CN204269618U - There is the TCD detecting device of cooling device - Google Patents

There is the TCD detecting device of cooling device Download PDF

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Publication number
CN204269618U
CN204269618U CN201420630271.0U CN201420630271U CN204269618U CN 204269618 U CN204269618 U CN 204269618U CN 201420630271 U CN201420630271 U CN 201420630271U CN 204269618 U CN204269618 U CN 204269618U
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CN
China
Prior art keywords
tcd
detecting device
generating means
cooling tube
tcd detecting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420630271.0U
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Chinese (zh)
Inventor
倪东华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shimadzu Corp
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Shimadzu Corp
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Filing date
Publication date
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Priority to CN201420630271.0U priority Critical patent/CN204269618U/en
Application granted granted Critical
Publication of CN204269618U publication Critical patent/CN204269618U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model provides a kind of TCD detecting device with cooling device, comprises: outer cover; TCD pond body assembly, is configured to be closed by described outer cover cover; Heat conducting sleeve, be configured to circumference and surround described TCD pond body assembly, and form an entirety with described TCD pond body assembly, described TCD detecting device comprises further: cooling tube, is configured to be coiled in described heat conducting sleeve outside surface; Refrigerant generating means, the delivery outlet of described refrigerant generating means is connected with the import of described cooling tube.

