CN204522379U - Change a kind ofly and use chromatographic column - Google Patents

Change a kind ofly and use chromatographic column Download PDF

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Publication number
CN204522379U
CN204522379U CN201520199052.6U CN201520199052U CN204522379U CN 204522379 U CN204522379 U CN 204522379U CN 201520199052 U CN201520199052 U CN 201520199052U CN 204522379 U CN204522379 U CN 204522379U
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cylinder
chromatographic column
arc
kind ofly
liquid
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CN201520199052.6U
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Chinese (zh)
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徐硕
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Northeast Petroleum University
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Northeast Petroleum University
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Abstract

The utility model belongs to technical field of chemical, change with chromatographic column a kind ofly, comprise cylinder, gear handle and piston, the top of cylinder is provided with liquid homogenizer, liquid homogenizer comprises edge, conical hopper, back taper funnel and even liquid disc, even liquid disc is provided with equally distributed point of fluid apertures, and the external diameter on upper edge is greater than the external diameter of cylinder, and conical hopper, back taper funnel and even liquid disc are positioned at the inside of cylinder; The outside of cylinder is provided with label box from top to bottom successively, gear handle, antiskid glue sleeve, symmetrical two arc lighting devices, temperature take into account hygrometer, arc lighting device comprises the arc transparent body, LED, button cell box and switch, and LED and button cell box (51) are positioned at the inside of the arc transparent body.Structure of the present utility model is simple, reasonable in design, safe and reliable, easy to use, with low cost, is easy to promote on a large scale and use.

Description

一种地化用层析柱A geochemical chromatography column

技术领域:Technical field:

本实用新型属于化工设备技术领域,具体涉及一种地化用层析柱。 The utility model belongs to the technical field of chemical equipment, in particular to a chromatographic column for geochemistry.

背景技术:Background technique:

柱层析法是生物、化学实验室中最为常用的分离提纯方法,在整个分离提纯的过程中,除了吸附剂、溶剂、溶质等因素外,层析柱本身的结构也影响着分离提纯效率。目前,在有机化学合成实验室中,一般是常压或者加压使用的层析柱,这些层析柱在使用的过程中,都存在着许多不足之处,尤其在进液环节,无法保证进液的均匀分布,极大影响纯化效率,而且缺乏必要的照明装置,也不具有记录提纯过程中温度和湿度的功能,为日后数据的统计和整理带来不便,另外在移动层析柱的工程中容易脱落,造成层析柱的损坏,影响化验周期好化验结果。  Column chromatography is the most commonly used separation and purification method in biological and chemical laboratories. During the entire separation and purification process, in addition to factors such as adsorbents, solvents, and solutes, the structure of the chromatography column itself also affects the separation and purification efficiency. At present, in organic chemical synthesis laboratories, chromatography columns are generally used under normal pressure or under pressure. These chromatography columns have many shortcomings in the process of use, especially in the liquid inlet link, which cannot guarantee The uniform distribution of the liquid greatly affects the purification efficiency, and it lacks the necessary lighting device, and does not have the function of recording the temperature and humidity during the purification process, which will bring inconvenience to the statistics and arrangement of data in the future. In addition, in the project of moving the chromatography column It is easy to fall off in the medium, causing damage to the chromatographic column, affecting the test cycle and good test results. the

实用新型内容:Utility model content:

本实用新型弥补和改善了上述现有技术的不足之处,提供了一种结构简单、设计合理、使用方便、安全可靠、成本低廉的地化用层析柱,可以大规模地推广和使用。 The utility model makes up for and improves the deficiencies of the above-mentioned prior art, and provides a geochemical chromatographic column with simple structure, reasonable design, convenient use, safety, reliability and low cost, which can be popularized and used on a large scale.

本实用新型采用的技术方案为:一种地化用层析柱,包括柱体、挡柄及活塞,柱体的顶部设有均液器,均液器包括上沿、锥形漏斗、倒锥形漏斗及均液盘,均液盘上设有均匀分布的分液孔,上沿的外径大于柱体的外径,锥形漏斗、倒锥形漏斗及均液盘位于柱体的内部;柱体的外部从上到下依次设有标签盒、挡柄、防滑胶套、对称分布的两个弧形照明装置、温度计及湿度计,弧形照明装置包括弧形透明体、LED灯、纽扣电池盒及开关,LED灯及纽扣电池盒(51)位于弧形透明体的内部。 The technical solution adopted in the utility model is: a chromatography column for geochemical use, including a column body, a retaining handle and a piston, and a liquid homogenizer is provided on the top of the column body, and the liquid homogenizer includes an upper edge, a tapered funnel, an inverted cone A shaped funnel and a liquid equalizing plate, the liquid equalizing plate is provided with evenly distributed liquid separation holes, the outer diameter of the upper edge is larger than the outer diameter of the cylinder, the conical funnel, the inverted conical funnel and the liquid equalizing plate are located inside the cylinder; From top to bottom, the exterior of the cylinder is provided with a label box, a retaining handle, an anti-slip rubber sleeve, two symmetrically distributed arc lighting devices, a thermometer and a hygrometer. The arc lighting device includes an arc transparent body, LED lights, and buttons Battery box and switch, LED light and button battery box (51) are positioned at the inside of curved transparent body.

