CN204522442U - Extraction by steam distillation nicotine residue equipment for separating liquid from solid - Google Patents
Extraction by steam distillation nicotine residue equipment for separating liquid from solid Download PDFInfo
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- CN204522442U CN204522442U CN201520214128.8U CN201520214128U CN204522442U CN 204522442 U CN204522442 U CN 204522442U CN 201520214128 U CN201520214128 U CN 201520214128U CN 204522442 U CN204522442 U CN 204522442U
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- filter cylinder
- pillar buoy
- conical filter
- solid
- steam distillation
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Abstract
The utility model provides a kind of extraction by steam distillation nicotine residue equipment for separating liquid from solid, comprise the pillar buoy be communicated with alembic slag-drip opening, pillar buoy one end is sealed by import gland retainer plate, there is in pillar buoy the rotating shaft arranged vertically, the two ends of rotating shaft are all stretched out pillar buoy and are arranged, the one end of wherein stretching out import gland retainer plate is connected with belt pulley, the other end of described rotating shaft is arranged with the conical filter cylinder connected with pillar buoy and the dregs discharge tube be connected with conical filter cylinder, conical filter cylinder and pillar buoy junction, inner and the conical filter cylinder of conical filter cylinder and dregs discharge tube junction are equipped with the resistance rotating disk of loop configuration, each resistance rotating disk inner ring is equipped with teeth radially, which solves conventional worm feed to the high material of moisture content almost without the problem of compressed capability, and can stop and escape from this discharging opening containing nicotine steam, not only can a large amount of alkali lye in recycle-water steam distillation residue, save resource, turn avoid environmental pollution.
Description
Technical field
The utility model relates to alkaloid extraction equipment technical field, is specifically related to a kind of extraction by steam distillation nicotine residue equipment for separating liquid from solid.
Background technology
Containing very valuable nicotine and Salanesol in Discarded Tobacco.Extraction nicotine and Salanesol, have organic solvent extraction-reverse-extraction method, CO 2 supercritical extraction method and carbonization decarboxylation (destructive distillation) method.Organic solvent extraction-reverse-extraction method not only will consume a large amount of organic solvents, and contaminated environment; Not only equipment needed thereby is expensive but also to mention cost too high for CO 2 supercritical extraction method; Carbonization decarboxylation (destructive distillation) method, because temperature is higher, has part Salanesol to be transformed to enantiomer, causes its biologically active to reduce.Under alkali condition, with steam distillation effective component extracting nicotine from tobacco waste, can effectively other compositions in nicotine and tobacco be separated, and in residue, the biologically active of Salanesol also can remain unchanged.But traditional steam distillation, on the one hand, needs steam evaporator and acid to absorb two devices; On the other hand, a large amount of steam condenses into water in sour absorption plant, not only wastes mass energy, and has rushed sour absorbent solution rare, and cause its aftertreatment technology also must arrange concentrator, economic benefit is not good.Just because of this reason, traditional extraction by steam distillation nicotine is general only for the lab analysis of tobacco sample nicotine content.Applicant is in its " steam extracted for nicotine occurs and sour absorption plant " of declaring, solve the steam that nicotine extracts to occur and sour absorption problem, while steam distillation tank also in steam distillation equipment in the urgent need to address and steam distillation after form the Separation of Solid and Liquid of residue, the problem of discharge.
Utility model content
The purpose of this utility model is to provide a kind of extraction by steam distillation nicotine residue equipment for separating liquid from solid, which solves conventional worm feed to the high material of moisture content almost without the problem of compressed capability, and can stop and escape from this discharging opening containing nicotine steam, not only can a large amount of alkali lye in recycle-water steam distillation residue, save resource, turn avoid environmental pollution.
