CN204324874U - A kind of sulfur oxychloride Matter Transfer reactive system - Google Patents
A kind of sulfur oxychloride Matter Transfer reactive system Download PDFInfo
- Publication number
- CN204324874U CN204324874U CN201420808912.7U CN201420808912U CN204324874U CN 204324874 U CN204324874 U CN 204324874U CN 201420808912 U CN201420808912 U CN 201420808912U CN 204324874 U CN204324874 U CN 204324874U
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- CN
- China
- Prior art keywords
- synthesizer
- water cooler
- knockout drum
- sulfur oxychloride
- feed opening
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Abstract
The utility model relates to a kind of sulfur oxychloride Matter Transfer reactive system, it comprises synthesizer, described synthesizer top is provided with raw material gas inlet, the bottom of described synthesizer is provided with feed opening, described feed opening is connected with water cooler, described feed opening is connected with one end of water cooler, the other end of water cooler is connected with crude product receiving tank, described water cooler is connected with the top of crude product receiving tank, the top of described crude product receiving tank is connected with injector, the top of described injector is connected with knockout drum, the bottom of described knockout drum is connected with recycle pump, described recycle pump is connected with the middle and upper part of injector, the top of described knockout drum is provided with gaseous phase materials outlet, the utility model simplicity of design, by gas-liquid ejector, material is squeezed in knockout drum, thus gas-liquid is thoroughly separated, and then gaseous phase materials is transported in synthesizer, recycle, economize on resources, protection of the environment.
Description
Technical field
The utility model belongs to chemical technology field, is specifically related to circulating reaction system, particularly a kind of sulfur oxychloride Matter Transfer reactive system.
Background technology
Sulfur oxychloride is the intermediate of a kind of important fine chemical product and the many chemical of synthesis, because it has very strong chlorination and chloride ability, the utilization ratio of some expensive raw materials can be improved significantly, as chlorination reagent and chloride reagent, sulfur oxychloride is mainly used in agricultural chemicals, medicine, the industries such as dyestuff, also can be used as alcohols, acid anhydrides, the synthesis of nitro-compound or the chlorizating agent of displacement, also can be used as thiazoline in ring-closure reaction, chlorine acylating agent and the catalyzer etc. in some organic synthesis of the compou nd synthesis such as tetramethyleneimine and acid amides, high tension battery also uses a large amount of sulfur oxychlorides in producing, at present, for the reactive system of sulfur oxychloride, all directly be discharged in air for the gas not participated in reaction, not only waste resource, also contaminate environment, more virtually add the cost of enterprise.
Summary of the invention
The purpose of this utility model is to overcome the deficiencies in the prior art, and provides that a kind of simplicity of design, cost are low, the sulfur oxychloride Matter Transfer reactive system of saving resource, protection of the environment.
The purpose of this utility model is achieved in that a kind of sulfur oxychloride Matter Transfer reactive system, it comprises synthesizer, described synthesizer top is provided with raw material gas inlet, the bottom of described synthesizer is provided with feed opening, described feed opening is connected with water cooler, described feed opening is connected with one end of water cooler, the other end of water cooler is connected with crude product receiving tank, described water cooler is connected with the top of crude product receiving tank, the top of described crude product receiving tank is connected with injector, the top of described injector is connected with knockout drum, the bottom of described knockout drum is connected with recycle pump, described recycle pump is connected with the middle and upper part of injector, the top of described knockout drum is provided with gaseous phase materials outlet.
Sulfur oxychloride solution is loaded with in described knockout drum.
Gas is sent to synthesizer by described gaseous phase materials outlet again.
Described raw material gas inlet is arranged on the centre at synthesizer top.
Described feed opening is arranged on the centre bottom synthesizer.
The beneficial effects of the utility model: the utility model simplicity of design, unstripped gas is after synthesizer reaction, crude product receiving tank is entered by water cooler cooling, liquid phase material is collected, gaseous phase materials is gone out from the top of crude product receptor and is entered injector, knockout drum passes through recycle pump in addition, sulfur oxychloride liquid is also squeezed in injector, deliver in knockout drum after gas-liquid compression, and then by gas-liquid separation, gaseous phase materials mixes with unstripped gas again, enter in synthesizer, again reaction is participated in, whole Process Design is simple, cost is low, save resource, protection of the environment.
Accompanying drawing explanation
Fig. 1 is the schema of a kind of sulfur oxychloride Matter Transfer of the utility model reactive system.
In figure: 1, synthesizer 2, raw material gas inlet 3, feed opening 4, water cooler 5, crude product receiving tank 6, injector 7, knockout drum 8, recycle pump 9, gaseous phase materials outlet.
Embodiment
Below in conjunction with accompanying drawing, the utility model is described further.
Embodiment 1
As shown in Figure 1, a kind of sulfur oxychloride Matter Transfer reactive system, it comprises synthesizer 1, described synthesizer 1 top is provided with raw material gas inlet 2, the bottom of described synthesizer 1 is provided with feed opening 3, described feed opening 3 is connected with water cooler 4, described feed opening 3 is connected with one end of water cooler 4, the other end of water cooler 4 is connected with crude product receiving tank 5, described water cooler 4 is connected with the top of crude product receiving tank 5, the top of described crude product receiving tank 5 is connected with injector 6, the top of described injector 6 is connected with knockout drum 7, the bottom of described knockout drum 7 is connected with recycle pump 8, described recycle pump 8 is connected with the middle and upper part of injector 6, the top of described knockout drum 7 is provided with gaseous phase materials outlet 9.
