CN204208540U - Based on the C of acetylene in a kind of PVC production process 2h 3cl synthesizer - Google Patents

Based on the C of acetylene in a kind of PVC production process 2h 3cl synthesizer Download PDF

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Publication number
CN204208540U
CN204208540U CN201420582315.7U CN201420582315U CN204208540U CN 204208540 U CN204208540 U CN 204208540U CN 201420582315 U CN201420582315 U CN 201420582315U CN 204208540 U CN204208540 U CN 204208540U
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China
Prior art keywords
inlet pipe
gas inlet
skirt
acetylene
main gas
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CN201420582315.7U
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钟鹤岩
熊俊
彭贤清
邱艳东
周瑶文
马雪峰
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QINGHAI YIHUA CHEMICAL CO Ltd
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QINGHAI YIHUA CHEMICAL CO Ltd
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Abstract

Based on the C of acetylene in a kind of PVC production process 2h 3cl synthesizer, comprise mixing arrangement and reforming unit, described mixing arrangement comprises main gas inlet pipe, the circumference of main gas inlet pipe connects the auxiliary gas inlet pipe of some tapers, the wealthy mouth of each auxiliary gas inlet pipe connects auxiliary gas generator, slot is connected to the sidewall of main gas inlet pipe, one end of main gas inlet pipe connects main gas generator, the other end connects the wealthy mouth of the skirt of taper, the slot of skirt is connected to mixed gas storehouse, described reforming unit comprises bobbin carriage, some catalytic bed dividing plates are had in bobbin carriage, the conversion tube device be communicated with the escape pipe in mixed gas storehouse is furnished with between adjacent catalytic bed dividing plate, the utility model mixing arrangement can make gas and vapor permeation even, mixing rate is fast, in reforming unit, distribution of gas is even, without Biased flow phenomenon, and the contact between mist and catalyst can be made even, can catalyst in saveall, promote changing effect simultaneously.