The technical scheme that the utility model adopts is: extraction by steam distillation nicotine residue equipment for separating liquid from solid, comprise the pillar buoy be communicated with alembic slag-drip opening, pillar buoy one end is sealed by import gland retainer plate, there is in pillar buoy the rotating shaft arranged vertically, the two ends of rotating shaft are all stretched out pillar buoy and are arranged, the one end of wherein stretching out import gland retainer plate is connected with belt pulley, the other end of described rotating shaft is arranged with the conical filter cylinder connected with pillar buoy and the dregs discharge tube be connected with conical filter cylinder, conical filter cylinder and pillar buoy junction, inner and the conical filter cylinder of conical filter cylinder and dregs discharge tube junction are equipped with the resistance rotating disk of loop configuration, each resistance rotating disk inner ring is equipped with teeth radially, rotating shaft in described pillar buoy, between adjacent two resistance rotating disks and in dregs discharge tube is all arranged with worm gear axle sleeve, be mutually permanently connected between adjacent worm gear axle sleeve, and the worm-wheel shaft between adjacent two resistance rotating disks and in pillar buoy puts and is all fixed with helical blade,
Be provided with multiple ring segment for filtering in described conical filter cylinder, ring segment periphery is evenly distributed with fixing feet, and fixing feet is provided with screw, and adjacent ring segment is fastened by bolt clip, and each screw place between adjacent ring segment is equipped with pad; Form between the bottom of ring segment and conical filter cylinder and connect liquid bath, connect liquid bath and be provided with fluid hole; The afterbody of described dregs discharge tube is provided with outlet gland retainer plate, and the bottom of dregs discharge tube is provided with solid discharge, and the worm-wheel shaft in dregs discharge tube puts and is provided with material toggling tooth.
Described conical filter cylinder and the axial direction of pillar buoy are 6 ° of angles.
Two teeth are provided with inside described resistance rotating disk.
All be fixedly connected with bayonet socket by the card convex matched between described adjacent worm gear axle sleeve.
Described ring segment periphery is evenly distributed with three fixing feet.
Described resistance rotating disk is fixed, all with screw on each leg by the equally distributed leg in periphery.
Described pad is the circular ring plate matched with screw aperture in aperture.
The beneficial effects of the utility model
Compared with prior art, the utility model at least has following advantage and beneficial effect:
1, the utility model solves conventional worm feed to the high material of moisture content almost without the problem of compressed capability, and is connected with the discharging opening of steam distillation tank, prevents and escapes from this discharging opening containing nicotine steam.Not only can a large amount of alkali lye in recycle-water steam distillation residue, save resource, turn avoid environmental pollution.
2, the isolated solid residue of the utility model is very beneficial for continuing to extract another high value added product Salanesol, if not, only namely isolated solid residue stack retting, fermentation can need be eliminated alkalescence, become high-quality organic fertilizer.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model;
Fig. 2 is the structural representation hindering rotating disk in the utility model;
Fig. 3 is the structural representation of ring segment in the utility model;
Fig. 4 is the structural representation of the utility model Intermediate gasket;
Reference numeral: 1, alembic slag-drip opening, 2, pillar buoy, 3, import gland retainer plate, 4, rotating shaft, 5, belt pulley, 6, conical filter cylinder, 7, dregs discharge tube, 8, rotating disk is hindered, 801, teeth, 9, worm gear axle sleeve, 10, helical blade, 11, ring segment, 1101, fixing feet, 12, pad, 13, connect liquid bath, 14, fluid hole, 15, material toggling tooth, 16, outlet gland retainer plate, 17, solid discharge.
Detailed description of the invention
For making content of the present utility model become apparent, below in conjunction with specific embodiment, the utility model is described in detail.
As shown in the figure, extraction by steam distillation nicotine residue equipment for separating liquid from solid, comprise the pillar buoy 2 be communicated with alembic slag-drip opening 1, pillar buoy 2 one end is sealed by import gland retainer plate 3, there is in pillar buoy 2 rotating shaft 4 arranged vertically, the two ends of rotating shaft 4 are all stretched out pillar buoy 2 and are arranged, the one end of wherein stretching out import gland retainer plate 3 is connected with belt pulley 5, the other end of described rotating shaft 4 is arranged with the conical filter cylinder 6 connected with pillar buoy 2 and the dregs discharge tube 7 be connected with conical filter cylinder 6, conical filter cylinder 6 and pillar buoy 2 junction, conical filter cylinder 6 inside and conical filter cylinder 6 are equipped with the resistance rotating disk 8 of loop configuration with dregs discharge tube 7 junction, each resistance rotating disk 8 inner ring is equipped with teeth 801 radially, rotating shaft 4 in described pillar buoy 2, between adjacent two resistance rotating disks 8 and in dregs discharge tube 7 is all arranged with worm gear axle sleeve 9, be mutually permanently connected between adjacent worm gear axle sleeve 9, and worm gear axle sleeve 9 between adjacent two resistance rotating disks 8 and in pillar buoy 2 is all fixed with helical blade 10, multiple ring segment 11 for filtering is provided with in described conical filter cylinder 6, ring segment 11 periphery is evenly distributed with fixing feet 1101, fixing feet 1101 is provided with screw, and adjacent ring segment 11 is fastened by bolt clip, and each screw place between adjacent ring segment 11 is equipped with pad 12, form between the bottom of ring segment 11 and conical filter cylinder 6 and connect liquid bath 13, connect liquid bath 13 and be provided with fluid hole 14, the afterbody of described dregs discharge tube 7 is provided with outlet gland retainer plate 16, and the bottom of dregs discharge tube 7 is provided with solid discharge 17, and the worm gear axle sleeve 9 in dregs discharge tube 7 is provided with material toggling tooth 15.
