CN204412315U - For the rack for test tube that nitrogen phosphorus is cleared up - Google Patents

For the rack for test tube that nitrogen phosphorus is cleared up Download PDF

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Publication number
CN204412315U
CN204412315U CN201420777960.4U CN201420777960U CN204412315U CN 204412315 U CN204412315 U CN 204412315U CN 201420777960 U CN201420777960 U CN 201420777960U CN 204412315 U CN204412315 U CN 204412315U
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CN
China
Prior art keywords
test tube
rack
hole
pillar
mounting plate
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420777960.4U
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Chinese (zh)
Inventor
王晓欧
孙鹏
田一梅
赵新华
彭森
吴卿
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Tianjin University
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Tianjin University
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Priority to CN201420777960.4U priority Critical patent/CN204412315U/en
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Publication of CN204412315U publication Critical patent/CN204412315U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a kind of rack for test tube cleared up for nitrogen phosphorus, adopt the preparation of acrylic resin (PP), polytetrafluoroethylene (PTFE) (PTFE) high-temperature resistance plastice, rack for test tube is disposed with base plate, bottom plate and mounting plate from the bottom to top, is circular configuration; The edge of base plate is provided with pillar, and it is in aggregates that base plate and bottom plate pass through pillar structure; Base plate is provided with groove uniform sequentially, bottom plate and groove are provided with through hole correspondingly, block is provided with accordingly with through hole below mounting plate, test tube is placed in groove through through hole, mounting plate is fixed by pillar hole and knob screw and bottom plate, and block adapts with the top of test tube.When this rack for test tube uses, first press test tube, shake up water sample, then knob screw is loosened, suitably improve mounting plate, then be placed in high-pressure bottle and clear up.The utility model solves the problem of complex operation when using conventional rack for test tube mensuration total phosphorus, total nitrogen, has ensured safety, has saved personnel and time.

