CN204347625U - Organic Experiment many consersion units coupling nitrogen constant flow environment control unit - Google Patents

Organic Experiment many consersion units coupling nitrogen constant flow environment control unit Download PDF

Info

Publication number
CN204347625U
CN204347625U CN201420856134.9U CN201420856134U CN204347625U CN 204347625 U CN204347625 U CN 204347625U CN 201420856134 U CN201420856134 U CN 201420856134U CN 204347625 U CN204347625 U CN 204347625U
Authority
CN
China
Prior art keywords
nitrogen
comb
entrance
reaction system
tubes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420856134.9U
Other languages
Chinese (zh)
Inventor
章结兵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xian University of Science and Technology
Original Assignee
Xian University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xian University of Science and Technology filed Critical Xian University of Science and Technology
Priority to CN201420856134.9U priority Critical patent/CN204347625U/en
Application granted granted Critical
Publication of CN204347625U publication Critical patent/CN204347625U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Sampling And Sample Adjustment (AREA)

Abstract

The utility model discloses a kind of Organic Experiment many consersion units coupling nitrogen constant flow environment control unit, comprise single row of tubes, flowmeter, rubber finger sleeve and beaker, described single row of tubes one end connection traffic meter, described flowmeter one end is connected with gas cylinder connector, described gas cylinder connector is provided with piston, in described single row of tubes, side is provided with the entrance that nitrogen in comb enters reaction system, opposite side is provided with nitrogen enters comb entrance from reaction system, in described comb, nitrogen enters the entrance of reaction system and nitrogen and enters between the entrance of comb from reaction system and be provided with sealed jacket, airtight in the middle of turnover comb, not circulated gases, described sealed jacket is arranged in described single row of tubes, the described single row of tubes other end is connected with rubber finger sleeve, described rubber finger sleeve one end is inserted in described beaker.The design of the utility model apparatus structure is unique, simple, uses easy to operate and low cost, is applicable to, in organic synthetic experiment teaching and scientific research laboratory, can be in large-scale application.