In order to make the utility model, there is better result of use, described conical filter cylinder 6 is 6 ° of angles with the axial direction of pillar buoy 2, two resistance rotating disks 8 are provided with in conical filter cylinder 6, the utility model arranges 4 resistance rotating disks 8 altogether, two teeth 801 are provided with inside described resistance rotating disk 8, two teeth 801 are oppositely arranged, and be upper and lower relation, resistance rotating disk 8 is fixed by the equally distributed leg in periphery, all with screw on each leg, together with resistance rotating disk 8, pad 12 are bolted with the screw on ring segment 11, and fix with the flange of conical filter cylinder 6.Such setting, first hinders rotating disk 8 and prevents solid-liquid material to rotate with rotating vane, can only advance, add that conical filter cylinder 6 has certain tapering, solid-liquid material is compressed, then liquid is filtered off by the gap between ring segment, flows into and connects liquid bath 13, and discharge from fluid hole 14, reclaim alkali lye, solid residue then moves on and arrives dregs discharge tube 7, along with solid material gathers in dregs discharge tube 7, under the effect of material toggling tooth 15, solid material slag is discharged from solid discharge 17.
In the technical solution of the utility model, be all fixedly connected with bayonet socket by the card convex matched between adjacent worm gear axle sleeve 9, the gap between the tooth head place distance worm gear axle sleeve 9 of the teeth 801 of resistance rotating disk 8 is 10mm.Described ring segment 11 periphery is evenly distributed with three fixing feet 1101, and the thickness of ring segment 11 is 4mm.Described pad 12 is the circular ring plate matched with screw aperture in aperture, and the diameter of pad 12 is 36mm, and thickness is 0.5mm.
Using method of the present utility model:
The rotating speed first arranging rotating shaft 4 of the present utility model is 112% of feeder rotating shaft rotating speed, motor of the present utility model was started before solid-liquid material discharged by steam distillation tank, after solid-liquid material enters pillar buoy 2, under helical blade 10 advances, solid-liquid material enters conical filter cylinder 6, because resistance rotating disk 8 prevents solid-liquid material to rotate with helical blade 10, can only advance, add that conical filter cylinder 6 is with tapering, solid-liquid material is compressed, then liquid is filtered off by the gap between ring segment 11, inflow connects liquid bath 13, and discharge recovery alkali lye from its fluid hole 14, solid residue then moves on and arrives in dregs discharge tube 7, because solid material is at the sidewall of dregs discharge tube 7, and outlet is less, solid material must produce gathering to a certain degree in dregs discharge tube 7, thus stop gas to pass through, along with the gathereding degree of solid material increases, under the effect of material toggling tooth 15, final solid material is discharged the utility model.
If do not pass into steam in steam distillation tank, can directly the alkali lye that the first step reclaims be turned back in the lye tank (vat) of feed arrangement, solid residue directly turns back in charging hopper, and turns down the rotating speed of lye pump;
If pass into steam in steam distillation tank, and the nicotine content of solid residue < 0.1% after testing, can by solid residue, stack retting, fermentation make organic fertilizer, or are used as the raw material extracting Salanesol, isolated alkali lye is according to analysis result, supplemental hydrogen sodium oxide molybdena, becomes this technique alkali lye used, repeatedly reclaims several times, after its viscosity increase loses this technique recovery value, can used as one of raw material of foam concrete foaming agent.
If more than one day stops using this device, first start the utility model and discharge solid residue, then clean it with running water.
Technical scheme cited by the utility model and embodiment be not restriction, be equal to the technical scheme cited by the utility model and embodiment or effect same approach all in the scope that the utility model is protected.
