The dehydrating unit of chromatograph gas source purification
Technical field
The utility model relates to a kind of petroleum prospecting logging equipment, particularly relates to a kind of dehydrating unit of chromatograph gas source purification.
Background technology
Chromatograph is the core devices of logging equipment system, is the visual plant finding hydrocarbon zone and drilling engineering security monitoring in oil-gas exploration process.At the scene in use procedure, the humidity of chromatograph to point gassing sample has higher requirement, the chromatograph of current use all must adopt gas dehumidification drying process, but owing to being subject to the restriction of technical conditions, Ge Jia well logging company all adopts chemical agent anhydrous calcium chloride (hydrocarbon gas) and silica gel (hydrogen, air) dehumidifying.And mainly there is following shortcoming in chemical agent dehumidification process: 1) chemical agent moisture removal is less, chromatogram work just needs after 3 working days to change chemical agent, by the sea, drilling platform and rainy humid area change then more frequent, normally works cause interference when changing chemical agent to chromatogram; 2) anhydrous calcium chloride easily expands, lumps in adsorption and dehumidification process, not easily processes after using; Anhydrous calcium chloride aqueous solution is alkalescent simultaneously, has certain danger; 3) chemical agent easily produces medicament powder and causes chromatogram pollution or airway blockage; 4) the chemical agent dehumidizier phase after a procedure, effect on moisture extraction reduces, and chromatogram can cause amplifier decreasing insulating because of high humidity, and during the operation of high sensitivity gear, chromatogram response declines, and Chromatogram Baseline is unstable.
Summary of the invention
In order to solve the problems of the technologies described above, the utility model provides a kind of dehydrating unit of chromatograph gas source purification, chemical agent need not be used can to meet the test request of chromatograph, both improve measuring accuracy, and again reduced testing cost.
For this reason, the technical solution of the utility model is as follows:
A dehydrating unit for chromatograph gas source purification, comprises gas drying instrument and moisture trap; Described gas drying instrument comprises shell, is fixed on the mounting base of outer casing bottom, is symmetricly set in the louvre of shell both sides, insulation cladding, condensation chamber, heating radiator, semiconductor cooling condenser and stainless steel pipeline; Described insulation cladding is fixed on mounting base, its inside is embedded with condensation chamber, top is provided with semiconductor cooling condenser, the chamber wall of described condensation chamber is individually fixed in mounting base and insulation cladding top, between the cold junction that described condensation chamber is formed at described semiconductor cooling condenser and mounting base; Described condensation chamber outer wall is provided with temperature sensor, for determining whether semiconductor cooling condenser is opened; Described heating radiator is installed on the outside in semiconductor cooling condenser hot junction; Described stainless steel pipeline is located in described condensation chamber, and its one end extends to the air intake opening place of described shell, and the other end is connected with described moisture trap through the gas outlet of described shell.Temperature sensor is used for Real-Time Monitoring condensation chamber temperature, and when condensation cavity temperature is higher than preset upper limit value, semiconductor cooling condenser is opened, and cold junction freezes; When condensation cavity temperature is lower than preset lower limit value, semiconductor cooling condenser is out of service.
Described stainless steel pipeline is equipped with pressure transducer at air intake opening place.Preferred pressure sensor is connected with a piezo buzzer.
Air intake opening and gas outlet interface adopt pagoda joint.
Described stainless steel pipeline is the horizontal pipeline of multistage connected by bend pipe, and the inlet end of every section of horizontal pipeline is higher 5 ° on horizontal level than outlet side.
Described condensation chamber is made up of two pieces of identical aluminium alloy heat-conducting blocks, and two pieces of aluminium alloy heat-conducting block faying faces are processed with the groove of combining closely with stainless steel pipeline, and condensation chamber is fixed on mounting base; Stainless steel pipeline is embedded in the groove of condensation chamber.
Be aluminum alloy material outside described insulation cladding, embedded with high-density glass fibre cotton.
The container of described moisture trap collection water is connected to level sensor, and two probes of described level sensor are longitudinally arranged on described moisture trap and collect on the sidewall of the container of water.
