CN204233818U - A kind of high efficiency extraction separation device - Google Patents
A kind of high efficiency extraction separation device Download PDFInfo
- Publication number
- CN204233818U CN204233818U CN201420710763.0U CN201420710763U CN204233818U CN 204233818 U CN204233818 U CN 204233818U CN 201420710763 U CN201420710763 U CN 201420710763U CN 204233818 U CN204233818 U CN 204233818U
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- extraction flask
- extraction
- flask
- agitator
- condenser pipe
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Abstract
The utility model relates to a kind of high efficiency extraction separation device, comprise agitator, condenser pipe, first extraction flask and the second extraction flask, the inlet Inner edge co-axial seal of the second extraction flask connects the drain hole lower end outer rim of the first extraction flask, the top of the first extraction flask arranges an agitator, the puddler of agitator coaxially inserts in the charging aperture of the first extraction flask, and deeply to the middle and lower part of the first extraction flask, puddler outer rim radial direction installs paddle, coaxially a condenser pipe is installed respectively in two drains on the first extraction flask top, the root connection of described condenser pipe is shaped with a branch road charge pipe, the end co-axial seal sealing-plug of branch road charge pipe.In this device, extraction flask is pyramidal structure, be convenient to extract separatory, shorten disengaging time, its material is high boron glass, the high grade of transparency, can extraction process directly perceived, high boron glass low thermal expansion, high temperature resistant, high rigidity, high strength, acid and alkali-resistance, anticorrosive, do chemical stability, extend the service life of equipment.
Description
Technical field
The utility model belongs to chemical device field, especially a kind of high efficiency extraction separation device.
Background technology
Extraction is one of important chemical engineering unit operation, it is one of important means of purifying substance, its general principle utilizes the similar principle that mixes, utilize component in system to have different solubility to carry out the desired component of separation and concentration in a solvent, extraction is widely used in the fields such as chemistry, metallurgy, food, atomic energy industry.
The most frequently used is artificial shaking out, not only time-consuming but also require great effort, more cannot be competent at large batch of industrial extraction needs, extractant is generally the physical and mental health of harmful substance, crisis staff simultaneously.
Utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art part, provides a kind of high efficiency extraction separation device, and the extraction environment that this device provides is airtight, and operation automatic control, reduces environmental pollution and the harm to producers, saves manpower.
The utility model is that technical solution problem adopts following technical scheme:
A kind of high efficiency extraction separation device, comprise agitator, condenser pipe, the first extraction flask and the second extraction flask, the structure of the first and second extraction flasks is identical, top is shaped with charging aperture, bottom is shaped with discharge gate, discharge gate mounted valve, the extraction flask body of charging aperture both sides is communicated with and is shaped with two drains upwards; The inlet Inner edge co-axial seal of the second extraction flask connects the drain hole lower end outer rim of the first extraction flask, the top of the first extraction flask arranges an agitator, the puddler of agitator coaxially inserts in the charging aperture of the first extraction flask, and deeply to the middle and lower part of the first extraction flask, puddler outer rim radial direction installs paddle, coaxially a condenser pipe is installed respectively in two drains on the first extraction flask top, the root connection of described condenser pipe is shaped with a branch road charge pipe, the end co-axial seal sealing-plug of branch road charge pipe.
And described agitator has and rotates and reverse two kinds of selection modes.
Good effect of the present utility model is as follows:
1, in this device, extraction flask is pyramidal structure, be convenient to extract separatory, shorten disengaging time, its material is high boron glass, the high grade of transparency, can extraction process directly perceived, high boron glass low thermal expansion, high temperature resistant, high rigidity, high strength, acid and alkali-resistance, anticorrosive, do chemical stability, extend the service life of equipment.
2, this device electric mixer replaces artificial jolting, can forward and reversely stir, and shortens extraction time, ensures effect of extracting, improve extraction efficiency, meanwhile, the paddle of stirring motor is double-deck, and can mixing direction be converted, substantially increase extraction efficiency, shorten the process time.
3, all operations extraction space of this device is airtight, and operation automatic control, decreases environmental pollution and the harm to producers.
4, this device adopts two-stage extraction flask, ensures that separatory is complete, reduce the loss of target product after twice separating and extracting.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
Detailed description of the invention
Below in conjunction with accompanying drawing, also by specific embodiment, the utility model is described in further detail, and following examples are descriptive, are not determinate, can not limit protection domain of the present utility model with this.
A kind of high efficiency extraction separation device, comprise agitator 1, condenser pipe 2, first extraction flask 5 and the second extraction flask 7, the structure of the first and second extraction flasks is identical, top is shaped with charging aperture, bottom is shaped with discharge gate 6, discharge gate mounted valve, the extraction flask body of charging aperture both sides is communicated with and is shaped with two drains 8 upwards; Wherein, the inlet Inner edge co-axial seal of the second extraction flask connects the drain hole lower end outer rim of the first extraction flask, the top of the first extraction flask arranges an agitator, the puddler 4 of agitator coaxially inserts in the charging aperture of the first extraction flask, and deeply to the middle and lower part of the first extraction flask, puddler outer rim radial direction installs paddle, coaxially a condenser pipe is installed respectively in two drains on the first extraction flask top, the root connection of described condenser pipe is shaped with a branch road charge pipe 3, the end co-axial seal sealing-plug of branch road charge pipe.
