CN204330705U - A kind of multifunctional intelligent catalyst test apparatus - Google Patents
A kind of multifunctional intelligent catalyst test apparatus Download PDFInfo
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- CN204330705U CN204330705U CN201520002657.1U CN201520002657U CN204330705U CN 204330705 U CN204330705 U CN 204330705U CN 201520002657 U CN201520002657 U CN 201520002657U CN 204330705 U CN204330705 U CN 204330705U
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Abstract
The utility model relates to a kind of multifunctional intelligent catalyst test apparatus, this device comprises gas and liquid line unit, catalytic reaction unit, analytic unit and control module, and wherein control module comprises traffic controller (21), pressure control plate (22), temperature control panel (23), local monitor unit (24), remote real-time monitoring unit (25).This device can evaluate the reaction between gas and gas, the reaction between gas and liquid, temperature of reaction between the reaction of room temperature-1000 DEG C, reaction pressure between the catalyst performance of the reaction of 0-20MPa, there is multi-functional characteristic, can show in real time and all flows, the temperature and pressure in control device simultaneously, and flow, temperature and pressure data are real-time transmitted on remote real-time monitoring unit by network, achieve the intellectuality of catalyst test apparatus.
Description
Technical field
The utility model belongs to catalyst development field of engineering technology, is specifically related to a kind of multifunctional intelligent catalyst test apparatus.
Background technology
The purposes of catalyst test apparatus investigates the activity of catalyzer, selectivity and life-span, and screening high performance catalyst, for the application of catalyzer provides support.
Current catalyst test apparatus has very strong specific aim, and a catalyst test apparatus often can only be used for a reaction.For dissimilar reaction, must purchase different catalyst test apparatus, fund input is larger.
Current catalyst test apparatus still needs people manually to arrange required flow, temperature and pressure on evaluating apparatus, operates cumbersome, and needs people to wait for the running status of supervising device on evaluating apparatus limit always, very labor intensive resource.Therefore, a kind of multifunctional intelligent catalyst test apparatus is developed significant.
Utility model content
For solving the problems of the technologies described above, the utility model provides a kind of multifunctional intelligent catalyst test apparatus, solves the technical matters existed in existing apparatus: 1, evaluating apparatus poor universality; 2, the flow of evaluating apparatus, temperature and pressure need people manually to go to arrange; 3, need people to wait for the running status of supervising device on evaluating apparatus limit, labor intensive resource always.
The purpose of this utility model is achieved through the following technical solutions: disclosed in the utility model, multifunctional intelligent catalyst test apparatus comprises the first gas piping, second gas piping, 3rd gas piping, liquid line, first gas flow rate control unit, second gas flow rate control unit, 3rd gas flow rate control unit, fluid flow control module, pressure transducer, first heating cabinet, second heating cabinet, catalytic reactor, display thermopair, catalyzer, heating furnace, 3rd heating cabinet, needle-valve, cold-trap, analytic unit, counterbalance valve, traffic controller, pressure control plate, temperature control panel, local monitor unit, remote real-time monitoring unit,
Wherein: catalyzer is positioned at the middle part of catalytic reactor; Catalytic reactor is positioned at the middle part of heating furnace; Display thermopair is positioned at the middle part of catalytic reactor; Heating furnace is arranged in the first heating cabinet; The top and bottom of catalytic reactor lay respectively in the middle of the second heating cabinet and the 3rd heating cabinet;
First gas piping, the second gas piping and the 3rd gas piping are connected with the 3rd gas flow rate control unit with the first gas flow rate control unit, the second gas flow rate control unit respectively, a road is merged into further by four-way connection, a road is merged into the liquid line by fluid flow control module, gas piping is divided into two-way by three-way connection, one tunnel is connected with pressure transducer, and another road is connected with the upper end of catalytic reactor through the second heating cabinet after carrying out spiral beating circle after the first heating cabinet; The lower end of catalytic reactor is divided into two-way by three-way connection, and needle-valve of leading up to is connected with analytic unit, and another road is connected with cold-trap, and cold-trap outlet is connected with counterbalance valve, and the pipeline after counterbalance valve carries out emptying;
First gas flow rate control unit, the second gas flow rate control unit, the 3rd gas flow rate control unit are connected with traffic controller respectively by circuit with fluid flow control module; Pressure transducer is connected with pressure control plate by circuit; First heating cabinet, the second heating cabinet, heating furnace are connected with temperature control panel respectively by circuit with the 3rd heating cabinet; Display thermopair is connected with temperature control panel by circuit; Traffic controller, pressure control plate are connected with local monitor unit respectively by circuit with temperature control panel; Analytic unit is connected with local monitor unit by circuit; Local monitor unit is connected with remote real-time monitoring unit by network.