A dehydrating unit for chromatograph gas source purification, comprises gas drying instrument, moisture trap and main control board; Described gas drying instrument comprises shell, is fixed on the mounting base of outer casing bottom, is symmetricly set in the louvre of shell both sides, insulation cladding, condensation chamber, semiconductor cooling condenser, heating radiator, stainless steel pipeline, pressure transducer and level sensor, described insulation cladding is fixed on mounting base, its inside is embedded with condensation chamber, top is provided with semiconductor cooling condenser, the chamber wall of described condensation chamber is individually fixed in mounting base and insulation cladding top, between the cold junction that described condensation chamber is formed at described semiconductor cooling condenser and mounting base; Described condensation chamber outer wall is provided with temperature sensor, for determining whether semiconductor cooling condenser is opened; Described heating radiator is installed on the outside in semiconductor cooling condenser hot junction; Described stainless steel pipeline is located in described condensation chamber, and its one end extends to the air intake opening place of described shell and pressure transducer is housed, and the other end is connected with described moisture trap through the gas outlet of described shell; Two probes of described level sensor are longitudinally arranged on described moisture trap and collect on the sidewall of the container of water; Described main control board is respectively equipped with the circuit be connected with described semiconductor cooling condenser, pressure transducer, level sensor, temperature sensor and power supply, described main control board is also equipped with whether connect for display power supply power light, for showing refrigeration pilot lamp that whether semiconductor cooling condenser work, whether reaching the water-level alarm pilot lamp of the upper limit for showing the pressure alarm pilot lamp whether admission pressure exceed standard and the container middle water level of collecting water for showing moisture trap.
The upper limit place of water level in container is located at the probe of upper described level sensor in position.
Described level sensor is also connected with a piezo buzzer.Preferred pressure sensor is connected with a piezo buzzer I.Described level sensor can be connected with same piezo buzzer with pressure transducer.
The dehydrating unit of this chromatograph gas source purification has the following advantages:
1) adopt independent design, equipment little (150mm*150mm*90mm), quality light (0.5Kg), is easy to carry;
2) gas circuit adopts pagoda joint, and plug and play is easy to use;
3) dehydrating unit of this chromatograph gas source purification is not only applicable to chromatograph, and the FID hydrogen flame color that can also be used for using in comprehensive logging instrument, gas instrument, geologic parameter instrument is composed, the test air feed of TCD thermal conductance chromatogram.
4) chemical agent removal moisture drying mode, need change chemical agent in 3 days, and the dehydrating unit of this utility model chromatograph gas source purification can continuous dehumidifying, drying, and without daily consumptive material, individual well can save consumables cost more than 1300 yuan.
5) this chromatograph gas source purification dehydrating unit dehumidifying scope wide: can work under 25%-95% humidity, moisture removal is large: 300mL/D, without medicament powder generation, totally pollution-free; Removal moisture drying is effective, stable, reliable.
Accompanying drawing explanation
Fig. 1 is the structural representation of the dehydrating unit of chromatograph gas source purification of the present utility model.
Embodiment
Be described in detail below in conjunction with the dehydrating unit of the drawings and specific embodiments to the chromatograph gas source purification that the utility model provides.
As described in Figure 1, a kind of dehydrating unit of chromatograph gas source purification, comprises gas drying instrument 0 and moisture trap 21; Gas drying instrument 0 comprises shell 19, is fixed on the mounting base 18 bottom shell 19, the louvre 16 being symmetricly set in shell both sides, insulation cladding 15, condensation chamber 13, heating radiator 11, semiconductor cooling condenser 12 and stainless steel pipeline 14; Insulation cladding 15 is fixed on mounting base 18, and its inside is embedded with condensation chamber 13, top is provided with semiconductor cooling condenser 12; The chamber wall of condensation chamber 13 is individually fixed in mounting base 18 and insulation cladding 15 top, and condensation chamber 13 is formed between the cold junction 12-1 of semiconductor cooling condenser 12 and mounting base 18; Condensation chamber 13 outer wall is provided with for determining the temperature sensor 17 whether semiconductor cooling condenser is opened; Heating radiator 11 is installed on the outside of semiconductor cooling condenser hot junction 12-2; Stainless steel pipeline 14 is located in condensation chamber 13, and its one end extends to air intake opening 3 place of shell 19, and the other end is connected with moisture trap 21 through the gas outlet 20 of shell 19.The interface at air intake opening 3 and gas outlet 20 place adopts pagoda joint.Plug and play, easy to use.
In an embodiment of the present utility model, stainless steel pipeline 14 is equipped with pressure transducer 10 at air intake opening 3 place.Preferred pressure sensor 10 is connected with a piezo buzzer.
In another embodiment of the present utility model, described stainless steel pipeline 14 is the horizontal pipeline of multistage connected by bend pipe, and the inlet end of every section of horizontal pipeline is higher 5 ° on horizontal level than outlet side.
In the 3rd embodiment of the present utility model, the container that water collected by moisture trap 21 is connected to level sensor 9, two probes 24,25 of level sensor 9 are longitudinally arranged on moisture trap 21 and collect on the sidewall of the container of water.Optimum position is located at the upper limit place of water level 27 at upper probe 25.
Preferable water level sensor 9 is connected with a piezo buzzer 23 again; When water level 27 did not have upper probe, this piezo buzzer 23 sound.