Description

There is the TCD detecting device of cooling device
Technical field
The utility model relates to a kind of TCD detecting device with cooling device that all kinds of gas chromatograph is commonly used.
Background technology
At present, the TCD detecting device generally used in gas chromatograph after a procedure temperature is very high, but existing TCD detecting device is all Temperature fall type cools down and need long time.If adjust to a relatively low temperature, will exhaust a lot of time, concerning very inconvenient experimenter, and conventional efficient is also very low.Therefore, have a kind of TCD detecting device with quick cooling function of design, realizing can fast to detecting device cooling, the needs effectively shortening detecting device temperature fall time in experimentation, raising analytical test efficiency in stratographic analysis testing process.
As the example of thermal conductivity detector (TCD) with quick cooling function, Chinese CN203324238U patent (patent documentation 1) discloses a kind of thermal conductivity detector (TCD) with quick cooling function, and it is made up of thermal conductivity detector (TCD) and semiconductor chilling plate.This patent, by the control to thermal conductivity detector (TCD) and cooling piece of the main frame temperature-controlled portion of gas chromatograph, can realizing the gradient constant-temperatureactivation of detecting device, effectively can shorten experimental period by cooling detector functions fast.
Relate art literature
Patent documentation
Patent documentation 1: Chinese CN203324238U patent
But, technical scheme disclosed in patent documentation 1 adopts semiconductor chilling plate, although rapid cooling thermal can be played in theory to be led detecting device, effectively shorten the technique effect of experimental period, but in practical operation, because TCD pond maximum temperature can reach 400 DEG C, semiconductor is difficult to bear this temperature.That is, the easy Yin Wendu in TCD sensors work process of the semiconductor chilling plate disclosed in patent documentation 1 is too high and damage, and makes to cool thermal conductivity detector (TCD).
Utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art, a kind of TCD detecting device with cooling device is provided, it can not only meet TCD detecting device and use rear fast cooling, improve the requirement of conventional efficient, also solve the too high and technical matters damaged of semiconductor chilling plate easy Yin Wendu in TCD sensors work process disclosed in patent documentation 1, and this installation cost is very low, without the need to semiconductor chilling plate as disclosed in Patent Document 1 in TCD detecting device the required main frame temperature-controlled portion by gas chromatograph to the Special controlling of the control of thermal conductivity detector (TCD) and cooling piece etc., be easy to user operation.
The utility model provides a kind of TCD detecting device with quick cooling function, comprises: outer cover; TCD pond body assembly, is configured to be closed by described outer cover cover; Heat conducting sleeve, be configured to circumference and surround described TCD pond body assembly, and form an entirety with described TCD pond body assembly, described TCD detecting device comprises further: cooling tube, is configured to be coiled in described heat conducting sleeve outside surface; Refrigerant generating means, the delivery outlet of described refrigerant generating means is connected with the import of described cooling tube.
The import of the described cooling tube of this TCD detecting device and outlet are passed through described outer cover and are exposed from described outer cover.
This TCD detecting device comprises joint transition components and flexible pipe further, and the delivery outlet of described refrigerant generating means is connected with the described import of described cooling tube with described flexible pipe via described joint transition components.
The described cooling tube of this TCD detecting device is copper pipe.
The described refrigerant generating means of this TCD detecting device exports normal temperature or the gas lower than normal temperature.
The described gas that the described refrigerant generating means of this TCD detecting device exports is air.
The described refrigerant generating means of this TCD detecting device exports normal temperature or the liquid lower than normal temperature.
The refrigerant generating means of this TCD detecting device is pump.
Accompanying drawing explanation
When read in conjunction with the accompanying drawings, from detailed description below, other object and the further feature of embodiment will become apparent, wherein:
Fig. 1 is the schematic diagram with the TCD detecting device of cooling device of diagram according to the first embodiment;
Fig. 2 is the schematic diagram with the TCD detecting device of cooling device of diagram according to the second embodiment.
Symbol description
1 cooling tube
2 heat conducting sleeves
3TCD pond body assembly
4 outer covers
5 well heaters
6 temperature sensors
7 thermal conductance blocks
8 transition components
9 flexible pipes
10 refrigerant generating meanss.
Embodiment
Below in conjunction with Fig. 1, embodiment of the present utility model is elaborated.The example below illustrated is only illustration, content of the present utility model do not get rid of following do not express various distortion, technology be suitable for.That is, the utility model can carry out various distortion and implement in the scope not exceeding its aim.
First embodiment
Fig. 1 is the schematic diagram with the TCD detecting device of cooling device of diagram according to the first embodiment.As shown in Figure 1, first embodiment of the present utility model provides a kind of TCD detecting device with quick cooling function, and it comprises: outer cover 4, because TCD pool part temperature is more stable better, outer cover 4 can isolate the interference of outer bound pair pond temperature effectively, makes interior space temperature more stable; TCD pond body assembly 3, be configured to be covered conjunction by outer cover 4, this TCD pond body assembly 3 is cores of TCD detecting device, is the parts detecting chromatographic signal; Heat conducting sleeve 2, be configured to circumference and surround TCD pond body assembly 3, and form an entirety with TCD pond body assembly 3, when needs heating TCD pond, can even heat be conducted on the body of TCD pond, TCD pond body is heated more even, when needs fast cooling, needs equally by heat conducting sleeve to take away the heat on the body of TCD pond.This TCD detecting device comprises further: cooling tube 1, is configured to be coiled in heat conducting sleeve 2 outside surface; Refrigerant generating means 10, the delivery outlet of this refrigerant generating means 10 is connected with the import of cooling tube 1.TCD detecting device also comprises well heater 5, temperature sensor 6 and thermal conductance block 7.Well heater 5 is heaters, by applying voltage, calandria is generated heat, thus makes TCD pond temperature increase by heat transfer.By temperature sensor 6 feedback signal, thus realize the control of accurate temperature.The heat conduction that calandria produces by thermal conductance block 7 is to TCD pond body assembly.The refrigerant generating means of this TCD detecting device is the pump exporting gas or liquid, such as, by the device of the air in the external world by Output pressure, and the air compressor machine or small air pump etc. of such as delivery air.The import of the described cooling tube of this TCD detecting device and outlet are passed through described outer cover and are exposed from described outer cover.
According to the TCD detecting device with cooling device of the utility model first embodiment in use as a detection part of gas chromatograph, for detections such as gas concentrations, the control circuit of time gas chromatography instrument is used to be detected the internal temperature of TCD detecting device by temperature sensor 6, heated up by TCD detecting device internal heater 5 pairs of TCD detecting devices, realize detection at high temperature.When needing cooling after detection terminates, well heater 5 just quits work.Under normal circumstances, because TCD pond body is combined in an almost airtight space, so cooling slowly.And according to the TCD detecting device with cooling device of the utility model first embodiment, have cooling tube 1, such as copper pipe, glass tube, leather hose etc. in the coiling of heat conducting sleeve 2 outside surface, but the example of cooling tube 1 is not limited thereto, and can be resistance to high high temperature, any pipe of such as more than 400 DEG C.Now, refrigerant generating means 10 is started working and is exported refrigerant, and flow in cooling tube 1 refrigerant fast that exported by refrigerant generating means 10, thus taken away by heat rapidly.Especially, the refrigerant exported by refrigerant generating means 10 is normal temperature or lower than the gas of normal temperature or liquid, such as, can be gas or the liquid of less than 35 DEG C, be more preferably, the gas of less than 15 DEG C or liquid, but the temperature of gas or liquid is not limited to concrete numerical value described above, and the lower gas of temperature or liquid, cooling effect is better.Again, such as, the refrigerant exported by refrigerant generating means 10 is the air of normal temperature.For example, the flow velocity of the refrigerant exported by refrigerant generating means 10 that to flow fast in cooling tube 1 can control at about 5L/min, can realize comparatively significantly cooling-down effect.And the flow velocity of this refrigerant is not limited thereto, such as, can be the arbitrary value higher than 5L/min, and the flow velocity of refrigerant is faster, cooling effect be better.
Thus, when needing cooling after detection terminates, by cooling fast according to the cooling device work of the utility model first embodiment, meet the requirement that TCD detecting device cools fast, simultaneously, also solve the too high and technical matters damaged of semiconductor chilling plate easy Yin Wendu in TCD sensors work process disclosed in patent documentation 1, and this installation cost is very low, without the need to semiconductor chilling plate as disclosed in Patent Document 1 in TCD detecting device the required main frame temperature-controlled portion by gas chromatograph to the Special controlling of the control of thermal conductivity detector (TCD) and cooling piece etc., be easy to user operation.
Second embodiment
Comprise joint transition components 8 and flexible pipe 9 further according to the TCD detecting device of the second embodiment of the present utility model, the delivery outlet of refrigerant generating means 10 is connected with the import of flexible pipe 9 with cooling tube 1 via joint transition components 8.Joint transition components 8 is the X-overs be connected with flexible pipe 9 by cooling tube 1.Flexible pipe 9 is the supporting pipes being connected to refrigerant generating means 10.By configuration joint transition components 8 and flexible pipe 9, make more to be easy to control the operation to refrigerant generating means 10, such as, make it start working or quit work.
Consider above-mentioned instruction, much other distortion and change are possible.Therefore be understandable that, within the scope of the appended claims, can to realize content disclosed in the utility model except specifically described mode herein.For example, in the scope of the disclosure with additional claim, the parts of different examples and illustrative embodiment and/or characteristic can be combined with each other and/or phase trans-substitution.

