CN204261362U - A kind of gathering-device of Rotary Evaporators volatile matter distillation oil - Google Patents

A kind of gathering-device of Rotary Evaporators volatile matter distillation oil Download PDF

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Publication number
CN204261362U
CN204261362U CN201420680052.3U CN201420680052U CN204261362U CN 204261362 U CN204261362 U CN 204261362U CN 201420680052 U CN201420680052 U CN 201420680052U CN 204261362 U CN204261362 U CN 204261362U
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China
Prior art keywords
flask
rotary evaporators
receiving flask
volatile matter
gathering
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CN201420680052.3U
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Chinese (zh)
Inventor
张必荣
张敏
张勇
闫高颖
杨妍
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Shaanxi Tiangu Pharmaceutical Co.,Ltd.
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SHAANXI TEEGOO BIOTECHNOLOGY GROUP Co Ltd
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Abstract

The utility model discloses a kind of gathering-device of Rotary Evaporators volatile matter distillation oil, comprise: evaporative flask (9), described evaporative flask (9) connects a teflon seal mechanism (7), described teflon seal mechanism (7) inside arranges a feed tube (8), and teflon seal mechanism (7) is connected with evaporative flask (9) by a tube connector, and be connected with a condenser (6) by another connection feed tube (5), the lower end of this condenser (6) connects one second receiving flask (3), this second receiving flask (3) connects again one first receiving flask (2), the upper end of described first receiving flask (2) arranges a spiracle (1).It can make the refinement more of volatile oil quality according to different to distill further the oil content do not steamed under normal pressure of negative pressure, and its rational in infrastructure, easy to use, efficient volatile matter distillation oil, has good effect.

Description

A kind of gathering-device of Rotary Evaporators volatile matter distillation oil
Technical field
The utility model relates to a kind of gathering-device of Rotary Evaporators volatile matter distillation oil.
Background technology
At present, Rotary Evaporators be mainly used in the industries such as medicine, chemical industry and bio-pharmaceuticals concentrated, crystallization, drying, be separated solvent.
Volatile matter distillation oil now by mature equipment, but can utilize Rotary Evaporators can obtain continuous still volatile oil device through simple transformation.
Utility model content
The utility model has expanded the scope of application of Rotary Evaporators, utilizes the advantage of Rotary Evaporators evaporimeter dynamic rotary (conventional volatile oil distiller raw material is for static) simultaneously.This application is novel provides a kind of Rotary Evaporators volatile oil gathering-device, its rational in infrastructure, easy to use, efficient volatile matter distillation oil.
It is as follows that the utility model solves the problems of the technologies described above taked technical scheme:
A kind of gathering-device of Rotary Evaporators volatile matter distillation oil, comprise: evaporative flask (9), described evaporative flask (9) connects a teflon seal mechanism (7), described teflon seal mechanism (7) inside arranges a feed tube (8), and teflon seal mechanism (7) is connected with evaporative flask (9) by a tube connector, and be connected with a condenser (6) by another connection feed tube (5), the lower end of this condenser (6) connects one second receiving flask (3), this second receiving flask (3) connects again one first receiving flask (2), the upper end of described first receiving flask (2) arranges a spiracle (1).
Further, preferably, the lower end of described condenser (6) is a tube connector, and this tube connector is connected to described second receiving flask (3), and on tube connector, arrange link folder (4).
Further, preferably, described evaporative flask is the evaporative flask of Rotary Evaporators.
After the utility model takes such scheme, can make the refinement more of volatile oil quality according to different to distill further the oil content do not steamed under normal pressure of negative pressure, its rational in infrastructure, easy to use, efficient volatile matter distillation oil, has good effect.
Other features and advantages of the utility model will be set forth in the following description, and, partly become apparent from description, or understand by implementing the utility model.The purpose of this utility model and other advantages realize by structure specifically noted in write description, claims and accompanying drawing and obtain.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the utility model is described in detail, to make above-mentioned advantage of the present utility model definitely.
Fig. 1 is the structural representation of the gathering-device of a kind of Rotary Evaporators volatile matter distillation of the utility model oil.
Detailed description of the invention
Below in conjunction with specific embodiment, the utility model is described in detail.
As shown in Figure 1, the gathering-device of described Rotary Evaporators volatile matter distillation oil, comprise: evaporative flask 9, described evaporative flask 9 connects a teflon seal mechanism 7, described teflon seal mechanism 7 inside arranges a feed tube 8, and teflon seal mechanism 7 is connected with evaporative flask 9 by a tube connector, and be connected with a condenser 6 by another connection feed tube 5, the lower end of this condenser 6 connects one second receiving flask 3, this second receiving flask 3 connects one first receiving flask 2 again, the upper end of described first receiving flask 2 arranges a spiracle 1, valve 10 is provided with in the bottom of the second receiving flask 3.
Further, preferably, the lower end of described condenser 6 is a tube connector, and this tube connector is connected to described second receiving flask 3, and on tube connector, arrange a link folder 4.
Further, preferably, described evaporative flask is the evaporative flask of Rotary Evaporators.
In addition, be also connected with a ground valve at the sidewall of described second receiving flask 3, connect volatile oil second receiving flask.The utility model can utilize the transformation of Rotary Evaporators receiving flask to achieve the continuous still of volatile oil, increases the usage range of Rotary Evaporators.
Wherein, operation principle of the present invention is:
Utilize the evaporative flask of Rotary Evaporators to accommodate and wait to steam raw material, utilize negative pressure of vacuum from feed tube suction water to evaporative flask, evaporation process closes vacuum, open condensed water, air-distillation, when liquid to be distilled is collected into the discharge valve of the second receiving flask, adjustment receiving flask bleeder valve, make volatile oil remain on discharge valve, make volatile oil flow to the first receiving flask.
This application is novel also can make the refinement more of volatile oil quality according to different to distill further the oil content do not steamed under normal pressure of negative pressure.
Wherein, it utilizes the evaporative flask 9 of Rotary Evaporators to accommodate to wait to steam raw material, utilize negative pressure of vacuum from feed tube 5,8 suction water to evaporative flask 9, evaporation process closes vacuum, opens condensed water, air-distillation, when liquid to be distilled is collected into the discharge valve of the second receiving flask, adjust the bleeder valve of the second receiving flask, make volatile oil remain on discharge valve, make volatile oil flow to the first receiving flask.
After the utility model takes such scheme, can make the refinement more of volatile oil quality according to different to distill further the oil content do not steamed under normal pressure of negative pressure, its rational in infrastructure, easy to use, efficient volatile matter distillation oil, has good effect.
Last it is noted that the foregoing is only preferred embodiment of the present utility model, be not limited to the utility model, although be described in detail the utility model with reference to previous embodiment, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.All within spirit of the present utility model and principle, any amendment done, equivalent replacement, improvement etc., all should be included within protection domain of the present utility model.