Description

For the rack for test tube that nitrogen phosphorus is cleared up
Technical field
The utility model, about experiment rack for test tube, is specifically related to a kind of rack for test tube cleared up for nitrogen phosphorus.
Background technology
In the water that " water and waste water method for monitoring and analyzing " (the 4th edition) relates to and waste water, total phosphorus yield needs to carry out pretreatment to water sample, preprocess method conventional in laboratory is digest by potassium persulfate, concrete operation step described in this book is: draw 25.0ml and mix water sample if desired, take the circumstances into consideration water sampling less, and add water to 25ml, phosphorus content is made to be no more than 30ug in 50ml tool plug graded tube, add potassium persulfate solution 4ml, mouth of pipe bag one fritter gauze after jumping a queue also is tightened with line, in order to avoid glass stopper is gone out during heating.Tool plug graded tube is placed in large beaker, is placed in autoclave or pressure cooker heats, treat that pot inner pressure reaches 1.1kg/cm 2time (relevant temperature is 120 DEG C), after regulating furnace temperature to make this pressure of maintenance 30min, stop heating, after gauge hand is down to zero, taking-up lets cool.As solutions turbid, then use Filter paper filtering, constant volume after washing.
The assay method of the water that " water and waste water method for monitoring and analyzing " (the 4th edition) relates to and Determination of Total Nitrogen in Waste Water has potassium persulfate oxidation-ultraviolet spectrophotometry and gas molecule in space absorption spectrometry, two kinds of methods all need water sample to put into color-comparison tube, add constant volume after alkaline chitinase, close plug, bottle stopper is wrapped with gauze and yarn rope, in case splash out, then colorimetric cylinder is put into High pressure steam sterilizer and clear up.
From the above, all need to clear up to the mensuration of total phosphorus, total nitrogen in water and waste water, before clearing up, need the bottle stopper wrapping color-comparison tube with gauze and yarn rope, in order to avoid glass stopper is gone out during heating.Conventional rack for test tube is the wooden or bamboo shelf in 6 holes and 12 holes, without any other parts, so just make experimenter spend the plenty of time to be carried out one by one by the test tube on rack for test tube shaking up and use gauze and yarn rope bottle stopper to be wrapped clear up water sample, clear up after also need test tube to put back to rack for test tube one by one in order.As can be seen here, for the mensuration of total phosphorus, total nitrogen in water and waste water, conventional rack for test tube complex operation and a large amount of time can be wasted, and gauze and yarn rope need often to change.
Through finding the literature search of prior art, if CN201210366462.6 is a kind of Multifunctional test tube shelf, rack for test tube flexible adjustment in this invention, be convenient to rack for test tube grafting each other, solve that existing rack for test tube structure is fixed, can not be regulated, storage capacity is little, the shortcoming of function singleness to a certain extent; ZL201120562088.8 is a kind of device being elevated upset rack for test tube, device in this utility model solves the trouble that test tube need be overturn one by one, laboratory technician can be made to reduce by the working time of 20 times, and the distance with sterilamp can be reduced when carrying out sterilamp irradiation by hoisting depth, high degree add exposure intensity, improve sterilizing efficiency; ZL201320479509.X is a kind of rack for test tube, this rack for test tube when testing can placing height higher than its test tube, can also the low test tube of placing height, collect folding for rack for test tube after finishing experiment, greatly can save space, conveniently to store; CN201410060580.3 is a kind of rack for test tube with locking function, this rack for test tube can be widely used in test tube transport, deposit and in other operating process, ensured the security of test tube.But the full inconvenience of above-mentioned rack for test tube of the prior art is used for total phosphorus, the clearing up of total nitrogen.
Summary of the invention
The purpose of this utility model, during for water and waste water monitoring analysis, the existing shortcoming that rack for test tube inconvenience is used for total phosphorus, total nitrogen is cleared up, provides a kind of rack for test tube being suitable for nitrogen phosphorus simply and easily and clearing up.
The utility model is achieved by following technical solution.
A kind of rack for test tube cleared up for nitrogen phosphorus, comprise pillar, base plate, bottom plate, mounting plate, knob screw, it is characterized in that, rack for test tube is disposed with base plate 1, bottom plate 2 and mounting plate 3 from the bottom to top, described base plate 1, bottom plate 2 and mounting plate 3 is circular configuration, be provided with pillar 4 evenly, symmetrically at the circular edge place of base plate 1, base plate 1 and bottom plate 2 form an entirety by pillar 4; Base plate 1 is provided with circular groove 6 uniform sequentially, and groove 6 matches with the bottom of test tube; Bottom plate 2 is provided with and groove 6 through hole 7 one to one, through hole 7 and groove 6 are positioned on same vertical axis, and test tube is placed in groove 6 through through hole 7; Mounting plate 3 is provided with pillar hole 10 with the correspondence position of pillar 4, pillar hole 10 is provided with screw 11 with the upright position of mounting plate 3 sidewall, knob screw 9 is provided with in screw 11, pillar 4 passes the pillar hole 10 of mounting plate 3 and knob screw 9 passes screw 11 and mounting plate 3 fixes, and knob screw 9 makes mounting plate 3 dismantle and can regulate its height; Position corresponding with through hole 7 below mounting plate 3 is provided with block 8, and block 8 and through hole 7 are positioned on same vertical axis, and block 8 adapts with the top of test tube;
Described pillar 4 is 4; 2 portions 5 of giving a hand are provided with, in order to steadily to hold rack for test tube above bottom plate 2, on two symmetrical pillars 4;
Described 2 surfaces, portion 5 of giving a hand are provided with annular knurl, the shape that portion 5 of giving a hand is recessed in middle convex two ends, match with the palm of experimenter.
The diameter of described groove 6 is more than or equal to the diameter bottom test tube.
