CN204439647U - Laboratory COD automatic analyzer - Google Patents

Laboratory COD automatic analyzer Download PDF

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Publication number
CN204439647U
CN204439647U CN201520126613.XU CN201520126613U CN204439647U CN 204439647 U CN204439647 U CN 204439647U CN 201520126613 U CN201520126613 U CN 201520126613U CN 204439647 U CN204439647 U CN 204439647U
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way valve
digestion tank
electrode
automatic analyzer
peristaltic pump
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刘昊骋
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Qingdao Long Cheng Environmental Technology Co ltd
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Shandong Long Fa Ecotechnology Co Ltd
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Abstract

本实用新型涉及一种水质在线分析仪,特别涉及实验室COD自动分析仪。包括光检计量装置、消解池、电极滴定装置。其还包括注射器以及蠕动泵,所述注射器下端通过三通阀与所述光检计量装置相通,所述光检计量装置下端安装蠕动泵,所述消解池上下两端各设有二通阀以及三通阀,所述消解池上方通过二通阀以及三通阀连接注射器下端的三通阀,所述消解池下端的三通阀一端与所述蠕动泵相通,所述消解池下端的三通阀另一端与所述电极滴定装置连接。本实用新型设计独特,解决了传统的检测液体过程麻烦,误差较大的问题。本实用新型连续自动的进行水质监测分析,省时省力。本实用新型装置设有安全阀,能够平衡消解池内的压力,增加了消解池的安全性。

The utility model relates to an online water quality analyzer, in particular to a laboratory COD automatic analyzer. Including light detection metering device, digestion tank, electrode titration device. It also includes a syringe and a peristaltic pump, the lower end of the syringe communicates with the light detection and metering device through a three-way valve, the lower end of the light detection and metering device is equipped with a peristaltic pump, and the upper and lower ends of the digestion tank are respectively provided with two-way valves and A three-way valve, the top of the digestion tank is connected to the three-way valve at the lower end of the syringe through a two-way valve and a three-way valve, one end of the three-way valve at the lower end of the digestion tank is connected to the peristaltic pump, and the three-way valve at the lower end of the digestion tank is connected One end is connected with the electrode titration device. The utility model has a unique design and solves the problems of troublesome and large errors in the traditional liquid detection process. The utility model continuously and automatically monitors and analyzes water quality, saving time and effort. The device of the utility model is provided with a safety valve, which can balance the pressure in the digestion tank and increase the safety of the digestion tank.

Description

实验室COD自动分析仪Laboratory COD automatic analyzer

技术领域technical field

本发明涉及一种水质在线分析仪,特别涉及实验室COD自动分析仪。The invention relates to an online water quality analyzer, in particular to a laboratory COD automatic analyzer.

背景技术Background technique

化学需氧量COD(Chemical Oxygen Demand)是以化学方法测量水样中需要被氧化的还原性物质的量。废水、废水处理厂出水和受污染的水中,能被强氧化剂氧化的物质(一般为有机物)的氧当量。在河流污染和工业废水性质的研究以及废水处理厂的运行管理中,是一个重要的而且能较快测定的有机物污染参数。COD (Chemical Oxygen Demand) is a chemical method to measure the amount of reducing substances that need to be oxidized in a water sample. The oxygen equivalent of substances (generally organic matter) that can be oxidized by strong oxidants in wastewater, wastewater treatment plant effluent and polluted water. In the study of river pollution and industrial wastewater properties and the operation and management of wastewater treatment plants, it is an important and quickly determined organic pollution parameter.

传统的水质COD分析仪,工作流程不连续,危险系数较大,加重了工作人员的工作,费时费力。The traditional water quality COD analyzer has a discontinuous working process and a high risk factor, which increases the work of the staff and is time-consuming and labor-intensive.

发明内容Contents of the invention

本发明要解决的技术问题是如何克服现有技术存在的不足,提供实验室COD自动分析仪,连续、方便、及时的进行水质监测。The technical problem to be solved by the present invention is how to overcome the deficiencies in the prior art and provide a laboratory COD automatic analyzer for continuous, convenient and timely water quality monitoring.

