CN204365484U - A kind of grading plant of superfine powder - Google Patents
A kind of grading plant of superfine powder Download PDFInfo
- Publication number
- CN204365484U CN204365484U CN201420804790.4U CN201420804790U CN204365484U CN 204365484 U CN204365484 U CN 204365484U CN 201420804790 U CN201420804790 U CN 201420804790U CN 204365484 U CN204365484 U CN 204365484U
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- China
- Prior art keywords
- supercentrifuge
- classification
- measuring pump
- superfine powder
- stirred tank
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- 239000000843 powder Substances 0.000 title claims abstract description 34
- 238000007599 discharging Methods 0.000 claims abstract description 10
- 238000000703 high-speed centrifugation Methods 0.000 claims abstract description 6
- 229910001220 stainless steel Inorganic materials 0.000 claims abstract description 5
- 239000010935 stainless steel Substances 0.000 claims abstract description 5
- 239000002002 slurry Substances 0.000 abstract description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 19
- 238000000034 method Methods 0.000 description 8
- 238000009826 distribution Methods 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005194 fractionation Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013590 bulk material Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000010332 dry classification Methods 0.000 description 1
- 230000005684 electric field Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 229910052755 nonmetal Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000006722 reduction reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000010333 wet classification Methods 0.000 description 1
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- Centrifugal Separators (AREA)
- Separation Of Solids By Using Liquids Or Pneumatic Power (AREA)
Abstract
The utility model discloses a kind of grading plant of superfine powder, it is characterized in that: comprise stirred tank, the shaft be arranged in stirred tank, measuring pump, supercentrifuge and collection still, described measuring pump charging aperture is connected with bottom stirred tank by PU pipe, measuring pump discharging opening is connected with high speed centrifugation machine inlet capable by PU pipe, and supercentrifuge discharging opening is connected with collection still by stainless steel flexible hose.The utility model adopts supercentrifuge to carry out classification to superfine powder slurry, not only simple to operate, classification efficiency is high but also product after classification is pollution-free, fully ensure that the quality stability of classification powder.
Description
Technical field
The utility model relates to superfine powder preparation field, is specifically related to a kind of grading plant of superfine powder.
Background technology
Superfine powder refers to that yardstick is between molecule, and between atom and bulk material, micron and nano level minute solid particles, comprise metal, the multiple material particle such as nonmetal, organic and inorganic and biological.Superfine powder and densified be one of study hotspot of Material Field, compared with conventional material, superfine powder has the physics of a series of excellence, chemistry and surface and interface character.
At present, the stage division of superfine powder has been reported, and the state according to point stage material can be divided into dry classification, wet classification and supercritical fractionation.According to the difference in the classification field of force, gravitational field classification, centrifugal force field classification, inertial force field classification, electric field force classification, magnetic field force classification, the classification of the thermal gradient field of force and chromatographic fractionation etc. can be divided into again.According to the different qualities of superfine powder, the various suitable field of force is utilized to carry out effective classification to superfine powder, to obtain the raw material of different-grain diameter.But existing stage division cannot realize continuous operations mostly, and before carrying out classification to superfine powder, the superfine powder synthesized by chemical reduction method is all needed through following process process such as super-dries, very easily agglomeration occurs, and is unfavorable for classification.
Utility model content
The utility model, for the deficiency proposed in background technology, provides one effectively can carry out classification to superfine powder, enables superfine powder reach the device of required each type product.
Technical solution of the present utility model:
A kind of grading plant of superfine powder, it is characterized in that: comprise stirred tank, the shaft be arranged in stirred tank, measuring pump, supercentrifuge and collection still, described measuring pump charging aperture is connected with bottom stirred tank by PU pipe, measuring pump discharging opening is connected with high speed centrifugation machine inlet capable by PU pipe, and supercentrifuge discharging opening is connected with collection still by stainless steel flexible hose.
Described shaft is connected with motor.
Described supercentrifuge is tubular-bowl centrifuge.
The beneficial effects of the utility model: the utility model adopts supercentrifuge to carry out classification to superfine powder slurry, not only simple to operate, classification efficiency is high but also product after classification is pollution-free, fully ensure that the quality stability of classification powder.
Accompanying drawing explanation
Fig. 1 is powder classification device structural representation in the utility model.
1-stirred tank, 2-shaft, 3-measuring pump, 3-1 measuring pump charging aperture, 3-2 measuring pump discharging opening, 4-supercentrifuge, 4-1 high speed centrifugation machine inlet capable, 4-2 supercentrifuge discharging opening, 5-collect still, 6-PU pipeline, 7-motor, 8-stainless steel soft pipeline.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing, the utility model is described further.
A kind of grading plant of superfine powder, comprise stirred tank 1, the shaft 2 be arranged in stirred tank 1, measuring pump 3, supercentrifuge 4 and collect still 5, measuring pump charging aperture 3-1 is connected with bottom stirred tank 1 by PU pipe 6, measuring pump discharging opening 3-2 is connected with high speed centrifugation machine inlet capable 4-1 by PU pipe 6, supercentrifuge discharging opening 4-2 is connected with collection still 5 by stainless steel flexible hose 8, shaft 2 is connected with motor 7, and supercentrifuge 4 is tubular-bowl centrifuge.