The diameter of described through hole 7 is consistent with the diameter of groove 6.
The diameter of described block 8 is more than or equal to the diameter of test tube mouth, is highly 1 ~ 2cm.
The whole height of this rack for test tube is 19 ~ 23cm, and diameter is 16 ~ 20cm.
The thickness of this rack for test tube base plate 1 is 1cm, the thickness of bottom plate 2 and mounting plate 3 is 0.5cm, and the diameter of pillar 4 is 1cm.
This rack for test tube adopts acrylic resin-PP, polytetrafluoroethylene (PTFE)-PTFE high-temperature resistance plastice preparation.
Compared with prior art, tool has the following advantages the utility model:
1. solve when measuring total phosphorus, total nitrogen, test tube need be carried out one by one shake up and use gauze and yarn rope bottle stopper to be wrapped clear up water sample, clear up after also need test tube to put back to one by one in order the trouble of rack for test tube, laboratory technician can be made to reduce the extensive work time.
2. rack for test tube adopts acrylic resin (PP), the high-temperature resistance plastice such as polytetrafluoroethylene (PTFE) (PTFE), lightweight and be not easy to break into pieces, durable in use, solves the trouble needing often to change gauze and yarn rope.
3. avoid the danger broken test tube when putting into large beaker because of carelessness into pieces and solution is spilt, ensure the security of test tube.
4., in autoclave or pressure cooker, this rack for test tube Absorbable organic halogens ground superposition is placed, and is applicable to the situation that water sample is more.
5. except clearing up for nitrogen phosphorus, this rack for test tube also can be used for the placement of test tube in other experiment, and the rack for test tube of comparable routine holds more test tube and is convenient to sample and shakes up.
Accompanying drawing explanation
Fig. 1 is the perspective view of the utility model rack for test tube;
Fig. 2 is the stereochemical structure upward view of Fig. 1;
Fig. 3 is the perspective view of rack for test tube mounting plate;
Fig. 4 is the stereochemical structure top view of rack for test tube mounting plate;
Fig. 5 is the arrays of openings schematic diagram of bottom plate in embodiment.
The utility model Reference numeral is as follows:
1---base plate 2---bottom plate
3---mounting plate 4---pillar
5---portion 6 of giving a hand---groove
7---through hole 8---blocks a shot
9---knob screw 10---pillar hole
11---screw
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the utility model is described further.
The rack for test tube cleared up for nitrogen phosphorus of the present utility model adopts the high-temperature resistance plastices such as acrylic resin (PP), polytetrafluoroethylene (PTFE) (PTFE) to be prepared.
As shown in accompanying drawing 1, Fig. 2, rack for test tube is disposed with base plate 1, bottom plate 2 and mounting plate 3 from the bottom to top, described base plate 1, bottom plate 2 and mounting plate 3 is circular configuration, be provided with 4 pillars 4 evenly, symmetrically at the circular edge place of base plate 1, base plate 1 and bottom plate 2 form an entirety by 4 pillars 4; Base plate 1 is provided with circular groove 6 uniform sequentially, and groove 6 matches with the bottom of test tube; Bottom plate 2 is provided with and groove 6 through hole 7 one to one, through hole 7 and groove 6 are positioned on same vertical axis, test tube is placed in groove 6 through through hole 7, and the diameter of groove 6 is more than or equal to the diameter bottom test tube, and the diameter of through hole 7 is consistent with the diameter of groove 6; 2 portions 5 of giving a hand are provided with, in order to steadily to hold rack for test tube above bottom plate 2, on two symmetrical pillars 4; 2 surfaces, portion 5 of giving a hand are provided with annular knurl, the shape that portion 5 of giving a hand is recessed in middle convex two ends, match with the palm of experimenter; As shown in accompanying drawing 3, Fig. 4, mounting plate 3 is provided with pillar hole 10 with the correspondence position of pillar 4, pillar hole 10 is provided with screw 11 with the upright position of mounting plate 3 sidewall, knob screw 9 is provided with in screw 11, pillar 4 passes the pillar hole 10 of mounting plate 3 and knob screw 9 passes screw 11 and mounting plate 3 fixes, and knob screw 9 makes mounting plate 3 dismantle and can regulate its height.Position corresponding with through hole 7 below mounting plate 3 is provided with block 8, and block 8 and through hole 7 are positioned on same vertical axis, and block 8 adapts with the top of test tube, and the diameter of block 8 is more than or equal to the diameter of test tube mouth, is highly 2cm.
The whole height of rack for test tube is 23cm, and diameter is 20cm, and the thickness of base plate 1 is 1cm, the thickness of bottom plate 2 and mounting plate 3 is 0.5cm, and the diameter of pillar 4 is 1cm; Rack for test tube can place 19 test tubes simultaneously.
Through hole in the bottom plate 2 of the present embodiment arranges by rule below:
See Fig. 5, middle 1 through hole in bottom plate 2 and bottom plate 2 are concentric circles, and the spaced 60 degree of angles of through hole in intermediate layer are evenly distributed, amount to 6, the spaced 30 degree of angles of outermost layer through hole are evenly distributed, amount to 12, so whole rack for test tube arranges through hole 19 altogether.The Edge Distance of outermost layer through hole and bottom plate 2 is 1cm.
The quantity of concrete size and holding test tubes can adjust according to actual needs above.
Mounting plate 3 in use, is first dismantled by the rack for test tube cleared up for nitrogen phosphorus of the present utility model, and by the lower end of test tube through being against in the groove 6 of base plate 1 after the through hole 7 of bottom plate 2, test tube is that vertical state is placed on rack for test tube.After in vitro adding water sample and medicament, cover glass stopper, by pillar hole 10, mounting plate 3 is penetrated pillar 4, and regulate the height of mounting plate 3 by the knob screw 9 in screw 11, then tighten knob screw 9, make block 8 press test tube.Experimenter holds portion 5 of giving a hand and lifts rack for test tube, rack for test tube is turned upside down, shake up water sample, again knob screw 9 is unscrewed, mounting plate 3 is improved 0.5-1cm, tighten knob screw 9 again, to prevent, digestion process pilot scale overpressure is excessive blasts, and finally puts into autoclave or pressure cooker is cleared up.
Rack for test tube of the present utility model also can be used for the placement of test tube in other experiment.