本发明的技术解决方案是:实验室COD自动分析仪,包括光检计量装置、消解池、电极滴定装置,其还包括注射器以及蠕动泵,所述注射器下端通过三通阀与所述光检计量装置相通,所述光检计量装置下端安装蠕动泵,所述消解池上下两端各设有二通阀以及三通阀,所述消解池上方通过二通阀以及三通阀连接注射器下端的三通阀,所述消解池下端的三通阀一端与所述蠕动泵相通,所述消解池下端的三通阀另一端与所述电极滴定装置连接。The technical solution of the present invention is: a laboratory COD automatic analyzer, including a photodetection metering device, a digestion tank, an electrode titration device, and a syringe and a peristaltic pump, the lower end of the syringe is connected to the photodetection metering device through a three-way valve The devices are connected, and a peristaltic pump is installed at the lower end of the light detection and metering device. Two-way valves and three-way valves are respectively provided at the upper and lower ends of the digestion tank. One end of the three-way valve at the lower end of the digestion tank communicates with the peristaltic pump, and the other end of the three-way valve at the lower end of the digestion tank is connected with the electrode titration device.

作为优选,本发明还包括辅助进药系统,所述辅助进药系统通过进药管连接于电极滴定装置。Preferably, the present invention also includes an auxiliary drug feeding system, which is connected to the electrode titration device through a drug feeding tube.

作为优选,所述辅助进药系统安装有蠕动泵。Preferably, the auxiliary feeding system is equipped with a peristaltic pump.

作为优选,本发明所述电极滴定装置包括磁力搅拌器、滴定杯以及电极,所述滴定杯位于磁力搅拌器上,电极伸入滴定杯中,所述消解池下端的三通阀下端设有滴定管,所述滴定管伸入滴定杯中。As preferably, the electrode titration device of the present invention comprises a magnetic stirrer, a titration cup and an electrode, the titration cup is located on the magnetic stirrer, the electrode extends into the titration cup, the lower end of the three-way valve at the lower end of the digestion tank is provided with a burette, The burette extends into the titration cup.

作为优选,本发明还包括废液槽,所述废液槽通过排出管道与电极滴定装置相通。Preferably, the present invention also includes a waste liquid tank, and the waste liquid tank communicates with the electrode titration device through a discharge pipe.

作为优选,所述排出管道设有两通阀。Preferably, the discharge pipeline is provided with a two-way valve.

本发明设计独特,解决了传统的检测液体过程麻烦,误差较大的问题。本发明将光检计量装置、消解池、电极滴定装置,注射器以及蠕动泵连接在一起,保证连续自动的进行水质监测分析,省时省力。本发明装置设有安全阀,能够平衡消解池内的压力,增加了消解池的安全性。本发明采用三通阀以及两通阀,进一步保证安全。The invention has a unique design and solves the problems of troublesome and large errors in the traditional liquid detection process. The invention connects the optical detection and metering device, the digestion tank, the electrode titration device, the syringe and the peristaltic pump to ensure continuous and automatic water quality monitoring and analysis, saving time and effort. The device of the invention is provided with a safety valve, which can balance the pressure in the digestion tank and increase the safety of the digestion tank. The present invention adopts a three-way valve and a two-way valve to further ensure safety.

附图说明Description of drawings

下面结合附图和实施例对本发明作进一步说明。The present invention will be further described below in conjunction with drawings and embodiments.

图1为实验室COD自动分析仪结构示意图;Fig. 1 is the schematic structural diagram of laboratory COD automatic analyzer;

具体实施方式Detailed ways

以下参照附图,详细说明本发明实验室COD自动分析仪。The laboratory COD automatic analyzer of the present invention will be described in detail below with reference to the accompanying drawings.

如图1所示,实验室COD自动分析仪,包括光检计量装置1、消解池2、电极滴定装置3、注射器4以及蠕动泵5。以上各部件的连接方式为:所述注射器4下端通过三通阀a与所述光检计量装置1相通,便于注射器4给予所述光检计量装置1压力,所述光检计量装置1下端安装蠕动泵5,样品通过蠕动泵5进入光检计量装置1中。As shown in FIG. 1 , the laboratory COD automatic analyzer includes a light detection and metering device 1 , a digestion tank 2 , an electrode titration device 3 , a syringe 4 and a peristaltic pump 5 . The connection mode of the above components is as follows: the lower end of the syringe 4 communicates with the photodetection and metering device 1 through a three-way valve a, so that the syringe 4 can give the pressure to the photodetection and metering device 1, and the lower end of the photodetection and metering device 1 is installed A peristaltic pump 5, through which the sample enters the photodetection metering device 1.