Description

Organic Experiment many consersion units coupling nitrogen constant flow environment control unit
Technical field
The utility model relates to experimental facilities, is specifically related to a kind of Organic Experiment many consersion units coupling nitrogen constant flow environment control unit.
Background technology
In organic synthesis process, scientific experiment is carried out for student experimenting or researchist, sometimes need under nitrogen protection environment, carry out experiment synthesis, much all that nitrogen in nitrogen cylinder is directly received in experimental provision in experimentation in the past, or protect with nitrogen bag release nitrogen, the maximum problem of these devices is exactly the flow that well can not control nitrogen, and then can not control nitrogen gas concn in experiment reaction environment, can not the change of good Control release reaction environment, even sometimes the waste of a large amount of nitrogen can also be caused, and this experimentation is all generally the single consersion unit of single cover nitrogen unit protection, efficiency is lower.
Utility model content
For solving the problem, the utility model provides a kind of Organic Experiment many consersion units coupling nitrogen constant flow environment control unit, and structural design is unique, simple, uses easy to operate and low cost, be applicable to, in organic synthetic experiment teaching and scientific research laboratory, can be in large-scale application.
For achieving the above object, the technical scheme that the utility model is taked is:
Organic Experiment many consersion units coupling nitrogen constant flow environment control unit, comprise single row of tubes, flowmeter, rubber finger sleeve and beaker, described single row of tubes one end connection traffic meter, described flowmeter one end is connected with gas cylinder connector, described gas cylinder connector is provided with piston, in described single row of tubes, side is provided with the entrance that nitrogen in comb enters reaction system, opposite side is provided with nitrogen enters comb entrance from reaction system, in described comb, nitrogen enters the entrance of reaction system and nitrogen and enters between the entrance of comb from reaction system and be provided with sealed jacket, airtight in the middle of turnover comb, not circulated gases, described sealed jacket is arranged in described single row of tubes, the described single row of tubes other end is connected with rubber finger sleeve, described rubber finger sleeve one end is inserted in described beaker, also comprise there-necked flask, described there-necked flask is provided with air intake opening and gas outlet, described air intake opening and gas outlet are all provided with rubber plug and hollow glass tube, the entrance that in described comb, nitrogen enters reaction system is connected with described air intake opening, described nitrogen enters comb entrance from reaction system is connected with described gas outlet.
As preferably, the entrance that described nitrogen enters reaction system is provided with glass piston switch.
As preferably, the entrance that described nitrogen enters comb from reaction system is provided with glass piston switch.
As preferably, the range of described flowmeter is 1-10L/h.
As preferably, in described beaker, be filled with water.
The utility model has following beneficial effect:
The utility model device is single row of tubes, constant flow design philosophy, and one-piece construction is simple, reasonable in design, and easy to use, and can meet many group identical experiment reaction environment conditional requests, conventional efficient improves greatly simultaneously; Taken into account the setting of the piston switch under flowmeter by flow, control gas flow accurately; Cost is low, easily manufactures, and not only can meet scientific research personnel's scientific research use, also can large-scale application apply in Organic Experiment teaching process.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: Fig. 1 a is the single row of tubes of Fig. 1 and the structural representation of beaker; Fig. 1 b is the structural representation of there-necked flask in Fig. 1.
Embodiment
In order to make the purpose of this utility model and advantage clearly understand, below in conjunction with embodiment, the utility model is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the utility model, and be not used in restriction the utility model.
As shown in Figure 1, the utility model embodiment provides a kind of Organic Experiment many consersion units coupling nitrogen constant flow environment control unit, comprises single row of tubes 13, flowmeter 9, rubber finger sleeve 11 and beaker 12, described single row of tubes 13 one end connection traffic meter 9, described flowmeter 9 one end is connected with gas cylinder connector 15, and described gas cylinder connector 15 is provided with piston 14, and in described single row of tubes 13, side is provided with the entrance 1 that nitrogen in comb enters reaction system, 2, 3, 4, opposite side is provided with nitrogen enters comb entrance 5 from reaction system, 6, 7, 8, in described comb, nitrogen enters the entrance of reaction system and nitrogen and enters between the entrance of comb from reaction system and be provided with sealed jacket 10, airtight in the middle of turnover comb, not circulated gases, described sealed jacket 10 is arranged in described single row of tubes 13, described single row of tubes 13 other end is connected with rubber finger sleeve 11, described rubber finger sleeve 11 one end is inserted in described beaker 12, also comprise there-necked flask 16, described there-necked flask 16 is provided with air intake opening and gas outlet, described air intake opening and gas outlet are all provided with rubber plug 17 and hollow glass tube 18, and in described comb, nitrogen enters the entrance 1 of reaction system, 2, 3, 4 are connected with described air intake opening, and described nitrogen enters the entrance 5 of comb from reaction system, 6, 7, 8 are connected with described gas outlet.
The entrance 1,2,3,4 that described nitrogen enters reaction system is provided with glass piston switch.
The entrance 5,6,7,8 that described nitrogen enters comb from reaction system is provided with glass piston switch.
The range of described flowmeter 9 is 1-10L/h.
Water is filled with in described beaker 12.
Wherein, the connection between the import and export of single row of tubes and the import and export of experimental provision is all connected and sealed with the emulsion tube of correspondingly-sized or rubber tube.
This concrete principle implemented is: in gas cylinder, in nitrogen or airbag, nitrogen enters single row of tubes from the lower end of flowmeter, nitrogen nitrogen from comb enters the entrance 1 of reaction system, 2, 3, 4 enter in the air intake opening (left mouth) of 4 different there-necked flasks respectively, gas is discharged from the gas outlet (right mouth) of there-necked flask, Exhaust Gas enters the entrance 5 of comb from reaction system respectively by nitrogen, 6, 7, the interface of 8 enters in comb again, the emulsion tube 11 connected from comb enters the beaker 12 of dress water, when in beaker, bubbles volume is larger, adjust flux meter lower end piston makes bubble flow amount diminish, otherwise, adjust flux meter lower end piston makes bubble flow quantitative change large, experimentally need the bubble regulated arbitrarily by adjust flux meter lower end piston in beaker, and then the concentration of blanket gas nitrogen in control reactor, reach final and control reaction blanket gas environment.
The above is only preferred implementation of the present utility model; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the utility model principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection domain of the present utility model.

