kind of efficient chemical industry evaporating kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520061749.7U CN204543581U (en) 2015-01-23 2015-01-23 A kind of efficient chemical industry evaporating kettle

Publications (1)

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CN204543581U true CN204543581U (en) 2015-08-12

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106512452A (en) * 2016-12-15 2017-03-22 宁波宝硕美机械设备工程有限公司 Ejection and flash evaporation circulated concentration device
CN106943757A (en) * 2017-03-30 2017-07-14 上海东富龙科技股份有限公司 A kind of continous way medicinal extract enrichment machine and its work, cleaning method
CN109580284A (en) * 2018-12-25 2019-04-05 三友(天津)高分子技术有限公司 A kind of sample tap for reaction kettle pipeline

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106512452A (en) * 2016-12-15 2017-03-22 宁波宝硕美机械设备工程有限公司 Ejection and flash evaporation circulated concentration device
CN106943757A (en) * 2017-03-30 2017-07-14 上海东富龙科技股份有限公司 A kind of continous way medicinal extract enrichment machine and its work, cleaning method
CN109580284A (en) * 2018-12-25 2019-04-05 三友(天津)高分子技术有限公司 A kind of sample tap for reaction kettle pipeline

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150812

Termination date: 20180123