CN204395954U - The preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single - Google Patents
The preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single Download PDFInfo
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- CN204395954U CN204395954U CN201420874149.8U CN201420874149U CN204395954U CN 204395954 U CN204395954 U CN 204395954U CN 201420874149 U CN201420874149 U CN 201420874149U CN 204395954 U CN204395954 U CN 204395954U
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- reactor
- constant temperature
- oil bath
- measuring tank
- annular space
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Abstract
The utility model discloses the preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single.The top cover of reactor has the toluene solution of agitator and pentamethylcyclopentadiene base titanium trichloride (IV) add entrance, described in add entrance and be communicated with Feed metering device, described Feed metering device comprises measuring tank and microprocessor pump drive; Have annular space between described reactor wall and outer wall, described annular space is connected by pipeline with constant temperature oil bath; The bottom of described reactor is provided with material outlet and reactor frame.Effect is: in Kaolinite Preparation of Catalyst process, what adopt the toluene solution of measuring tank and microprocessor pump drive control pentamethylcyclopentadiene base titanium trichloride (IV) adds speed simultaneously, make that feed operation is simple, safety and environmental protection, inlet amount be accurate, and can also regulate the speed of charging and quantity according to demand; Because the bottom at reactor is provided with material outlet, operation is simple, safety and environmental protection to make feeding.
Description
Technical field
The utility model relates to petrochemical industry equipment technology field, particularly relates to the preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single.
Background technology
The luxuriant titanium complex catalyst of non-bridged single of nitrogen coordination belongs to the homogenous olefin polymerization catalyst of a new generation; its preparation process is normally carried out in the reactor; need nitrogen protection; and need the toluene solution of pentamethylcyclopentadiene base titanium trichloride (IV) slowly to join in reactor, react for a long time at a constant temperature with the lithium salts of secondary amine.In prior art, add toluene solution many employings manual methods of pentamethylcyclopentadiene base titanium trichloride (IV), when taking out product, also how material outlet not to be set in the bottom of reactor.When adding the toluene solution of pentamethylcyclopentadiene base titanium trichloride (IV) like this, not only measure inaccuracy, error is large, operating difficulties, and liquid charging stock is easily revealed, affect the healthy of operating personnel, expend time in length, when taking out product, also there is operating difficulties and liquid charging stock and the problem such as easily to reveal.
Utility model content
Technical problem to be solved in the utility model is: the deficiency existed for prior art, the preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single is provided, make that feed operation is simple, safety and environmental protection, inlet amount are accurate, and can also regulate the speed of charging and quantity according to demand, and operation is simple, safety and environmental protection to make feeding.
For solving the problems of the technologies described above, the technical solution of the utility model is:
A preparation facilities for the luxuriant titanium complex catalyst of non-bridged single, comprises reactor, constant temperature oil bath, measuring tank and microprocessor pump drive; The top cover of described reactor is fixed with agitator; The bottom of described reactor is provided with material outlet and reactor frame; Annular space is had between described reactor wall and outer wall, phenyl silicone oil is had in annular space between described reactor wall and outer wall, the outlet of described constant temperature oil bath connects the annular space medium inlet of described reactor by pipeline, the medium inlet of described constant temperature oil bath connects the annular space media outlet of described reactor by pipeline, described constant temperature oil bath provides applicable reaction temperature for described reactor; Described reactor is equipped with thermocouple, and described thermocouple is connected with described constant temperature oil bath by wire, monitors the temperature in described reactor; The top cover of described reactor is connected with nitrogen inlet pipeline and nitrogen outlet pipeline; The toluene solution that the top cover of described reactor is provided with pentamethylcyclopentadiene base titanium trichloride (IV) adds entrance, the toluene solution of described pentamethylcyclopentadiene base titanium trichloride (IV) adds entrance and is communicated with Feed metering device, described Feed metering device comprises measuring tank, material outlet is provided with bottom described measuring tank, described material outlet is communicated with valve and microprocessor pump drive, and described microprocessor pump drive adds entrance with the toluene solution of described pentamethylcyclopentadiene base titanium trichloride (IV) and is communicated with; Described measuring tank side is provided with liquid level metering device, and described liquid level metering device is linker, and described linker is provided with scale.
Owing to have employed technique scheme, the beneficial effects of the utility model are:
1. the preparation facilities of the utility model catalyst, preparing in the luxuriant titanium complex catalyst process of non-bridged single, what adopt the toluene solution of measuring tank and microprocessor pump drive control pentamethylcyclopentadiene base titanium trichloride (IV) adds speed simultaneously, make that feed operation is simple, safety and environmental protection, inlet amount be accurate, and can also regulate the speed of charging and quantity according to demand.
2. the preparation facilities of the utility model catalyst, because the bottom at reactor is provided with material outlet, operation is simple, safety and environmental protection to make feeding.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1. reactor, 2. agitator, 3. thermocouple, 4. constant temperature oil bath, 5. stirring motor, 6. valve, 7. microprocessor pump drive, 8. material outlet, 9. reactor frame, 10. measuring tank, 11. linkers, 12. scales.
Detailed description of the invention
Below in conjunction with drawings and Examples, the utility model is described in further detail.It should be noted that, these embodiments are mainly used in those skilled in the art to further understanding of the present utility model, and the utility model is not limited to these embodiments.