Claims (7)
1. extraction by steam distillation nicotine residue equipment for separating liquid from solid, comprise the pillar buoy (2) be communicated with alembic slag-drip opening (1), pillar buoy (2) one end is by import gland retainer plate (3) sealing, there is in pillar buoy (2) rotating shaft (4) arranged vertically, the two ends of rotating shaft (4) are all stretched out pillar buoy (2) and are arranged, the one end of wherein stretching out import gland retainer plate (3) is connected with belt pulley (5), it is characterized in that: the other end of described rotating shaft (4) is arranged with the conical filter cylinder (6) connected with pillar buoy (2) and the dregs discharge tube (7) be connected with conical filter cylinder (6), conical filter cylinder (6) and pillar buoy (2) junction, conical filter cylinder (6) inside and conical filter cylinder (6) are equipped with the resistance rotating disk (8) of loop configuration with dregs discharge tube (7) junction, each resistance rotating disk (8) inner ring is equipped with teeth (801) radially, rotating shaft (4) in described pillar buoy (2), between adjacent two resistance rotating disks (8) and in dregs discharge tube (7) is all arranged with worm gear axle sleeve (9), be mutually permanently connected between adjacent worm gear axle sleeve (9), and worm gear axle sleeve (9) between adjacent two resistance rotating disks (8) and in pillar buoy (2) is all fixed with helical blade (10),
Multiple ring segment (11) for filtering is provided with in described conical filter cylinder (6), ring segment (11) periphery is evenly distributed with fixing feet (1101), fixing feet (1101) is provided with screw, adjacent ring segment (11) is fastened by bolt clip, and each screw place between adjacent ring segment (11) is equipped with pad (12); Form between the bottom of ring segment (11) and conical filter cylinder (6) and connect liquid bath (13), connect liquid bath (13) and be provided with fluid hole (14); The afterbody of described dregs discharge tube (7) is provided with outlet gland retainer plate (16), and the bottom of dregs discharge tube (7) is provided with solid discharge (17), and the worm gear axle sleeve (9) in dregs discharge tube (7) is provided with material toggling tooth (15).
2. extraction by steam distillation nicotine residue equipment for separating liquid from solid as claimed in claim 1, is characterized in that: described conical filter cylinder (6) is 6 ° of angles with the axial direction of pillar buoy (2).
3. extraction by steam distillation nicotine residue equipment for separating liquid from solid as claimed in claim 1, is characterized in that: described resistance rotating disk (8) inner side is provided with two teeth (801).
4. extraction by steam distillation nicotine residue equipment for separating liquid from solid as claimed in claim 1, be is characterized in that: be all fixedly connected with bayonet socket by the card convex matched between described adjacent worm gear axle sleeve (9).
5. extraction by steam distillation nicotine residue equipment for separating liquid from solid as claimed in claim 1, is characterized in that: described ring segment (11) periphery is evenly distributed with three fixing feet (1101).
6. extraction by steam distillation nicotine residue equipment for separating liquid from solid as claimed in claim 1, is characterized in that: described resistance rotating disk (8) is fixed, all with screw on each leg by the equally distributed leg in periphery.
7. extraction by steam distillation nicotine residue equipment for separating liquid from solid as claimed in claim 1, is characterized in that: the circular ring plate that described pad (12) matches with screw aperture for aperture.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520214128.8U CN204522442U (en) | 2015-04-10 | 2015-04-10 | Extraction by steam distillation nicotine residue equipment for separating liquid from solid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520214128.8U CN204522442U (en) | 2015-04-10 | 2015-04-10 | Extraction by steam distillation nicotine residue equipment for separating liquid from solid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204522442U true CN204522442U (en) | 2015-08-05 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520214128.8U Expired - Fee Related CN204522442U (en) | 2015-04-10 | 2015-04-10 | Extraction by steam distillation nicotine residue equipment for separating liquid from solid |
Country Status (1)
| Country | Link |
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| CN (1) | CN204522442U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108514395A (en) * | 2018-04-04 | 2018-09-11 | 广东美的厨房电器制造有限公司 | Dish-washing machine and its filtration system |
-
2015
- 2015-04-10 CN CN201520214128.8U patent/CN204522442U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108514395A (en) * | 2018-04-04 | 2018-09-11 | 广东美的厨房电器制造有限公司 | Dish-washing machine and its filtration system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150805 Termination date: 20200410 |