Claims (5)

1. Organic Experiment many consersion units coupling nitrogen constant flow environment control unit, it is characterized in that, comprise single row of tubes (13), flowmeter (9), rubber finger sleeve (11) and beaker (12), described single row of tubes (13) one end connection traffic meter (9), described flowmeter (9) one end is connected with gas cylinder connector (15), described gas cylinder connector (15) is provided with piston (14), the upper side of described single row of tubes (13) is provided with the entrance (1 that nitrogen in comb enters reaction system, 2, 3, 4), opposite side is provided with nitrogen enters comb entrance (5 from reaction system, 6, 7, 8), in described comb, nitrogen enters the entrance of reaction system and nitrogen and enters between the entrance of comb from reaction system and be provided with sealed jacket (10), described sealed jacket (10) is arranged in described single row of tubes (13), described single row of tubes (13) other end is connected with rubber finger sleeve (11), described rubber finger sleeve (11) one end is inserted in described beaker (12), also comprise there-necked flask (16), described there-necked flask (16) is provided with air intake opening and gas outlet, described air intake opening and gas outlet are all provided with rubber plug (17) and hollow glass tube (18), in described comb, nitrogen enters the entrance (1 of reaction system, 2, 3, 4) be connected with described air intake opening, described nitrogen enters the entrance (5 of comb from reaction system, 6, 7, 8) be connected with described gas outlet.
2. Organic Experiment many consersion units coupling nitrogen constant flow environment control unit according to claim 1, it is characterized in that, the entrance (1,2,3,4) that described nitrogen enters reaction system is provided with glass piston switch.
3. Organic Experiment many consersion units coupling nitrogen constant flow environment control unit according to claim 1, it is characterized in that, the entrance (5,6,7,8) that described nitrogen enters comb from reaction system is provided with glass piston switch.
4. Organic Experiment many consersion units coupling nitrogen constant flow environment control unit according to claim 1, it is characterized in that, the range of described flowmeter (9) is 1-10L/h.
5. Organic Experiment many consersion units coupling nitrogen constant flow environment control unit according to claim 1, it is characterized in that, described beaker is filled with water in (12).
CN201420856134.9U 2014-12-25 2014-12-25 Organic Experiment many consersion units coupling nitrogen constant flow environment control unit Expired - Fee Related CN204347625U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420856134.9U CN204347625U (en) 2014-12-25 2014-12-25 Organic Experiment many consersion units coupling nitrogen constant flow environment control unit

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420856134.9U CN204347625U (en) 2014-12-25 2014-12-25 Organic Experiment many consersion units coupling nitrogen constant flow environment control unit

Publications (1)

Publication Number Publication Date
CN204347625U true CN204347625U (en) 2015-05-20

Family

ID=53230883

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201420856134.9U Expired - Fee Related CN204347625U (en) 2014-12-25 2014-12-25 Organic Experiment many consersion units coupling nitrogen constant flow environment control unit

Country Status (1)

Country Link
CN (1) CN204347625U (en)

Similar Documents

Publication Publication Date Title
CN204347625U (en) Organic Experiment many consersion units coupling nitrogen constant flow environment control unit
CN202638453U (en) Gas collecting and metering device
CN205300996U (en) Vacuum pressure pollutes water sample collection system
CN203673734U (en) Environment-friendly type demonstration apparatus for experiment of reducing copper oxide with carbon monoxide
CN203648377U (en) Impinging stream reaction tower for flue gas desulfurization and dust removal
CN203342642U (en) Fermentation exhaust-gas treatment device
CN102855787A (en) Experiment teaching simulation system
CN202849385U (en) Device for safely and quantitatively collecting and purifying bio-methane in laboratory
CN203123735U (en) Novel tail gas treatment environment-friendly equipment
CN204380712U (en) A kind of Organic Experiment biexhaust pipe device
CN203786991U (en) Oxygen, carbon dioxide and hydrogen preparation and property verification device
CN104163429B (en) Carbon monoxide generator with a scale
CN202725210U (en) Gas collecting device
CN104873296A (en) Operating method for up-and-down type carbon monoxide poisoning device through filtration
CN203159611U (en) Shake flask facilitating sampling
CN203812478U (en) Reaction of concentrated nitric acid and dilute nitric acid with copper demonstration device
CN204718420U (en) Flue dust cooling-sedimentation system
CN203929560U (en) A kind of improved Catalytic Decomposition of Hydrogen Peroxide reaction rate determination experiment device
CN203706549U (en) NO experimental device
CN202996153U (en) Dry chlorine and moist chlorine bleaching property contrast demonstrating device
CN210574589U (en) Experimental device for preparing oxygen by using hydrogen peroxide
CN202387275U (en) Simple suction filter
CN202495185U (en) Integrated chlorine property demonstration experiment device
CN205028558U (en) Experimental device for carbon dioxide gas is prepared in laboratory
CN204523000U (en) Experiment dropper device special in a kind of pharmaceutical engineering compound experiment room

Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150520

Termination date: 20151225

EXPY Termination of patent right or utility model