Specific operation process: a collection of 100kg is made into the not classified extra-fine nickel powder (300nm) after slurry, is divided into 2 batches, every batch of 50kg high speed centrifugation classification process.
Embodiment 1 (batch one)
(1) starter motor, shaft starts to rotate, and is added in stirred tank by extra-fine nickel powder slurry 50kg and stirs;
(2) start supercentrifuge, after the rotating speed of supercentrifuge reaches 15000 revs/min, start measuring pump and start charging;
(3) extra-fine nickel powder slurry enters supercentrifuge classification through measuring pump, and overflow enters from supercentrifuge outlet flow source and collects still, collects nickel powder 36.48kg;
(4), after classification terminates, the powder on cleaning supercentrifuge rotary drum is gone forward side by side collection, collects the nickel powder 13.47kg on rotary drum.
Embodiment 2(batches two)
(1) starter motor, shaft starts to rotate, and is added in stirred tank by extra-fine nickel powder slurry 50kg and stirs;
(2) start supercentrifuge, after the rotating speed of supercentrifuge reaches 15000 revs/min, start measuring pump and start charging;
(3) extra-fine nickel powder slurry enters supercentrifuge classification through measuring pump, and overflow enters from supercentrifuge outlet flow source and collects still, collects nickel powder 37.25kg;
(4), after classification terminates, the powder on cleaning supercentrifuge rotary drum is gone forward side by side collection, collects the nickel powder 12.69kg on rotary drum.
Grain size analysis test is carried out to the original nickel powder of the overflow nickel powder in embodiment 1 and embodiment 2, the nickel powder on rotatory drum wall and not classified process and BET detects, its result respectively as shown in Table 1 and Table 2:
The Laser particle-size distribution test result of table 1 powder
The BET testing result of table 2 powder
As can be seen from Table 1 and Table 2, the extra-fine nickel powder that the extra-fine nickel powder collected through centrifuge outlet overflows, rotatory drum wall are collected is compared with the original nickel powder of not classified process, the former powder of not classified process is not due to through dispersed with stirring, intergranular often soft-agglomerated, add that itself particle size distribution is comparatively wide, so Laser particle-size distribution detection numerical value is larger; Extra-fine nickel powder overflow portion is made up of the particle diameter smaller portions in former powder, and obtains good dispersion, thus its Laser particle-size distribution and droplet measurement numerical value all little than the numerical value of former powder; The extra-fine nickel powder that rotatory drum wall is collected is made up of particle diameter major part in former powder, and Laser particle-size distribution and droplet measurement numerical value are all greater than the numerical value of former powder.
adopt the extra-fine nickel powder grading effect of the utility model device classification obvious, the dispersity of nickel powder of overflow is good.
To sum up, the utility model produces a desired effect.
Claims (3)
1. the grading plant of a superfine powder, it is characterized in that: comprise stirred tank, the shaft be arranged in stirred tank, measuring pump, supercentrifuge and collection still, described measuring pump charging aperture is connected with bottom stirred tank by PU pipe, measuring pump discharging opening is connected with high speed centrifugation machine inlet capable by PU pipe, and supercentrifuge discharging opening is connected with collection still by stainless steel flexible hose.
2. the grading plant of a kind of superfine powder as claimed in claim 1, is characterized in that: described shaft is connected with motor.
3. the grading plant of a kind of superfine powder as claimed in claim 1, is characterized in that: described supercentrifuge is tubular-bowl centrifuge.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201420804790.4U CN204365484U (en) | 2014-12-18 | 2014-12-18 | A kind of grading plant of superfine powder |
Applications Claiming Priority (1)
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CN201420804790.4U CN204365484U (en) | 2014-12-18 | 2014-12-18 | A kind of grading plant of superfine powder |
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CN204365484U true CN204365484U (en) | 2015-06-03 |
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CN201420804790.4U Active CN204365484U (en) | 2014-12-18 | 2014-12-18 | A kind of grading plant of superfine powder |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104475239A (en) * | 2014-12-18 | 2015-04-01 | 江苏博迁新材料有限公司 | Grading device and grading method for ultra-fine powder |
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2014
- 2014-12-18 CN CN201420804790.4U patent/CN204365484U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104475239A (en) * | 2014-12-18 | 2015-04-01 | 江苏博迁新材料有限公司 | Grading device and grading method for ultra-fine powder |
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GR01 | Patent grant | ||
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CP03 | Change of name, title or address |
Address after: 223800 Suqian province high tech Development Zone, Jiangshan Road, No. 23, No. Patentee after: Jiangsu Bo move new materials Limited by Share Ltd Address before: 223800 Huashan Road, Suyu Economic Development Zone, Jiangsu, No. 109, No. Patentee before: Jiangsu Boqian New Materials Co., Ltd. |