Claims (8)

1. there is a TCD detecting device for cooling device, comprise:
Outer cover;
TCD pond body assembly, is configured to be closed by described outer cover cover;
Heat conducting sleeve, be configured to circumference and surround described TCD pond body assembly, and form an entirety with described TCD pond body assembly, the feature of described TCD detecting device is, comprises further:
Cooling tube, is configured to be coiled in described heat conducting sleeve outside surface;
Refrigerant generating means, the delivery outlet of described refrigerant generating means is connected with the import of described cooling tube.
2. TCD detecting device as claimed in claim 1, it is characterized in that, the import of described cooling tube and outlet are passed through described outer cover and are exposed from described outer cover.
3. TCD detecting device as claimed in claim 1, it is characterized in that, comprise joint transition components and flexible pipe further, the delivery outlet of described refrigerant generating means is connected with the described import of described cooling tube with described flexible pipe via described joint transition components.
4. TCD detecting device as claimed in claim 1, it is characterized in that, described cooling tube is copper pipe.
5. TCD detecting device as claimed in claim 1, is characterized in that, described refrigerant generating means exports normal temperature or the gas lower than normal temperature.
6. TCD detecting device as claimed in claim 5, it is characterized in that, described gas is air.
7. TCD detecting device as claimed in claim 1, is characterized in that, described refrigerant generating means exports normal temperature or the liquid lower than normal temperature.
8. TCD detecting device as claimed in claim 1, it is characterized in that, refrigerant generating means is pump.
CN201420630271.0U 2014-10-28 2014-10-28 There is the TCD detecting device of cooling device Expired - Fee Related CN204269618U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420630271.0U CN204269618U (en) 2014-10-28 2014-10-28 There is the TCD detecting device of cooling device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420630271.0U CN204269618U (en) 2014-10-28 2014-10-28 There is the TCD detecting device of cooling device

Publications (1)

Publication Number Publication Date
CN204269618U true CN204269618U (en) 2015-04-15

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201420630271.0U Expired - Fee Related CN204269618U (en) 2014-10-28 2014-10-28 There is the TCD detecting device of cooling device

Country Status (1)

Country Link
CN (1) CN204269618U (en)

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150415

Termination date: 20151028

EXPY Termination of patent right or utility model