CN204364930U - Electric supersonic crystallization tank - Google Patents
Electric supersonic crystallization tank Download PDFInfo
- Publication number
- CN204364930U CN204364930U CN201420861388.XU CN201420861388U CN204364930U CN 204364930 U CN204364930 U CN 204364930U CN 201420861388 U CN201420861388 U CN 201420861388U CN 204364930 U CN204364930 U CN 204364930U
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- Prior art keywords
- crystallization
- cell body
- crystallization tank
- seal cover
- ultrasonic wave
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Abstract
The utility model discloses a kind of electric supersonic crystallization tank, crystallization tank is columniform cell body, the top of cell body is provided with seal cover, the bottom of cell body is provided with leakage fluid dram, columniform crystallization screen cloth is fixedly connected with below seal cover, the external surface area of crystallization screen cloth is identical with the internal surface area of cell body, seal cover is provided with dog-house, the outside of cell body is provided with the ultrasonic wave emission layer of annular, the side of ultrasonic wave emission layer is provided with supersonic generator, and ultrasonic wave emission layer is fixedly mounted on the top of leakage fluid dram; The utility model passes through crystallization tank cell body and the crystallization screening web frame of coupling mutually, after crystallization operation completes, the lock out operation of solute and solution can be carried out in crystallization tank, avoid the impact of temperature change on solute solubility, material simultaneously in order to prevent crystallization screening online remains, by ultrasonic generator and auxiliary paddle auxiliary separating from, good separating effect, improves the operating efficiency of lock out operation.
Description
Technical field
The utility model relates to the chemical purification apparatus field of teaching, particularly relates to one conveniently electric supersonic crystallization tank.
Background technology
In chemistry the inside, after the saturated solution cooling of heat, solute is separated out with the form of crystal, and this process is crystallization.Crystallization is as one of the main method of laboratory isolation andpurification material.
In operation, first need to be dissolved completely in by solute in the solvent after heating, then cooled by solution, in cooling procedure, solute is constantly separated out from solvent, after solute is separated out completely, itself and solution is separated by filter operation; Operate relatively loaded down with trivial details, in particularly filter operation process, filter paper and filter plant can remain a large amount of crystalline products, not easily collecting, simultaneously in filter process, the temperature of solution itself also can change, and then affects the solubility of solute, cause residual fraction solute in product waste liquid, further operation and extraction difficulty.
Utility model content
For above-mentioned Problems existing, the utility model object is to provide a kind of simple to operate, facilitates the electric supersonic crystallization tank that solute rapid crystallization is separated.
In order to achieve the above object, the technical solution adopted in the utility model is as follows: a kind of electric supersonic crystallization tank, described crystallization tank is columniform cell body, the top of described cell body is provided with seal cover, the bottom of described cell body is provided with leakage fluid dram, columniform crystallization screen cloth is fixedly connected with below described seal cover, the external surface area of described crystallization screen cloth is identical with the internal surface area of cell body, described seal cover is provided with dog-house, the outside of described cell body is provided with the ultrasonic wave emission layer of annular, the side of described ultrasonic wave emission layer is provided with supersonic generator, described ultrasonic wave emission layer is fixedly mounted on the top of leakage fluid dram.
Improve as one of the present utility model, described dog-house is provided with the auxiliary groove that feeds intake, and the bottom of the described auxiliary groove that feeds intake is provided with the filter screen of taper; Drop into heated solution in crystallization tank by the filter screen screening of the auxiliary trench bottom that feeds intake, impurity not consoluet in solution or other solid particles are separated, prevents it on the impact of final crystalline product purity.
Improve as one of the present utility model, auxiliary paddle is provided with below described seal cover, described auxiliary paddle is provided with positioning through hole, is provided with backstay in described positioning through hole, and described auxiliary paddle is fixedly connected on seal cover by backstay.The top of described auxiliary paddle is provided with thread groove, is connected with lengthening shaft in described thread groove; By the crystalline solid in the artificial stirred crystallization groove of auxiliary paddle and solution, by the mode of ultrasonic wave and physical agitation, the solid being sticky in crystallization screening online is scraped down, convenient collection; Simultaneously in crystallization process, auxiliary paddle is accommodated on seal cover, does not affect normal crystallization operation in crystallization tank, simple to operation, improves the operating efficiency of the operation of device Crystallization Separation.