为保证消解池2的安全,所述消解池2上下两端由内向外各设有二通阀b以及三通阀a,所述消解池2上方通过二通阀b以及三通阀a连接注射器4下端的三通阀a上,便于排出消解池2内的气泡,平衡压力。In order to ensure the safety of the digestion tank 2, the upper and lower ends of the digestion tank 2 are respectively provided with a two-way valve b and a three-way valve a from the inside to the outside, and the top of the digestion tank 2 is connected to the syringe through the two-way valve b and the three-way valve a 4. On the three-way valve a at the lower end, it is convenient to discharge the air bubbles in the digestion tank 2 and balance the pressure.

所述消解池2下端的三通阀a一端与所述蠕动泵5相通,便于样品从光检计量装置1中通过蠕动泵5缓慢进入消解池2中,进行消解处理。One end of the three-way valve a at the lower end of the digestion tank 2 communicates with the peristaltic pump 5, so that the sample can slowly enter the digestion tank 2 from the light detection and metering device 1 through the peristaltic pump 5 for digestion.

为方便下一步过程,所述消解池2下端的三通阀另一端与所述电极滴定装置3连接,便于消解完成的样品通过三通阀a进入电极滴定装置3,进行滴定反应,确认含量。本发明所述电极滴定装置3包括磁力搅拌器31、滴定杯32以及电极33,所述滴定杯32位于磁力搅拌器31上,电极33伸入滴定杯32中,所述消解池2下端的三通阀a下端设有滴定管21,所述滴定管21伸入滴定杯32中,方便消解完成的样品通过三通阀a进入滴定管21然后再进行电极滴定。为实现连续过程,本发明还包括废液槽6,所述废液槽6通过排出管道直接连接在滴定杯32下端,同时排出管道也设有两通阀b,方便开关。For the convenience of the next step, the other end of the three-way valve at the lower end of the digestion tank 2 is connected to the electrode titration device 3, so that the digested sample enters the electrode titration device 3 through the three-way valve a for titration reaction to confirm the content. The electrode titration device 3 of the present invention comprises a magnetic stirrer 31, a titration cup 32 and an electrode 33. The titration cup 32 is located on the magnetic stirrer 31, and the electrode 33 extends into the titration cup 32. A burette 21 is arranged at the lower end of the through valve a, and the burette 21 extends into the titration cup 32, so that the sample that is conveniently digested enters the burette 21 through the three-way valve a and then undergoes electrode titration. In order to realize the continuous process, the present invention also includes a waste liquid tank 6, which is directly connected to the lower end of the titration cup 32 through a discharge pipe, and the discharge pipe is also provided with a two-way valve b for easy opening and closing.

为保证样品检测,本发明还包括辅助进药系统7,所述辅助进药7系统通过进药管71直接连接于滴定杯32中,为方便进药,进药系统7设有蠕动泵,方便药物匀速进入。In order to ensure sample detection, the present invention also includes an auxiliary drug feeding system 7, which is directly connected to the titration cup 32 through a drug feeding tube 71. For the convenience of drug feeding, the drug feeding system 7 is provided with a peristaltic pump, which is convenient. The drug enters at a uniform rate.

对所公开的实施例的上述说明,使本领域专业技术人员能够实现或使用本发明。对这些实施例的多种修改对本领域的专业技术人员来说将是显而易见的,本文中所定义的一般原理可以在不脱离本发明的精神或范围的情况下,在其它实施例中实现。因此,本发明将不会被限制于本文所示的实施例,而是要符合与本文所公开的原理和新颖特点相一致的最宽的范围。The above description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the general principles defined herein may be implemented in other embodiments without departing from the spirit or scope of the invention. Therefore, the present invention will not be limited to the embodiments shown herein, but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (6)