所述的均液器是一个整体结构,且能够方便地从柱体内取出。 The liquid homogenizer is an integral structure and can be easily taken out from the cylinder.

所述的柱体由玻璃材质制成。 The cylinder is made of glass material.

所述的弧形透明体的材质为透明塑料或玻璃。 The material of the curved transparent body is transparent plastic or glass.

所述的标签盒的材质为透明材料或玻璃。 The material of the label box is transparent material or glass.

所述的弧形照明装置使用纽扣电池供电。 The arc lighting device is powered by a button battery.

本实用新型的有益效果:结构简单,设计合理,安全可靠,使用方便,成本低廉,易于大规模地推广和使用。在使用过程中,液体通过均液器倒入柱体内,锥形漏斗的设计避免了液体喷溅到手上而给操作者带来伤害,液体经过均液盘后,被均匀地分配到柱体内,提高了提纯的效率及质量;所述的温度计和湿度计能够准确地记录提纯过程中温度及湿度的数据,为分析和研究提纯过程提供了有效的数据支持;所述的弧形照明装置方便操作者在夜间观察提纯的情况,也有利于温度和湿度的准确记录;所述的标签盒可以放置提纯物质的相关参数说明,可与更加方便操作者工作,提高工作效率;所述的防滑胶套及挡柄能够避免操作者在移动层析柱时发生滑落,减少损失,降低成本。 The utility model has the beneficial effects of simple structure, reasonable design, safety and reliability, convenient use, low cost, and easy popularization and use on a large scale. During use, the liquid is poured into the column through the homogenizer. The design of the conical funnel prevents the operator from being hurt by splashing the liquid on the hand. The liquid is evenly distributed into the column after passing through the homogenizer. The efficiency and quality of purification are improved; the thermometer and hygrometer can accurately record the data of temperature and humidity in the purification process, which provides effective data support for analysis and research of the purification process; the arc lighting device is convenient to operate It is also beneficial for the operator to observe the purification situation at night, which is also conducive to the accurate recording of temperature and humidity; the described label box can place the relevant parameter descriptions of the purified substance, which can be more convenient for the operator to work and improve work efficiency; the described non-slip rubber sleeve And the stop handle can prevent the operator from slipping when moving the chromatographic column, reducing losses and costs.

附图说明:Description of drawings:

图1是本实用新型的结构示意图。 Fig. 1 is the structural representation of the utility model.

图2是本实用新型的后视图。 Fig. 2 is the rear view of the utility model.

图3是本实用新型中均液器的结构示意图。 Fig. 3 is a schematic structural view of the liquid homogenizer in the utility model.

图4是图3的俯视图。 FIG. 4 is a top view of FIG. 3 .

图5是本实用新型中标签盒的结构示意图。 Fig. 5 is a structural schematic diagram of the label box in the present invention.

图6是本实用新型中弧形照明装置的结构示意图。 Fig. 6 is a structural schematic diagram of an arc-shaped lighting device in the present invention.

图7是图6的俯视图。 FIG. 7 is a top view of FIG. 6 .

具体实施方式:Detailed ways:

参照各图,一种地化用层析柱,包括柱体7、挡柄3及活塞8,柱体7的顶部设有均液器1,均液器1包括上沿11、锥形漏斗12、倒锥形漏斗13及均液盘14,均液盘14上设有均匀分布的分液孔15,上沿11的外径大于柱体7的外径,锥形漏斗12、倒锥形漏斗13及均液盘14位于柱体7的内部;柱体7的外部从上到下依次设有标签盒2、挡柄3、防滑胶套4、对称分布的两个弧形照明装置5、温度计6及湿度计9,弧形照明装置5包括弧形透明体52、LED灯53、纽扣电池盒51及开关54,LED灯53及纽扣电池盒51位于弧形透明体52的内部;所述的均液器1是一个整体结构,且能够方便地从柱体7内取出;所述的柱体7由玻璃材质制成;所述的弧形透明体52的材质为透明塑料或玻璃;所述的标签盒2的材质为透明材料或玻璃;所述的弧形照明装置5使用纽扣电池供电。。在使用过程中,液体通过均液器1倒入柱体7内,锥形漏斗12的设计避免了液体喷溅到手上而给操作者带来伤害,液体经过均液盘14后,被均匀地分配到柱体7内,提高了提纯的效率及质量;所述的温度计6和湿度计9能够准确地记录提纯过程中温度及湿度的数据,为分析和研究提纯过程提供了有效的数据支持;所述的弧形照明装置5方便操作者在夜间观察提纯的情况,也有利于温度和湿度的准确记录;所述的标签盒2可以放置提纯物质的相关参数说明,可与更加方便操作者工作,提高工作效率;所述的防滑胶套4及挡柄3能够避免操作者在移动层析柱时发生滑落,减少损失,降低成本。本实用新型的结构简单,设计合理,安全可靠,使用方便,成本低廉,易于大规模地推广和使用。 With reference to each figure, a geochemical chromatography column includes a column body 7, a retaining handle 3 and a piston 8. The top of the column body 7 is provided with a homogenizer 1, and the homogenizer 1 includes an upper edge 11 and a conical funnel 12. 1. Inverted conical funnel 13 and equal liquid pan 14, evenly distributed liquid separation holes 15 are provided on the even liquid pan 14, the outer diameter of upper edge 11 is greater than the outer diameter of cylinder 7, conical funnel 12, inverted conical funnel 13 and the liquid equalizing plate 14 are located inside the cylinder 7; the outside of the cylinder 7 is provided with a label box 2, a retaining handle 3, a non-slip rubber sleeve 4, two symmetrically distributed arc lighting devices 5, and a thermometer from top to bottom. 6 and hygrometer 9, arc lighting device 5 comprises arc transparent body 52, LED lamp 53, button battery box 51 and switch 54, and LED lamp 53 and button battery box 51 are positioned at the inside of arc shaped transparent body 52; Described The homogenizer 1 is an integral structure, and can be easily taken out from the cylinder 7; the cylinder 7 is made of glass material; the curved transparent body 52 is made of transparent plastic or glass; The label box 2 is made of transparent material or glass; the arc lighting device 5 is powered by a button battery. . During use, the liquid is poured into the cylinder 7 through the homogenizer 1. The design of the conical funnel 12 prevents the liquid from splashing on the hands and causing harm to the operator. After the liquid passes through the homogenizer 14, it is evenly Distributed in the column body 7, the efficiency and quality of the purification are improved; the thermometer 6 and the hygrometer 9 can accurately record the data of temperature and humidity in the purification process, and provide effective data support for the analysis and research of the purification process; The arc-shaped lighting device 5 is convenient for the operator to observe the purification situation at night, and is also conducive to the accurate recording of temperature and humidity; the label box 2 can be placed to explain the relevant parameters of the purified substance, which can be more convenient for the operator to work with , improve work efficiency; the anti-slip rubber sleeve 4 and the retaining handle 3 can prevent the operator from slipping when moving the chromatography column, reduce losses and reduce costs. The utility model has the advantages of simple structure, reasonable design, safety and reliability, convenient use, low cost and easy large-scale popularization and use.

Claims (6)

1. a groundization chromatographic column, comprise cylinder (7), gear handle (3) and piston (8), it is characterized in that: the top of cylinder (7) is provided with liquid homogenizer (1), liquid homogenizer (1) comprises edge (11), conical hopper (12), back taper funnel (13) and even liquid disc (14), even liquid disc (14) is provided with equally distributed point of fluid apertures (15), the external diameter on upper edge (11) is greater than the external diameter of cylinder (7), and conical hopper (12), back taper funnel (13) and even liquid disc (14) are positioned at the inside of cylinder (7); The outside of cylinder (7) is provided with label box (2), gear handle (3), antiskid glue sleeve (4), symmetrical two arc lighting devices (5), thermometer (6) and hygrometers (9) from top to bottom successively, arc lighting device (5) comprises the arc transparent body (52), LED (53), button cell box (51) and switch (54), and LED (53) and button cell box (51) are positioned at the inside of the arc transparent body (52).
2. according to claim 1 change uses chromatographic column a kind ofly, it is characterized in that: described liquid homogenizer (1) is an overall structure, and can take out in cylinder (7) easily.
3. according to claim 1 change uses chromatographic column a kind ofly, it is characterized in that: described cylinder (7) is made up of glass material.
4. according to claim 1 change uses chromatographic column a kind ofly, it is characterized in that: the material of the described arc transparent body (52) is transparent plastic or glass.
5. according to claim 1 change uses chromatographic column a kind ofly, it is characterized in that: the material of described label box (2) is transparent material or glass.
6. according to claim 1 change uses chromatographic column a kind ofly, it is characterized in that: described arc lighting device (5) uses button cell to power.
CN201520199052.6U 2015-04-03 2015-04-03 Change a kind ofly and use chromatographic column Expired - Fee Related CN204522379U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108245933A (en) * 2016-12-29 2018-07-06 天津领世生物科技开发有限公司 Portable normal pressure chromatographic column sampling device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108245933A (en) * 2016-12-29 2018-07-06 天津领世生物科技开发有限公司 Portable normal pressure chromatographic column sampling device

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Granted publication date: 20150805

Termination date: 20160403