Improve as one of the present utility model, the bottom of described cell body is provided with yielding rubber base; Because supersonic generator can produce certain vibration in the course of the work, in order to the stability of assurance device, anti-locking apparatus slides on the table, and the bottom of cell body is fixedly connected with desktop by yielding rubber base.
The utility model has the advantage of: the utility model passes through crystallization tank cell body and the crystallization screening web frame of coupling mutually, after crystallization operation completes, the lock out operation of solute and solution can be carried out in crystallization tank, avoid the impact of temperature change on solute solubility, material simultaneously in order to prevent crystallization screening online remains, by ultrasonic generator and auxiliary paddle auxiliary separating from, avoid the online material of crystallization screening largely to remain, avoid unnecessary material loss, improve the rate of recovery of crystalline product, simple to operation; Solute and separated from solvent effective, improve the operating efficiency of lock out operation.
Accompanying drawing explanation
Fig. 1 is the utility model structure diagram;
Fig. 2 is the utility model ultrasonic wave emission layer plan structure sketch;
Wherein, 1 cell body, 2 seal covers, 3 crystallization screen clothes, 4 dog-houses, 5 leakage fluid drams, 6 ultrasonic wave emission layers, 7 supersonic generators, the 8 auxiliary grooves that feed intake, 9 filter screens, 10 auxiliary paddles, 11 positioning through hole, 12 backstays, 13 thread grooves, 14 yielding rubber bases.
Detailed description of the invention
Illustrate below in conjunction with accompanying drawing and with detailed description of the invention, the utility model to be described in further detail.
embodiment 1:a kind of electric supersonic crystallization tank as illustrated in fig. 1 and 2, described crystallization tank is columniform cell body 1, the top of described cell body 1 is provided with seal cover 2, the bottom of described cell body 1 is provided with leakage fluid dram 5, columniform crystallization screen cloth 3 is fixedly connected with below described seal cover 2, the external surface area of described crystallization screen cloth 3 is identical with the internal surface area of cell body 1, described seal cover 2 is provided with dog-house 4, the outside of described cell body 1 is provided with the ultrasonic wave emission layer 6 of annular, the side of described ultrasonic wave emission layer 6 is provided with supersonic generator 7, described ultrasonic wave emission layer 6 is fixedly mounted on the top of the leakage fluid dram 5 of cell body 1.
embodiment 2:as shown in Figure 1, described dog-house 4 is provided with the auxiliary groove 8 that feeds intake, and the described auxiliary bottom feeding intake groove 8 is provided with the filter screen 9 of taper; Screened by the filter screen 9 bottom the auxiliary groove 8 that feeds intake and drop into heated solution in crystallization tank 1, impurity not consoluet in solution or other solid particles are separated, prevents it on the impact of final crystalline product purity.
embodiment 3:as shown in Figure 1, auxiliary paddle 10 is provided with below described seal cover 2, described auxiliary paddle 10 is provided with positioning through hole 11, is provided with backstay 12 in described positioning through hole 11, and described auxiliary paddle 10 is fixedly connected on seal cover 2 by backstay 12.The top of described auxiliary paddle 10 is provided with thread groove 13, is connected with lengthening shaft in described thread groove 13; By the crystalline solid in the artificial stirred crystallization groove 1 of auxiliary paddle 10 and solution, by the mode of ultrasonic wave and physical agitation, the solid be sticky on crystallization screen cloth 3 is scraped down, convenient collection; Simultaneously in crystallization process, auxiliary paddle 10 is accommodated on seal cover 2, does not affect normal crystallization operation in crystallization tank 1, simple to operation, improves the operating efficiency of the operation of device Crystallization Separation.
embodiment 4:as illustrated in fig. 1 and 2, the bottom of described cell body 1 is provided with yielding rubber base 14; Because supersonic generator can produce certain vibration in the course of the work, in order to the stability of assurance device, anti-locking apparatus slides on the table, and the bottom of cell body 1 is fixedly connected with desktop by yielding rubber base 14.