1.实验室COD自动分析仪,包括光检计量装置、消解池、电极滴定装置,其特征在于:还包括注射器以及蠕动泵,所述注射器下端通过三通阀与所述光检计量装置相通,所述光检计量装置下端安装蠕动泵,所述消解池上下两端各设有二通阀以及三通阀,所述消解池上方通过二通阀以及三通阀连接注射器下端的三通阀,所述消解池下端的三通阀一端与所述蠕动泵相通,所述消解池下端的三通阀另一端与所述电极滴定装置连接。1. laboratory COD automatic analyzer, comprises light detection metering device, digestion tank, electrode titration device, is characterized in that: also comprises syringe and peristaltic pump, and described syringe lower end communicates with described light detection metering device by three-way valve, A peristaltic pump is installed at the lower end of the optical detection and metering device, and a two-way valve and a three-way valve are respectively provided at the upper and lower ends of the digestion tank, and the upper end of the digestion tank is connected to the three-way valve at the lower end of the syringe through the two-way valve and the three-way valve, One end of the three-way valve at the lower end of the digestion tank communicates with the peristaltic pump, and the other end of the three-way valve at the lower end of the digestion tank is connected with the electrode titration device. 2.根据权利要求1所述的实验室COD自动分析仪,其特征在于:还包括辅助进药系统,所述辅助进药系统通过进药管连接于电极滴定装置。2 . The laboratory COD automatic analyzer according to claim 1 , further comprising an auxiliary drug feeding system connected to the electrode titration device through a drug feeding tube. 3 . 3.根据权利要求2所述的实验室COD自动分析仪,其特征在于:所述辅助进药系统安装有蠕动泵。3. The laboratory COD automatic analyzer according to claim 2, characterized in that: the auxiliary medicine feeding system is equipped with a peristaltic pump. 4.根据权利要求1或2所述的实验室COD自动分析仪,其特征在于:所述电极滴定装置包括磁力搅拌器、滴定杯以及电极,所述滴定杯位于磁力搅拌器上,电极伸入滴定杯中,所述消解池下端的三通阀下端设有滴定管,所述滴定管伸入滴定杯中。4. laboratory COD automatic analyzer according to claim 1 or 2, is characterized in that: described electrode titration device comprises magnetic stirrer, titration cup and electrode, and described titration cup is positioned at magnetic stirrer, and electrode stretches into In the titration cup, a burette is provided at the lower end of the three-way valve at the lower end of the digestion tank, and the burette extends into the titration cup. 5.根据权利要求1至4所述的实验室COD自动分析仪,其特征在于:还包括废液槽,所述废液槽通过排出管道与电极滴定装置相通。5. The laboratory COD automatic analyzer according to claims 1 to 4, characterized in that it also includes a waste liquid tank, and the waste liquid tank communicates with the electrode titration device through a discharge pipe. 6.根据权利要求5所述的实验室COD自动分析仪,其特征在于:所述排出管道设有两通阀。6. The laboratory COD automatic analyzer according to claim 5, characterized in that: the discharge pipeline is provided with a two-way valve.
CN201520126613.XU 2015-03-05 2015-03-05 Laboratory COD automatic analyzer Expired - Lifetime CN204439647U (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107132362A (en) * 2017-05-16 2017-09-05 江苏德林环保技术有限公司 A kind of COD automatic Titrations detection method
CN111595633A (en) * 2020-06-22 2020-08-28 海南核电有限公司 Mobile oil trace moisture monitoring device and monitoring method thereof
CN112129959A (en) * 2020-09-25 2020-12-25 上海安杰环保科技股份有限公司 Full-automatic chemical oxygen demand analyzer based on different liquid transfer flow paths
CN112611833A (en) * 2020-12-28 2021-04-06 浙江大学昆山创新中心 Automatic titration device for chemical oxygen demand
CN117288884A (en) * 2023-09-20 2023-12-26 厦门市吉龙德环境工程有限公司 An automatic analyzer titration flow path and titration analysis method

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107132362A (en) * 2017-05-16 2017-09-05 江苏德林环保技术有限公司 A kind of COD automatic Titrations detection method
CN107132362B (en) * 2017-05-16 2018-07-03 江苏德林环保技术有限公司 A kind of COD automatic Titrations detection method
CN111595633A (en) * 2020-06-22 2020-08-28 海南核电有限公司 Mobile oil trace moisture monitoring device and monitoring method thereof
CN112129959A (en) * 2020-09-25 2020-12-25 上海安杰环保科技股份有限公司 Full-automatic chemical oxygen demand analyzer based on different liquid transfer flow paths
CN112129959B (en) * 2020-09-25 2021-06-25 上海安杰环保科技股份有限公司 Fully automatic chemical oxygen demand analyzer based on different liquid transfer flow paths
CN112611833A (en) * 2020-12-28 2021-04-06 浙江大学昆山创新中心 Automatic titration device for chemical oxygen demand
CN112611833B (en) * 2020-12-28 2022-08-23 浙江大学昆山创新中心 Automatic titration device for chemical oxygen demand
CN117288884A (en) * 2023-09-20 2023-12-26 厦门市吉龙德环境工程有限公司 An automatic analyzer titration flow path and titration analysis method

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