The first described gas flow rate control unit, the second gas flow rate control unit, the 3rd gas flow rate control unit include the switch valve, pressure maintaining valve, tensimeter, flow stabilizing valve, the mass flow controller that connect successively; Described fluid flow control module comprises the liquor pump, vaporizer, the retaining valve that connect successively.
Described analytic unit comprises multiport valve and gas chromatography.
The heating temperature range of described heating furnace: room temperature-1000 DEG C; The heating temperature range of the first described heating cabinet, the second heating cabinet, the 3rd heating cabinet: room temperature-500 DEG C.
The withstand voltage scope of device: 0-20MPa.
Device is for evaluating the reaction between gas and gas, the reaction between gas and liquid, temperature of reaction between the reaction of room temperature-1000 DEG C, reaction pressure between the catalyst performance of the reaction of 0-20MPa.
Described local monitor unit is used for all flows, temperature and pressure in display in real time and control device, and flow, temperature and pressure data is real-time transmitted on remote real-time monitoring unit 25 by network.
Described remote real-time monitoring unit is not limited to mobile phone, panel computer, computing machine; Described network is not limited to Wi-Fi, LAN (Local Area Network), note, 2G network, 3G network, 4G network.
Disclosed in the utility model, multifunctional intelligent catalyst test apparatus has following features:
1, this device can be used for evaluating the reaction between gas and gas, the reaction between gas and liquid, temperature of reaction between the catalyst performance of the reaction of 0-20MPa, have multi-functional characteristic between the reaction of room temperature-1000 DEG C, reaction pressure.
2, local monitor unit can show and all flows, temperature and pressure in control device in real time, and flow, temperature and pressure data are real-time transmitted on remote real-time monitoring unit by network, achieve the intellectuality of catalyst test apparatus, manpower can be freed and do more how creationary work.
Accompanying drawing explanation
The schematic diagram of Fig. 1 multifunctional intelligent catalyst test apparatus disclosed in the utility model, wherein: 1 is the first gas piping, 2 is the second gas piping, 3 is the 3rd gas piping, 4 is liquid line, 5 is the first gas flow rate control unit, 6 is the second gas flow rate control unit, 7 is the 3rd gas flow rate control unit, 8 is fluid flow control module, 9 is pressure transducer, 10 is the first heating cabinet, 11 is the second heating cabinet, 12 is catalytic reactor, 13 is display thermopair, 14 is catalyzer, 15 is heating furnace, 16 is the 3rd heating cabinet, 17 is needle-valve, 18 is cold-trap, 19 is analytic unit, 20 is counterbalance valve, 21 is traffic controller, 22 is pressure control plate, 23 is temperature control panel, 24 is local monitor unit, 25 is remote real-time monitoring unit.
Embodiment
Below in conjunction with accompanying drawing 1 and embodiment, the utility model is described in further detail.
Embodiment 1:
Multifunctional intelligent catalyst test apparatus disclosed in the utility model comprises the first gas piping 1, second gas piping 2, 3rd gas piping 3, liquid line 4, first gas flow rate control unit 5, second gas flow rate control unit 6, 3rd gas flow rate control unit 7, fluid flow control module 8, pressure transducer 9, first heating cabinet 10, second heating cabinet 11, catalytic reactor 12, display thermopair 13, catalyzer 14, heating furnace 15, 3rd heating cabinet 16, needle-valve 17, cold-trap 18, analytic unit 19, counterbalance valve 20, traffic controller 21, pressure control plate 22, temperature control panel 23, local monitor unit 24, remote real-time monitoring unit 25, wherein: catalyzer 14 is positioned at the middle part of catalytic reactor 12, catalytic reactor 12 is positioned at the middle part of heating furnace 15, display thermopair 13 is positioned at the middle part of catalytic reactor 12, heating furnace 15 is arranged in the first heating cabinet 10, the top and bottom of catalytic reactor 12 lay respectively in the middle of the second heating cabinet 11 and the 3rd heating cabinet 16,
First gas piping 1, second gas piping 2 and the 3rd gas piping 3 are connected with the 3rd gas flow rate control unit 7 with the first gas flow rate control unit 5, second gas flow rate control unit 6 respectively, a road is merged into further by four-way connection, a road is merged into the liquid line 4 by fluid flow control module 8, gas piping is divided into two-way by three-way connection, one tunnel is connected with pressure transducer 9, and another road is connected with the upper end of catalytic reactor 12 through the second heating cabinet 11 after carrying out spiral beating circle after the first heating cabinet 10; The lower end of catalytic reactor 12 is divided into two-way by three-way connection, and needle-valve 17 of leading up to is connected with analytic unit 19, and another road is connected with cold-trap 18, and cold-trap outlet is connected with counterbalance valve 20, and the pipeline after counterbalance valve 20 carries out emptying;
First gas flow rate control unit 5, second gas flow rate control unit 6, the 3rd gas flow rate control unit 7 are connected with traffic controller 21 respectively by circuit with fluid flow control module 8; Pressure transducer 9 is connected with pressure control plate 22 by circuit; First heating cabinet 10, second heating cabinet 11, heating furnace 15 are connected with temperature control panel 23 respectively by circuit with the 3rd heating cabinet 16; Display thermopair 13 is connected with temperature control panel 23 by circuit; Traffic controller 21, pressure control plate 22 are connected with local monitor unit 24 respectively by circuit with temperature control panel 23; Analytic unit 19 is connected with local monitor unit 24 by circuit; Local monitor unit 24 is connected with remote real-time monitoring unit 25 by network.