It should be noted that, above-mentioned is only preferred embodiment of the present utility model, is not used for limiting protection domain of the present utility model, and equivalents done on the basis of above-described embodiment all belongs to protection domain of the present utility model.
Claims (5)
1. an electric supersonic crystallization tank, described crystallization tank is columniform cell body, the top of described cell body is provided with seal cover, the bottom of described cell body is provided with leakage fluid dram, it is characterized in that, columniform crystallization screen cloth is fixedly connected with below described seal cover, the external surface area of described crystallization screen cloth is identical with the internal surface area of cell body, described seal cover is provided with dog-house, the outside of described cell body is provided with the ultrasonic wave emission layer of annular, the side of described ultrasonic wave emission layer is provided with supersonic generator, described ultrasonic wave emission layer is fixedly mounted on the top of leakage fluid dram.
2. electric supersonic crystallization tank as claimed in claim 1, is characterized in that, described dog-house is provided with the auxiliary groove that feeds intake, and the bottom of the described auxiliary groove that feeds intake is provided with the filter screen of taper.
3. electric supersonic crystallization tank as claimed in claim 1, it is characterized in that, auxiliary paddle is provided with below described seal cover, described auxiliary paddle is provided with positioning through hole, be provided with backstay in described positioning through hole, described auxiliary paddle is fixedly connected on seal cover by backstay.
4. electric supersonic crystallization tank as claimed in claim 3, it is characterized in that, the top of described auxiliary paddle is provided with thread groove, is connected with lengthening shaft in described thread groove.
5. electric supersonic crystallization tank as claimed in claim 1, it is characterized in that, the bottom of described cell body is provided with yielding rubber base.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420861388.XU CN204364930U (en) | 2014-12-31 | 2014-12-31 | Electric supersonic crystallization tank |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420861388.XU CN204364930U (en) | 2014-12-31 | 2014-12-31 | Electric supersonic crystallization tank |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204364930U true CN204364930U (en) | 2015-06-03 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420861388.XU Expired - Fee Related CN204364930U (en) | 2014-12-31 | 2014-12-31 | Electric supersonic crystallization tank |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204364930U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110354777A (en) * | 2019-07-31 | 2019-10-22 | 河北兰升生物科技有限公司 | Reaction unit of a kind of ultrasonic wave added crystallization and application thereof and preparation method using the device |
| CN110812937A (en) * | 2019-11-07 | 2020-02-21 | 徐州鑫泰镀锌设备有限公司 | Microwave waste acid deironing device of galvanizing production |
| CN112758969A (en) * | 2020-12-31 | 2021-05-07 | 宜昌华昊新材料科技有限公司 | Process for producing electronic grade barium hydroxide by recycling high-purity barium chloride mother liquor |
-
2014
- 2014-12-31 CN CN201420861388.XU patent/CN204364930U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110354777A (en) * | 2019-07-31 | 2019-10-22 | 河北兰升生物科技有限公司 | Reaction unit of a kind of ultrasonic wave added crystallization and application thereof and preparation method using the device |
| CN110354777B (en) * | 2019-07-31 | 2024-03-12 | 兰升生物科技集团股份有限公司 | Method for preparing cis-para-substituted cyclohexylamino nitrile maleate by using reaction device of ultrasonic-assisted crystallization |
| CN110812937A (en) * | 2019-11-07 | 2020-02-21 | 徐州鑫泰镀锌设备有限公司 | Microwave waste acid deironing device of galvanizing production |
| CN112758969A (en) * | 2020-12-31 | 2021-05-07 | 宜昌华昊新材料科技有限公司 | Process for producing electronic grade barium hydroxide by recycling high-purity barium chloride mother liquor |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150603 Termination date: 20161231 |
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| CF01 | Termination of patent right due to non-payment of annual fee |