Described agitator has and rotates and reverse two kinds of selection modes, can increase the agitating mode of paddle, make extraction quicker.
Puddler seals through the bottle mouth position plug of the first extraction flask.In order to ensure sealing, except the upper end open of condenser pipe, all exposed interfaces all adopt sealing-plug to seal.
The device of the application is adopted to carry out the case study on implementation 1 be separated
1, by CS
21500ml adds automatic first extraction flask in the branch road charge pipe of two condenser pipes, then adds acetaldehyde-H
3pO
4100ml, starts stirring, automatically controls by rotating forward 15 minutes-stop 30 seconds-reversion 15 minutes.So repeatedly, stir 2 hours, stratification.Lower floor's acid pickle is put into the second extraction flask, and secondary separatory, separates CS
2return the first extraction flask, with the CS in the first extraction flask
2be combined.
2, in the first extraction flask, acetaldehyde-H is added again
3pO
4400ml, repeats aforesaid operations three times, each stirring 1 hour.
3, the CS separated
2be placed in the first extraction flask, add 2000ml water, start stirring, by rotating forward 15 minutes-stop 30 seconds-reversion automatic control in 15 minutes.1 hour and so forth, stratification.By subnatant CS
2put into second point of flow container, again separatory, the residual water layer separated, discards the waste water in the first extraction flask, CS
2again be placed in the first extraction flask, add 2000ml water, start stirring and repeat aforesaid operations again three times, obtain crude product CS
2.
4, by crude product CS
2rectifying, obtains finished product CS
21050ml productive rate 70%, analyze through GC, wherein benzene content is 1ppm, and wherein, benzene feedstock content is 700ppm.
The device of the application is adopted to carry out the case study on implementation 2 be separated
1, by CS
21500ml adds the first extraction flask, then adds acetaldehyde-H
3pO
4100ml, starts stirring, by rotating forward 15 minutes-stop 30 seconds-rotate forward automatic control in 15 minutes.Operation like this, stirs 2 hours, stratification.Lower floor's acid pickle is put into secondary and divides flow container, secondary separatory, separates CS
2return the first extraction flask, be combined with the CS2 in the first extraction flask.
2, in the first extraction flask, acetaldehyde-H is added
3pO
4400ml, repeats aforesaid operations three times, each stirring 1 hour.
3, CS is separated
2be placed in the first extraction flask, add 2000ml water, start stirring, by rotating forward 15 minutes-stop 30 seconds-rotate forward automatic control in 15 minutes.Operation like this, stir 1 hour, stratification, by subnatant CS
2put into secondary and divide flow container, again separatory, the residual water layer separated, discards the waste water in the first extraction flask, by above-mentioned CS
2again be placed in the first extraction flask, add 2000ml water.Start stirring and repeat aforesaid operations again three times, obtain crude product CS2.
4, by crude product CS
2rectifying, obtains finished product CS21100ml productive rate 73%, and analyzing wherein benzene content through GC is 100ppm, and benzene feedstock content is 700ppm.
Claims (2)
1. a high efficiency extraction separation device, it is characterized in that: comprise agitator, condenser pipe, the first extraction flask and the second extraction flask, the structure of the first and second extraction flasks is identical, top is shaped with charging aperture, bottom is shaped with discharge gate, discharge gate mounted valve, the extraction flask body of charging aperture both sides is communicated with and is shaped with two drains upwards; The inlet Inner edge co-axial seal of the second extraction flask connects the drain hole lower end outer rim of the first extraction flask, the top of the first extraction flask arranges an agitator, the puddler of agitator coaxially inserts in the charging aperture of the first extraction flask, and deeply to the middle and lower part of the first extraction flask, puddler outer rim radial direction installs paddle, coaxially a condenser pipe is installed respectively in two drains on the first extraction flask top, the root connection of described condenser pipe is shaped with a branch road charge pipe, the end co-axial seal sealing-plug of branch road charge pipe.
2. high efficiency extraction separation device according to claim 1, is characterized in that: described agitator has and rotates and reverse two kinds of selection modes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420710763.0U CN204233818U (en) | 2014-11-24 | 2014-11-24 | A kind of high efficiency extraction separation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420710763.0U CN204233818U (en) | 2014-11-24 | 2014-11-24 | A kind of high efficiency extraction separation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204233818U true CN204233818U (en) | 2015-04-01 |
Family
ID=52763374
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420710763.0U Expired - Fee Related CN204233818U (en) | 2014-11-24 | 2014-11-24 | A kind of high efficiency extraction separation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204233818U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107224752A (en) * | 2017-07-31 | 2017-10-03 | 赣州市恒源科技股份有限公司 | A kind of extraction equipment |
| CN111803978A (en) * | 2020-09-01 | 2020-10-23 | 赛默飞世尔（上海）仪器有限公司 | Solvent evaporation device and solvent evaporation system |
-
2014
- 2014-11-24 CN CN201420710763.0U patent/CN204233818U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107224752A (en) * | 2017-07-31 | 2017-10-03 | 赣州市恒源科技股份有限公司 | A kind of extraction equipment |
| CN111803978A (en) * | 2020-09-01 | 2020-10-23 | 赛默飞世尔（上海）仪器有限公司 | Solvent evaporation device and solvent evaporation system |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150401 Termination date: 20151124 |