Claims (3)

1. the gathering-device of a Rotary Evaporators volatile matter distillation oil, it is characterized in that, comprise: evaporative flask (9), described evaporative flask (9) connects a teflon seal mechanism (7), described teflon seal mechanism (7) inside arranges a feed tube (8), and teflon seal mechanism (7) is connected with evaporative flask (9) by a tube connector, and be connected with a condenser (6) by another connection feed tube (5), the lower end of this condenser (6) connects one second receiving flask (3), this second receiving flask (3) connects again one first receiving flask (2), the upper end of described first receiving flask (2) arranges a spiracle (1).
2. the gathering-device of Rotary Evaporators volatile matter distillation oil according to claim 1, it is characterized in that, the lower end of described condenser (6) is a tube connector, and this tube connector is connected to described second receiving flask (3), and on tube connector, arrange link folder (4).
3. the gathering-device of Rotary Evaporators volatile matter distillation oil according to claim 1, is characterized in that, described evaporative flask is the evaporative flask of Rotary Evaporators.
CN201420680052.3U 2014-11-14 2014-11-14 A kind of gathering-device of Rotary Evaporators volatile matter distillation oil Active CN204261362U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420680052.3U CN204261362U (en) 2014-11-14 2014-11-14 A kind of gathering-device of Rotary Evaporators volatile matter distillation oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420680052.3U CN204261362U (en) 2014-11-14 2014-11-14 A kind of gathering-device of Rotary Evaporators volatile matter distillation oil

Publications (1)

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CN204261362U true CN204261362U (en) 2015-04-15

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112023430A (en) * 2019-06-03 2020-12-04 中石化南京化工研究院有限公司 Decoking method of chlorobenzene rectifying still liquid

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112023430A (en) * 2019-06-03 2020-12-04 中石化南京化工研究院有限公司 Decoking method of chlorobenzene rectifying still liquid
CN112023430B (en) * 2019-06-03 2022-06-21 中石化南京化工研究院有限公司 Decoking method of chlorobenzene rectifying still liquid

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Effective date of registration: 20211213

Address after: 723200 Liulin Town, Chenggu County, Hanzhong City, Shaanxi Province

Patentee after: Shaanxi Tiangu Pharmaceutical Co.,Ltd.

Address before: Room 10608, unit 1, building 6, Tsinghua Science Park, No. 65, Keji Second Road, high tech Zone, Xi'an, Shaanxi 710065

Patentee before: SHAANXI TEEGOO BIOTECHNOLOGY GROUP Co.,Ltd.