CN204485845U - Multi-point temp sensing high-temperature reactor - Google Patents

Multi-point temp sensing high-temperature reactor Download PDF

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Publication number
CN204485845U
CN204485845U CN201520006454.XU CN201520006454U CN204485845U CN 204485845 U CN204485845 U CN 204485845U CN 201520006454 U CN201520006454 U CN 201520006454U CN 204485845 U CN204485845 U CN 204485845U
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CN
China
Prior art keywords
reaction vessel
heating module
electrical heating
temperature sensor
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201520006454.XU
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Chinese (zh)
Inventor
张殿辉
张泽多
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing Crack Ze Xiang Laboratory Apparatus Co Ltd
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Beijing Crack Ze Xiang Laboratory Apparatus Co Ltd
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Filing date
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Priority to CN201520006454.XU priority Critical patent/CN204485845U/en
Application granted granted Critical
Publication of CN204485845U publication Critical patent/CN204485845U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses multi-point temp sensing high-temperature reactor, described Pressure gauge is connected to the top of reaction vessel by pipeline, described safety valve is arranged on manometric lower end, in described container, temperature sensor is connected to the top of reaction vessel, described heating module resistance wire is fixed on the both sides in electrical heating module, described magnetic stir bar is fixed on the bottom of reaction vessel, described pair of magnet is connected with motor, and be installed in the inside of electronic box, described LCDs is arranged on the shell of electronic box, center in described electrical heating module is placed with reaction vessel, the inwall of electrical heating module and the outer wall of reaction vessel fit tightly.The utility model increases temperature sensor in electrical heating module bottom, detection heating module real time temperature, controller software receives the temperature signal in heating part and reactor, the heating rate controlling heating part is eliminated temperature error, make heating-up temperature reach consistent with the temperature in reactor, realize temperature equalization.