Condensation chamber 13 is made up of two pieces of identical aluminium alloy heat-conducting blocks, and two pieces of aluminium alloy heat-conducting block faying faces are processed with the groove of combining closely with stainless steel pipeline 14, and condensation chamber is fixed on mounting base 18; Stainless steel pipeline 14 is embedded in the groove of condensation chamber 13.
Described insulation cladding 15 selects insulation material, is aluminium alloy outside it, embedded with high-density glass fibre cotton.
Be below a preferred embodiment of the present utility model: a kind of dehydrating unit of chromatograph gas source purification, comprises gas drying instrument 0, moisture trap 21 and main control board 8, gas drying instrument 0 comprises shell 19, be fixed on the mounting base 18 bottom shell 19, be symmetricly set in the louvre 16 of shell both sides, insulation cladding 15, condensation chamber 13, semiconductor cooling condenser 12, heating radiator 11, stainless steel pipeline 14, pressure transducer 10 and level sensor 9, insulation cladding 15 is fixed on mounting base 18, its inside is embedded with condensation chamber 13, top is provided with semiconductor cooling condenser 12, the chamber wall of condensation chamber 13 is individually fixed in mounting base 18 and insulation cladding 15 top, condensation chamber 13 is formed between the cold junction 12-1 of semiconductor cooling condenser 12 and mounting base 18, condensation chamber 13 outer wall is provided with for determining the temperature sensor 17 whether semiconductor cooling condenser is opened, heating radiator 11 is installed on the outside of semiconductor cooling condenser hot junction 12-2, stainless steel pipeline 14 is located in condensation chamber 13, and its one end extends to air intake opening 3 place of described shell 19 and pressure transducer 10 is housed, and the other end is connected with described moisture trap 21 through the gas outlet 20 of described shell 19, two probes 24,25 of level sensor 9 are longitudinally arranged on described moisture trap 21 and collect on the sidewall of the container of water, optimum position is located at the upper limit place of water level 27 at upper probe 25, main control board 8 is respectively equipped with the circuit be connected with described semiconductor cooling condenser 12, pressure transducer 10, level sensor 9 and temperature sensor 17 and power supply 2, main control board 8 is also equipped with whether connect for display power supply power light 4, for showing refrigeration pilot lamp 5 that whether semiconductor cooling condenser work, whether reaching the water-level alarm pilot lamp 7 of the upper limit for showing the pressure alarm pilot lamp 6 whether admission pressure exceed standard and the container middle water level of collecting water for showing moisture trap 21.Preferable water level sensor 9 is connected with a piezo buzzer 23; When water level 27 did not have upper probe, this piezo buzzer 23 sound.Preferred pressure sensor 10 is connected with a piezo buzzer.Level sensor 9 can be connected with same pressure type hummer 23 with pressure transducer 10.
During use: switch on power 2, open switch 1, power light 4 is bright, temperature sensor 17 detects, condensation cavity temperature is higher than (factory default set temperature when 5 degrees Celsius, adjustable), semiconductor cooling condenser 12 starts refrigeration, refrigeration pilot lamp 5 is bright, and the cold junction 12-1 of semiconductor cooling condenser 12 starts cooling, through heat-conduction effect, (factory default set temperature when condensation chamber 13 temperature that is interior, stainless steel pipeline 14 starts to be cooled to 3 degrees Celsius, adjustable), semiconductor cooling condenser 12 stops refrigeration, and refrigeration pilot lamp 5 extinguishes, and the heat that the hot junction 12-2 of semiconductor cooling condenser 12 produces is by heating radiator 11, shed through louvre 16, open chromatograph, ventilate from air intake opening 3, gas enters chromatograph through pressure transducer 10, stainless steel pipeline 14 and moisture trap 21, gas flow is when stainless steel pipeline 14, due to low temperature, water vapour is wherein liquefied as water, entering moisture trap 21 will exist in the container of collection water after water filtration, when water level 27 floods two probes 24 of level sensor simultaneously, when 25, water-level alarm pilot lamp 7 circuit turn-on, pilot lamp brightens, piezo buzzer 23 sends chimes of doom, the draining valve 22 that prompting operator opens moisture trap 21 carries out draining, when water level 27 in moisture trap 21 be down to position below the position of upper probe 25 time, water level alarm pilot lamp 7 circuit disconnects, water-level alarm pilot lamp 7 extinguishes, piezo buzzer 23 stop alarm.
When the gas circuit entering gas drying instrument 0 front end occurs to block, in pipeline, gaseous tension (negative pressure) can rise, pressure transducer 10 is monitored pipeline inner pressure in real time, when pressure reaches predetermined alarming value (setting of 15Kpa factory default) will activation pressure report to the police (pressure alarm pilot lamp 6 lights, alarm relay starts, piezo buzzer 23 sends chimes of doom), remind operating personnel to check that pipeline is fixed a breakdown.