The first described gas flow rate control unit 5, second gas flow rate control unit 6, the 3rd gas flow rate control unit 7 include the switch valve, pressure maintaining valve, tensimeter, flow stabilizing valve, the mass flow controller that connect successively; Described fluid flow control module 8 comprises the liquor pump, vaporizer, the retaining valve that connect successively.
Described analytic unit 19 comprises multiport valve and gas chromatography.
The heating temperature range of described heating furnace 15: room temperature-1000 DEG C; The first described heating cabinet 10, second heating cabinet 11, the heating temperature range of the 3rd heating cabinet 16: room temperature-500 DEG C.
The withstand voltage scope of device: 0-20MPa.
Flow, temperature and pressure data for all flows, the temperature and pressure in display in real time and control device, and are real-time transmitted on remote real-time monitoring unit 25 by network by described local monitor unit 24.
Described remote real-time monitoring unit 25 is mobile phone, and network is 4G wireless network.
Exemplary, disclosed in use the utility model, the method for multifunctional intelligent catalyst test apparatus evaluate catalysts can be as follows:
1, measure catalyzer, put into catalytic reactor, inert stone sand is all filled at upper and lower two ends;
2, the first gas piping 1, second gas piping 2, the 3rd gas piping 3 is opened, by the temperature of local monitor unit 24 adjusting gas flow, reaction pressure and reacting furnace;
3, gas flows through catalyzer generation catalytic reaction, generates product, by composition and the content of analytic unit 19 assay products;
4, the flow of monitoring, temperature and pressure data are passed through 4G wireless network transmissions to remote real-time monitoring mobile phone 25 by local monitor unit 24 in real time.
5, operator monitors the running status of reaction at any time by remote real-time monitoring mobile phone 25, is regulated flow, the temperature and pressure parameter of catalyst test apparatus according to the running status of reaction at any time by remote real-time monitoring mobile phone 25.
Above-described embodiment is only for illustration of the composition of multifunctional intelligent catalyst test apparatus disclosed in the utility model, connected mode and using method; the utility model is not attempted to protect any method; only protect the product met the legal requirements; above-described embodiment does not limit the utility model; all do within spirit of the present utility model and principle any amendment, parts equivalent replacement and improvement etc., be all included within protection domain of the present utility model.
Claims (8)
1. a multifunctional intelligent catalyst test apparatus, it is characterized in that: this device comprises the first gas piping (1), second gas piping (2), 3rd gas piping (3), liquid line (4), first gas flow rate control unit (5), second gas flow rate control unit (6), 3rd gas flow rate control unit (7), fluid flow control module (8), pressure transducer (9), first heating cabinet (10), second heating cabinet (11), catalytic reactor (12), display thermopair (13), catalyzer (14), heating furnace (15), 3rd heating cabinet (16), needle-valve (17), cold-trap (18), analytic unit (19), counterbalance valve (20), traffic controller (21), pressure control plate (22), temperature control panel (23), local monitor unit (24), remote real-time monitoring unit (25),
Wherein: catalyzer (14) is positioned at the middle part of catalytic reactor (12); Catalytic reactor (12) is positioned at the middle part of heating furnace (15); Display thermopair (13) is positioned at the middle part of catalytic reactor (12); Heating furnace (15) is arranged in the first heating cabinet (10); The top and bottom of catalytic reactor (12) lay respectively in the middle of the second heating cabinet (11) and the 3rd heating cabinet (16);
First gas piping (1), second gas piping (2) and the 3rd gas piping (3) respectively with the first gas flow rate control unit (5), second gas flow rate control unit (6) is connected with the 3rd gas flow rate control unit (7), a road is merged into further by four-way connection, a road is merged into the liquid line (4) by fluid flow control module (8), gas piping is divided into two-way by three-way connection, one tunnel is connected with pressure transducer (9), another road is connected with the upper end of catalytic reactor (12) through the second heating cabinet (11) after carrying out spiral beating circle after the first heating cabinet (10), the lower end of catalytic reactor (12) is divided into two-way by three-way connection, needle-valve (17) of leading up to is connected with analytic unit (19), another road is connected with cold-trap (18), cold-trap outlet is connected with counterbalance valve (20), and the pipeline after counterbalance valve (20) carries out emptying,
First gas flow rate control unit (5), the second gas flow rate control unit (6), the 3rd gas flow rate control unit (7) are connected with traffic controller (21) respectively by circuit with fluid flow control module (8); Pressure transducer (9) is connected with pressure control plate (22) by circuit; First heating cabinet (10), the second heating cabinet (11), heating furnace (15) are connected with temperature control panel (23) respectively by circuit with the 3rd heating cabinet (16); Display thermopair (13) is connected with temperature control panel (23) by circuit; Traffic controller (21), pressure control plate (22) are connected with local monitor unit (24) respectively by circuit with temperature control panel (23); Analytic unit (19) is connected with local monitor unit (24) by circuit; Local monitor unit (24) is connected with remote real-time monitoring unit (25) by network.