Description

Multi-point temp sensing high-temperature reactor
Technical field
The utility model relates to high-temperature reactor field, especially multi-point temp sensing high-temperature reactor.
Background technology
High-temperature reactor oil is widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food chemistry, and a lot of industry such as pharmacy needs the laboratory apparatus used.In existing like product, temperature mainly conducts heat to reaction vessel, in conductive process by electrical heating module, temperature error is comparatively large, and heating-up temperature and serviceability temperature error are at about 10 degree, and reaction temperature fluctuation is larger, have lost a large amount of heat energy, cause reaction vessel temperature uncontrollable.Existing reactor just has a sensor in reaction vessel, can only show solution temperature, cannot show the temperature of electrical heating module.
Utility model content
For the problems referred to above, the utility model aims to provide a kind of multi-point temp sensing high-temperature reactor realizing temperature equalization.
For realizing this technical purpose, scheme of the present utility model is:
Multi-point temp sensing high-temperature reactor, comprises Pressure gauge, safety valve, temperature sensor in container, air bleeding valve, control button, reaction vessel clamp nut, trip bolt, reaction vessel, reaction vessel supports, heating module resistance wire, magnetic stir bar, temperature sensor, two magnet, LCDs, motor, electronic box and electrical heating module, described Pressure gauge is connected to the top of reaction vessel by pipeline, described safety valve is arranged on manometric lower end, in described container, temperature sensor is connected to the top of reaction vessel, described air bleeding valve supports with reaction vessel and is connected, and be arranged on the both sides of reaction vessel, described control button is arranged on the shell of electronic box, together with described reaction vessel to be fastened and fixed with valve pipe by trip bolt and reaction vessel clamp nut, described reaction vessel supports and is arranged on reaction vessel interior, described heating module resistance wire is fixed on the both sides in electrical heating module, described magnetic stir bar is fixed on the bottom of reaction vessel, described temperature sensor is connected to the centre of electronic box and electrical heating module, described pair of magnet is connected with motor, and be installed in the inside of electronic box, described LCDs is arranged on the shell of electronic box, center in described electrical heating module is placed with reaction vessel, the inwall of electrical heating module and the outer wall of reaction vessel fit tightly.
As preferably, in described container, temperature sensor is the even type temperature sensor of K, and temperature sensor adopts PT100 type temperature sensor.
As preferably, described temperature sensor is fixed in the aperture of electrical heating module bottom by cutting ferrule screw, and the probe of temperature sensor is close to the bottom of electrical heating module.
As preferably, described electrical heating module is cylindrical furnace, and body is built with tubular silicon combustion chamber, and the thickness of the bottom of electrical heating module is 10mm, and is provided with aperture.
The utility model increases 1-3 temperature sensor in electrical heating module bottom, detection heating module real time temperature, by the temperature sensor in reactor, show the temperature difference of reactor and heating module, controller software receives the temperature signal in heating part and reactor, and the heating rate controlling heating part is eliminated temperature error, makes heating-up temperature reach consistent with the temperature in reactor, realize temperature equalization, reduce error within twice.Temperature error is reduced greatly, and temperature curve is balanced, ensures the reliability of accurate experiment, and reaches the effect reducing energy consumption.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the utility model is described in further details.
As shown in Figure 1, a kind of multi-point temp sensing high-temperature reactor of the utility model embodiment, comprises Pressure gauge 1, safety valve 2, temperature sensor 3 in container, air bleeding valve 4, control button 5, reaction vessel clamp nut 6, trip bolt 7, reaction vessel 8, reaction vessel supports 9, heating module resistance wire 10, magnetic stir bar 11, temperature sensor 12, two magnet 13, LCDs 14, motor 15, electronic box 16 and electrical heating module 17, described Pressure gauge 1 is connected to the top of reaction vessel 8 by pipeline, described safety valve 2 is arranged on the lower end of Pressure gauge 1, in described container, temperature sensor 3 is connected to the top of reaction vessel 8, described air bleeding valve 4 and reaction vessel support 9 and are connected, and be arranged on the both sides of reaction vessel 8, described control button 5 is arranged on the shell of electronic box 16, together with described reaction vessel 8 to be fastened and fixed with valve pipe by trip bolt 7 and reaction vessel clamp nut 6, described reaction vessel supports 9 and is arranged on reaction vessel 8 inside, described heating module resistance wire 10 is fixed on the both sides in electrical heating module 17, described magnetic stir bar 11 is fixed on the bottom of reaction vessel 8, described temperature sensor 12 is connected to the centre of electronic box 16 and electrical heating module 17, described pair of magnet 13 is connected with motor 15, and be installed in the inside of electronic box 16, described LCDs 14 is arranged on the shell of electronic box 16, center in described electrical heating module 17 is placed with reaction vessel 8, the inwall of electrical heating module 17 and the outer wall of reaction vessel 8 fit tightly.
As preferably, in described container, temperature sensor 3 is the even type temperature sensor of K, and temperature sensor 12 adopts PT100 type temperature sensor.
As preferably, described temperature sensor 12 is fixed in the aperture bottom electrical heating module 17 by cutting ferrule screw, and the probe of temperature sensor 12 is close to the bottom of electrical heating module 17.
As preferably, described electrical heating module 17 is cylindrical furnace, and body is built with tubular silicon combustion chamber, and the thickness of the bottom of electrical heating module 17 is 10mm, and is provided with aperture.
Reaction vessel 8 of the present utility model is processed by stainless steel, is built-in with temperature sensor 3 in container.Electrical heating module 17 is cylindrical furnace, and for aluminium is cast, body is built with tubular silicon combustion chamber, and heating module resistance wire 10 wears connection wherein, and have heat-transfer effect good, the features such as quick heating, lower end side is equipped with socket, is connected during use by cable with control button 5.Reaction vessel 8 is placed in the center of cast aluminium electrical heating module 17, and the outer wall of reaction vessel 8 and the inwall of electrical heating module 17 fit tightly, and realize the function of heat conduction; Be ten mm of thickness bottom electrical heating module 17, without resistive heater, convenient punching, reload temperature sensor, the bottom of electrical heating module 17 is control section.The magnetic stirring function adopted is two magnet modes, and the bottom of base is also provided with two magnet 13, and two magnet 13 is connected with motor 15.During work, two magnet 13 drives the magnetic stir bar 11 being surrounded by teflon outer to rotate, and motor 15 controls the rotating speed of magnetic stir bar 11.
The above; be only preferred embodiment of the present utility model; not in order to limit the utility model, every above embodiment is done according to technical spirit of the present utility model any trickle amendment, equivalently replace and improve, within the protection domain that all should be included in technical solutions of the utility model.