Claims (8)

1. the rack for test tube cleared up for nitrogen phosphorus, comprise pillar, base plate, bottom plate, mounting plate, knob screw, it is characterized in that, rack for test tube is disposed with base plate (1), bottom plate (2) and mounting plate (3) from the bottom to top, described base plate (1), bottom plate (2) and mounting plate (3) are circular configuration, be provided with pillar (4) evenly, symmetrically at the circular edge place of base plate (1), base plate (1) and bottom plate (2) form an entirety by pillar (4); Base plate (1) is upper is provided with circular groove (6) uniform sequentially, and groove (6) matches with the bottom of test tube; Bottom plate (2) is provided with and groove (6) through hole (7) one to one, through hole (7) and groove (6) are positioned on same vertical axis, and test tube is placed in groove (6) through through hole (7); Mounting plate (3) is provided with pillar hole (10) with the correspondence position of pillar (4), pillar hole (10) is provided with screw (11) with the upright position of mounting plate (3) sidewall, knob screw (9) is provided with in screw (11), pillar (4) through the pillar hole (10) of mounting plate (3) and knob screw (9) fix through screw (11) and mounting plate (3), knob screw (9) makes mounting plate (3) can dismantle and can regulate its height; Position corresponding with through hole (7) below mounting plate (3) is provided with block a shot (8), block (8) and through hole (7) are positioned on same vertical axis, and block (8) adapts with the top of test tube.
2. the rack for test tube cleared up for nitrogen phosphorus according to claim 1, is characterized in that, described pillar (4) is 4; The top, two symmetrical pillars (4) of bottom plate (2) are provided with 2 portions of giving a hand (5), in order to steadily to hold rack for test tube.
3. the rack for test tube cleared up for nitrogen phosphorus according to claim 2, is characterized in that, 2 described portion of giving a hand (5) surfaces are provided with annular knurl, the shape that portion of giving a hand (5) are recessed in middle convex two ends, match with the palm of experimenter.
4. the rack for test tube cleared up for nitrogen phosphorus according to claim 1, is characterized in that, the diameter of described groove (6) is more than or equal to the diameter bottom test tube.
5. the rack for test tube cleared up for nitrogen phosphorus according to claim 1, is characterized in that, the diameter of described through hole (7) is consistent with the diameter of groove (6).
6. the rack for test tube cleared up for nitrogen phosphorus according to claim 1, is characterized in that, the diameter of described block (8) is more than or equal to the diameter of test tube mouth, is highly 1 ~ 2cm.
7. the rack for test tube cleared up for nitrogen phosphorus according to claim 1, is characterized in that, the whole height of this rack for test tube is 19 ~ 23cm, and diameter is 16 ~ 20cm.
8. the rack for test tube cleared up for nitrogen phosphorus according to claim 1, it is characterized in that, the thickness of this rack for test tube base plate (1) is 1cm, the thickness of bottom plate (2) and mounting plate (3) is 0.5cm, and the diameter of pillar (4) is 1cm.
CN201420777960.4U 2014-12-10 2014-12-10 For the rack for test tube that nitrogen phosphorus is cleared up Expired - Fee Related CN204412315U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420777960.4U CN204412315U (en) 2014-12-10 2014-12-10 For the rack for test tube that nitrogen phosphorus is cleared up

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420777960.4U CN204412315U (en) 2014-12-10 2014-12-10 For the rack for test tube that nitrogen phosphorus is cleared up

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Publication Number Publication Date
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104525290A (en) * 2014-12-10 2015-04-22 天津大学 Test tube rack for nitrogen and phosphorus digestion
CN108855289A (en) * 2017-05-09 2018-11-23 广州康昕瑞基因健康科技有限公司 loading tool
CN109358016A (en) * 2018-07-06 2019-02-19 湖南大学 A kind of method and apparatus of hand-held pressure pot combination colorimetric cylinder rapid-digestion measurement water body total nitrogen
CN112934290A (en) * 2021-05-14 2021-06-11 山东科技职业学院 Experimental equipment matched with digestion tube

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104525290A (en) * 2014-12-10 2015-04-22 天津大学 Test tube rack for nitrogen and phosphorus digestion
CN108855289A (en) * 2017-05-09 2018-11-23 广州康昕瑞基因健康科技有限公司 loading tool
CN109358016A (en) * 2018-07-06 2019-02-19 湖南大学 A kind of method and apparatus of hand-held pressure pot combination colorimetric cylinder rapid-digestion measurement water body total nitrogen
CN112934290A (en) * 2021-05-14 2021-06-11 山东科技职业学院 Experimental equipment matched with digestion tube
CN112934290B (en) * 2021-05-14 2021-10-12 山东科技职业学院 Experimental equipment matched with digestion tube

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150624

Termination date: 20161210