2. multifunctional intelligent catalyst test apparatus according to claim 1, is characterized in that: described the first gas flow rate control unit (5), the second gas flow rate control unit (6), the 3rd gas flow rate control unit (7) comprise the switch valve, pressure maintaining valve, tensimeter, flow stabilizing valve, the mass flow controller that connect successively; Described fluid flow control module (8) comprises the liquor pump, vaporizer, the retaining valve that connect successively.
3. multifunctional intelligent catalyst test apparatus according to claim 1, is characterized in that: described analytic unit (19) comprises multiport valve and gas chromatography.
4. multifunctional intelligent catalyst test apparatus according to claim 1, is characterized in that: the heating temperature range of described heating furnace (15): room temperature-1000 DEG C; The heating temperature range of described the first heating cabinet (10), the second heating cabinet (11), the 3rd heating cabinet (16): room temperature-500 DEG C.
5. multifunctional intelligent catalyst test apparatus according to claim 1, is characterized in that: the withstand voltage scope of device: 0-20MPa.
6. multifunctional intelligent catalyst test apparatus according to claim 1, is characterized in that: device is for evaluating the reaction between gas and gas, the reaction between gas and liquid, temperature of reaction between the reaction of room temperature-1000 DEG C, reaction pressure between the catalyst performance of the reaction of 0-20MPa.
7. multifunctional intelligent catalyst test apparatus according to claim 1, it is characterized in that: flow, temperature and pressure data for all flows, the temperature and pressure in display in real time and control device, and are real-time transmitted on remote real-time monitoring unit (25) by network by described local monitor unit (24).
8. the multifunctional intelligent catalyst test apparatus according to any one of claim 1-7, is characterized in that: described remote real-time monitoring unit (25) comprises mobile phone, panel computer, computing machine; Described network packet is containing Wi-Fi, LAN (Local Area Network), note, 2G network, 3G network, 4G network.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105116096A (en) * | 2015-08-13 | 2015-12-02 | 中国石油化工股份有限公司 | Hydrodeoxygenation catalyst evaluation device |
CN105823820A (en) * | 2015-11-13 | 2016-08-03 | 亚申科技研发中心(上海)有限公司 | Catalyst evaluating apparatus |
CN109406726A (en) * | 2018-10-26 | 2019-03-01 | 上海化工研究院有限公司 | A kind of polyolefin catalyst kinetic assay device and method |
CN111207794A (en) * | 2020-03-18 | 2020-05-29 | 江苏建筑职业技术学院 | Catalyst preparation monitoring and control system |
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2015
- 2015-01-04 CN CN201520002657.1U patent/CN204330705U/en active Active
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105116096A (en) * | 2015-08-13 | 2015-12-02 | 中国石油化工股份有限公司 | Hydrodeoxygenation catalyst evaluation device |
CN105823820A (en) * | 2015-11-13 | 2016-08-03 | 亚申科技研发中心(上海)有限公司 | Catalyst evaluating apparatus |
CN105823820B (en) * | 2015-11-13 | 2019-02-15 | 亚申科技研发中心(上海)有限公司 | Catalyst test apparatus |
CN109406726A (en) * | 2018-10-26 | 2019-03-01 | 上海化工研究院有限公司 | A kind of polyolefin catalyst kinetic assay device and method |
CN111207794A (en) * | 2020-03-18 | 2020-05-29 | 江苏建筑职业技术学院 | Catalyst preparation monitoring and control system |
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