Claims (4)

1. multi-point temp sensing high-temperature reactor, comprises Pressure gauge, safety valve, temperature sensor in container, air bleeding valve, control button, reaction vessel clamp nut, trip bolt, reaction vessel, reaction vessel supports, heating module resistance wire, magnetic stir bar, temperature sensor, two magnet, LCDs, motor, electronic box and electrical heating module, described safety valve is arranged on manometric lower end, in described container, temperature sensor is connected to the top of reaction vessel, described air bleeding valve supports with reaction vessel and is connected, and be arranged on the both sides of reaction vessel, described control button is arranged on the shell of electronic box, together with described reaction vessel to be fastened and fixed with valve pipe by trip bolt and reaction vessel clamp nut, described reaction vessel supports and is arranged on reaction vessel interior, it is characterized in that: described Pressure gauge is connected to the top of reaction vessel by pipeline, described heating module resistance wire is fixed on the both sides in electrical heating module, described magnetic stir bar is fixed on the bottom of reaction vessel, described temperature sensor is connected to the centre of electronic box and electrical heating module, described pair of magnet is connected with motor, and be installed in the inside of electronic box, described LCDs is arranged on the shell of electronic box, center in described electrical heating module is placed with reaction vessel, the inwall of electrical heating module and the outer wall of reaction vessel fit tightly.
2. multi-point temp sensing high-temperature reactor according to claim 1, is characterized in that: in described container, temperature sensor is the even type temperature sensor of K, and temperature sensor adopts PT100 type temperature sensor.
3. multi-point temp sensing high-temperature reactor according to claim 1, it is characterized in that: described temperature sensor is fixed in the aperture of electrical heating module bottom by cutting ferrule screw, the probe of temperature sensor is close to the bottom of electrical heating module.
4. multi-point temp sensing high-temperature reactor according to claim 1, is characterized in that: described electrical heating module is cylindrical furnace, body is built with tubular silicon combustion chamber, and the thickness of the bottom of electrical heating module is 10mm, and is provided with aperture.
CN201520006454.XU 2015-01-07 2015-01-07 Multi-point temp sensing high-temperature reactor Expired - Fee Related CN204485845U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201520006454.XU CN204485845U (en) 2015-01-07 2015-01-07 Multi-point temp sensing high-temperature reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201520006454.XU CN204485845U (en) 2015-01-07 2015-01-07 Multi-point temp sensing high-temperature reactor

Publications (1)

Publication Number Publication Date
CN204485845U true CN204485845U (en) 2015-07-22

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201520006454.XU Expired - Fee Related CN204485845U (en) 2015-01-07 2015-01-07 Multi-point temp sensing high-temperature reactor

Country Status (1)

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CN (1) CN204485845U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106311106A (en) * 2016-08-22 2017-01-11 上海应用技术学院 Safe and high pressure type magnetic heating reactor
CN107952396A (en) * 2018-01-15 2018-04-24 安徽龙谷商贸有限公司 A kind of chemical experiment magnetic stirring apparatus

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106311106A (en) * 2016-08-22 2017-01-11 上海应用技术学院 Safe and high pressure type magnetic heating reactor
CN107952396A (en) * 2018-01-15 2018-04-24 安徽龙谷商贸有限公司 A kind of chemical experiment magnetic stirring apparatus

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150722

Termination date: 20160107