Embodiment 1:
Consult Fig. 1.A preparation facilities for the luxuriant titanium complex catalyst of non-bridged single, comprises the reactor (1) of 1000mL, constant temperature oil bath (4), the measuring tank (10) of 1000mL and microprocessor pump drive (7).The top cover of reactor (1) is fixed with agitator (2), the bottom of reactor (1) is provided with material outlet (8) and reactor frame (9).Reactor (1) has annular space between inwall and outer wall, phenyl silicone oil is had in annular space, the outlet of constant temperature oil bath (4) is by the annular space medium inlet of pipeline coupled reaction device (1), and the medium inlet of constant temperature oil bath (4) is by the annular space media outlet of pipeline coupled reaction device (1).What constant temperature oil bath (4) adopted is HH-SB digital display constant temperature oil bath (outer circulation).Reactor (1) is equipped with thermocouple (3), and thermocouple (3) is connected with constant temperature oil bath (4) by wire.The top cover of reactor (1) is connected with nitrogen inlet pipeline, the toluene solution of nitrogen outlet pipeline and pentamethylcyclopentadiene base titanium trichloride (IV) adds entrance, the toluene solution of described pentamethylcyclopentadiene base titanium trichloride (IV) adds entrance and is communicated with Feed metering device, described Feed metering device comprises measuring tank (10), described measuring tank (10) bottom is provided with material outlet, described material outlet is communicated with valve (6) and microprocessor pump drive (7), described microprocessor pump drive (7) adds entrance with the toluene solution of described pentamethylcyclopentadiene base titanium trichloride (IV) and is communicated with, measuring tank (10) side is provided with liquid level metering device, and described liquid level metering device is linker (11), and linker (11) is provided with scale (12).
Operation principle of the present utility model is: measuring tank (10) is provided with the linker (11) of (12) with a scale, be convenient to observe liquid level, first time metering is carried out to the toluene solution of pentamethylcyclopentadiene base titanium trichloride (IV).After measuring tank (10) charging, Open valve (6), by the toluene solution of pentamethylcyclopentadiene base titanium trichloride (IV) is transported to reactor (1) by microprocessor pump drive (7), react with the lithium salts of secondary amine in reactor (1), the toluene solution of microprocessor pump drive (7) to pentamethylcyclopentadiene base titanium trichloride (IV) carries out second time metering.Reactor (1) top cover is connected with nitrogen inlet pipeline and nitrogen outlet pipeline, provides nitrogen protection to reaction.Constant temperature oil bath (4) provides applicable reaction temperature for reactor (1).Agitator (2) fixing on reactor (1) top cover, stirs reactant mixture.After completion of the reaction, the material outlet (8) of reactor (1) bottom is used product to be taken out.
Claims (1)
1. the preparation facilities of the luxuriant titanium complex catalyst of non-bridged single, comprise reactor (1), constant temperature oil bath (4), measuring tank (10) and microprocessor pump drive (7), it is characterized in that: the top cover of described reactor (1) is fixed with agitator (2), the bottom of described reactor (1) is provided with material outlet (8) and reactor frame (9), described reactor (1) has annular space between inwall and outer wall, phenyl silicone oil is had in the annular space of described reactor (1) between inwall and outer wall, the outlet of described constant temperature oil bath (4) is by the annular space medium inlet of pipeline coupled reaction device (1), the medium inlet of described constant temperature oil bath (4) is by the annular space media outlet of pipeline coupled reaction device, and described constant temperature oil bath (4) provides applicable reaction temperature for reactor (1), described reactor (1) is equipped with thermocouple (3), and described thermocouple (3) is connected with described constant temperature oil bath (4) by wire, monitors the temperature in described reactor (1), the top cover of described reactor (1) is connected with nitrogen inlet pipeline and nitrogen outlet pipeline, the toluene solution that the top cover of described reactor (1) is provided with pentamethylcyclopentadiene base titanium trichloride (IV) adds entrance, the toluene solution of described pentamethylcyclopentadiene base titanium trichloride (IV) adds entrance and is communicated with Feed metering device, described Feed metering device comprises measuring tank (10), described measuring tank (10) bottom is provided with material outlet, described material outlet is communicated with valve (6) and microprocessor pump drive (7), described microprocessor pump drive (7) adds entrance with the toluene solution of described pentamethylcyclopentadiene base titanium trichloride (IV) and is communicated with, described measuring tank (10) side is provided with liquid level metering device, and described liquid level metering device is linker (11), and described linker (11) is provided with scale (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420874149.8U CN204395954U (en) | 2014-12-26 | 2014-12-26 | The preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420874149.8U CN204395954U (en) | 2014-12-26 | 2014-12-26 | The preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204395954U true CN204395954U (en) | 2015-06-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420874149.8U Expired - Fee Related CN204395954U (en) | 2014-12-26 | 2014-12-26 | The preparation facilities of the luxuriant titanium complex catalyst of a kind of non-bridged single |
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| CN (1) | CN204395954U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104925926A (en) * | 2015-06-26 | 2015-09-23 | 开平市开物化工建材有限公司 | Novel polymeric aluminum ferric sulphate parparing and curing device |
-
2014
- 2014-12-26 CN CN201420874149.8U patent/CN204395954U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104925926A (en) * | 2015-06-26 | 2015-09-23 | 开平市开物化工建材有限公司 | Novel polymeric aluminum ferric sulphate parparing and curing device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150617 Termination date: 20171226 |