The utility model simplicity of design, first the unstripped gas of synthesizing chlorinated sulfoxide is sent in synthesizer, participate in reaction in synthesizer after, by feed opening material is sent in water cooler and cools, crude product receiving tank is entered by water cooler cooling, thus liquid phase material is collected, gaseous phase materials is gone out from the top of crude product receptor and is entered injector, knockout drum passes through recycle pump in addition, sulfur oxychloride liquid is also squeezed in injector, deliver in knockout drum after gas-liquid compression, and then by gas-liquid separation, gaseous phase materials recycle, whole Process Design is simple, cost is low, save resource, protection of the environment.
Embodiment 2
As shown in Figure 1, a kind of sulfur oxychloride Matter Transfer reactive system, it comprises synthesizer 1, described synthesizer 1 top is provided with raw material gas inlet 2, the bottom of described synthesizer 1 is provided with feed opening 3, described feed opening 3 is connected with water cooler 4, described feed opening 3 is connected with one end of water cooler 4, the other end of water cooler 4 is connected with crude product receiving tank 5, described water cooler 4 is connected with the top of crude product receiving tank 5, the top of described crude product receiving tank 5 is connected with injector 6, the top of described injector 6 is connected with knockout drum 7, the bottom of described knockout drum 7 is connected with recycle pump 8, described recycle pump 8 is connected with the middle and upper part of injector 6, the top of described knockout drum 7 is provided with gaseous phase materials outlet 9.
Sulfur oxychloride solution is loaded with in described knockout drum 7.
Gas is sent to synthesizer by described gaseous phase materials outlet 9 again.
Described raw material gas inlet 2 is arranged on the centre at synthesizer top.
Described feed opening 3 is arranged on the centre bottom synthesizer.
The utility model simplicity of design, first the unstripped gas of synthesizing chlorinated sulfoxide is sent in synthesizer, participate in reaction in synthesizer after, by feed opening material is sent in water cooler and cools, crude product receiving tank is entered by water cooler cooling, thus liquid phase material is collected, gaseous phase materials is gone out from the top of crude product receptor and is entered injector, sulfur oxychloride liquid is loaded with in addition in knockout drum, pass through recycle pump, sulfur oxychloride liquid is also squeezed in injector, deliver in knockout drum after gas-liquid compression, and then by gas-liquid separation, gaseous phase materials mixes with unstripped gas again, enter in synthesizer, again reaction is participated in, raw material gas inlet and feed opening are separately positioned on the centre of synthesizer top and bottom, thus guarantee air inlet uniformity, blanking is also even, whole Process Design is simple in a word, cost is low, save resource, protection of the environment.
Claims (5)
1. a sulfur oxychloride Matter Transfer reactive system, it comprises synthesizer, it is characterized in that: described synthesizer top is provided with raw material gas inlet, the bottom of described synthesizer is provided with feed opening, described feed opening is connected with water cooler, described feed opening is connected with one end of water cooler, the other end of water cooler is connected with crude product receiving tank, described water cooler is connected with the top of crude product receiving tank, the top of described crude product receiving tank is connected with injector, the top of described injector is connected with knockout drum, the bottom of described knockout drum is connected with recycle pump, described recycle pump is connected with the middle and upper part of injector, the top of described knockout drum is provided with gaseous phase materials outlet.
2. a kind of sulfur oxychloride Matter Transfer reactive system according to claim 1, is characterized in that: be loaded with sulfur oxychloride solution in described knockout drum.
3. a kind of sulfur oxychloride Matter Transfer reactive system according to claim 1, is characterized in that: gas is sent to synthesizer by described gaseous phase materials outlet again.
4. a kind of sulfur oxychloride Matter Transfer reactive system according to claim 1, is characterized in that: described raw material gas inlet is arranged on the centre at synthesizer top.
5. a kind of sulfur oxychloride Matter Transfer reactive system according to claim 1, is characterized in that: described feed opening is arranged on the centre bottom synthesizer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420808912.7U CN204324874U (en) | 2014-12-19 | 2014-12-19 | A kind of sulfur oxychloride Matter Transfer reactive system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420808912.7U CN204324874U (en) | 2014-12-19 | 2014-12-19 | A kind of sulfur oxychloride Matter Transfer reactive system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204324874U true CN204324874U (en) | 2015-05-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420808912.7U Expired - Fee Related CN204324874U (en) | 2014-12-19 | 2014-12-19 | A kind of sulfur oxychloride Matter Transfer reactive system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204324874U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106185840A (en) * | 2016-07-04 | 2016-12-07 | 汇智工程科技有限公司 | Thionyl chloride subtractive process improves the extraction method and device of product quality |
| CN108036667A (en) * | 2017-11-30 | 2018-05-15 | 山东凯盛新材料股份有限公司 | Produce the raw material cryogenic energy utilization technique of thionyl chloride |
-
2014
- 2014-12-19 CN CN201420808912.7U patent/CN204324874U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106185840A (en) * | 2016-07-04 | 2016-12-07 | 汇智工程科技有限公司 | Thionyl chloride subtractive process improves the extraction method and device of product quality |
| CN108036667A (en) * | 2017-11-30 | 2018-05-15 | 山东凯盛新材料股份有限公司 | Produce the raw material cryogenic energy utilization technique of thionyl chloride |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee | ||
| CP03 | Change of name, title or address |
Address after: 453000 east section of Qinglong Road, Xinxiang Economic Development Zone, Henan Patentee after: XINXIANG RUICHENG TECHNOLOGY CO., LTD. Address before: Xinxiang City, Henan province 453000 Xinxiang County Langgongmiao town Qushui Village North Patentee before: XINXIANG RUICHENG TECHNOLOGY DEVELOPMENT CO., LTD. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150513 Termination date: 20161219 |