Description

Based on the C of acetylene in a kind of PVC production process 2h 3cl synthesizer
Technical field
The utility model belongs to calcium carbide applied technical field, particularly in a kind of PVC production process based on the C of acetylene 2h 3cl synthesizer.
Background technology
Acetylene is the synthesis material of many chemical products, and such as acetaldehyde, acetic acid, benzene, vinyl chloride, synthetic rubber, synthetic fibers etc., wherein, synthesize C with HCl acting in conjunction 2h 3cl is one of its important use, in synthesis, main technique is gas and vapor permeation and conversion, in prior art, gas and vapor permeation passes into gas respectively by two pipelines, make its natural diffuseness mixing in mixing chamber, this mode efficiency is lower, and be difficult to mix, and in reforming unit, generally adopt distributing plate structure, easily producing bias current causes distribution of gas poor effect, cause catalyst attrition excessive, and whole mists is in reforming unit, uneven with catalyst exposure, cause changing effect poor.
Summary of the invention
In order to overcome the shortcoming of above-mentioned prior art, the purpose of this utility model is to provide the C based on acetylene in a kind of PVC production process 2h 3cl synthesizer, the uneven problem occurred in mixed gas being solved preferably and transforming.
To achieve these goals, the technical solution adopted in the utility model is:
Based on the C of acetylene in a kind of PVC production process 2h 3cl synthesizer, comprise mixing arrangement and reforming unit, described mixing arrangement comprises main gas inlet pipe 11, the circumference of main gas inlet pipe 11 connects the auxiliary gas inlet pipe 12 of some tapers, the wealthy mouth of each auxiliary gas inlet pipe 12 connects auxiliary gas generator, slot is connected to the sidewall of main gas inlet pipe 11, one end of main gas inlet pipe 11 connects main gas generator, the other end connects the wealthy mouth of the skirt 13 of taper, the slot of skirt 13 is connected to mixed gas storehouse 15, described reforming unit comprises bobbin carriage 26, some catalytic bed dividing plates 24 are had in bobbin carriage 23, the conversion tube device be communicated with the escape pipe 16 in mixed gas storehouse 15 is furnished with between adjacent catalytic bed dividing plate 24.
Described conversion tube device comprises a band ring pipe 21 jaggy, multiple straight tube 22 is vertically connected on ring pipe 21, and be communicated with ring pipe 21, ring pipe 21 is communicated with escape pipe 16 by gaseous mixture air inlet pipe 25 simultaneously, the breach end of wherein said ring pipe 21 is closed with plug, the two ends of each straight tube 22 are also closed with plug, and ring pipe 21 and straight tube 22 are provided with the pore 23 being with stifled son.
Be furnished with baffle plate 14 in described mixed gas storehouse 15, the unsettled setting of baffle plate 14, just to the slot of skirt 13.
Described main gas inlet pipe 11 and skirt 13 respectively have two, and two skirts 13 are positioned opposite on mixed gas storehouse 15, and slot end is all just to baffle plate 14, and the bottom in mixed gas storehouse 15 is provided with deslagging outlet 17.
Described main gas inlet pipe 11 and skirt 13 respectively have multiple, are distributed in the same side in mixed gas storehouse 15, and the slot end of each skirt 13 is all just to baffle plate 14.
The outlet conduit of described auxiliary gas generator is provided with air pump.
Compared with prior art, the utility model mixing arrangement can make gas and vapor permeation even, and mixing rate is fast, in reforming unit, distribution of gas is even, without Biased flow phenomenon, and the contact between mist and catalyst can be made even, can catalyst in saveall, promote changing effect simultaneously.
Accompanying drawing explanation
Fig. 1 is the utility model structural representation.
Fig. 2 is the utility model conversion tube device top view.
Detailed description of the invention
Embodiment of the present utility model is described in detail below in conjunction with drawings and Examples.
Embodiment 1
As shown in Figure 1, in a kind of PVC production process based on the C of acetylene 2h 3cl synthesizer, comprise mixing arrangement and reforming unit, described mixing arrangement comprises main gas inlet pipe 11, the circumference of main gas inlet pipe 11 connects the auxiliary gas inlet pipe 12 of some tapers, the wealthy mouth of each auxiliary gas inlet pipe 12 connects auxiliary gas generator, slot is connected to the sidewall of main gas inlet pipe 11, one end of main gas inlet pipe 11 connects main gas generator, the other end connects the wealthy mouth of the skirt 13 of taper, the slot of skirt 13 is connected to mixed gas storehouse 15, described reforming unit comprises bobbin carriage 26, some catalytic bed dividing plates 24 are had in bobbin carriage 23, the conversion tube device be communicated with the escape pipe 16 in mixed gas storehouse 15 is furnished with between adjacent catalytic bed dividing plate 24.
As shown in Figure 2, conversion tube device comprises a band ring pipe 21 jaggy, multiple straight tube 22 is vertically connected on ring pipe 21, and be communicated with ring pipe 21, ring pipe 21 is communicated with escape pipe 16 by gaseous mixture air inlet pipe 25 simultaneously, the breach end of wherein said ring pipe 21 is closed with plug, and the two ends of each straight tube 22 are also closed with plug, and ring pipe 21 and straight tube 22 are provided with the pore 23 being with stifled son.
According to this device, namely acetylene mixes in main gas inlet pipe 11 with HCl gas, because auxiliary gas inlet pipe 12 is pyramidal structure, therefore, pressure increase when entering, good mixed effect can be played, skirt 13 again through taper enters mixed gas storehouse 15, and pressure increases further, after entering, pressure is rapid drop again, and the repeatedly change of pressure can make mixed effect better.Afterwards, mist enters into each ring pipe 21 by escape pipe 16, is then again disperseed by straight tube 22, eventually through each pore 23 by distribution of gas between catalytic bed, make mist and catalyst can produce good contact, promote changing effect.The length of straight tube 22 can be arranged according to the distance between adjacent catalytic bed dividing plate 24, ensures packing space to greatest extent, gas uniform is distributed.Simultaneously can select open some stifled sons according to actual conditions, shed situation to adjust gas.
Embodiment 2
As shown in Figure 1, agent structure is consistent with embodiment 1, and difference is, be furnished with baffle plate 14 in mixed gas storehouse 15, the unsettled setting of baffle plate 14, just to the slot of skirt 13.Main gas inlet pipe 11 and skirt 13 respectively have two, and two skirts 13 are positioned opposite on mixed gas storehouse 15, and slot end is all just to baffle plate 14, and the bottom in mixed gas storehouse 15 is provided with deslagging outlet 17.
Utilize this structure, the air inflow in mixing arrangement can be increased, and the mist entered is under the effect of baffle plate 14, can spread further, some particles (particulate that mainly may exist in industrial acetylene) in gas then can precipitated get off, and discharge eventually through deslagging outlet 17.
Embodiment 3
Agent structure is consistent with embodiment 1, and difference is, main gas inlet pipe 11 and skirt 13 respectively have multiple, is distributed in the same side in mixed gas storehouse 15, and the slot end of each skirt 13 is all just to baffle plate 14.In this structure, principle is similar to Example 2.
Embodiment 4
Agent structure is consistent with embodiment 1, and difference is, the outlet conduit of auxiliary gas generator is provided with air pump, can improve pressure by manual control, optimize mixed effect when auxiliary atmospheric pressure is not enough.

Claims (6)

1. in a PVC production process based on the C of acetylene 2h 3cl synthesizer, comprise mixing arrangement and reforming unit, it is characterized in that, described mixing arrangement comprises main gas inlet pipe (11), the circumference of main gas inlet pipe (11) connects the auxiliary gas inlet pipe (12) of some tapers, the wealthy mouth of each auxiliary gas inlet pipe (12) connects auxiliary gas generator, slot is connected to the sidewall of main gas inlet pipe (11), one end of main gas inlet pipe (11) connects main gas generator, the other end connects the wealthy mouth of the skirt (13) of taper, the slot of skirt (13) is connected to mixed gas storehouse (15), described reforming unit comprises bobbin carriage (26), some catalytic bed dividing plates (24) are had in bobbin carriage (23), the conversion tube device be communicated with the escape pipe (16) of mixed gas storehouse (15) is furnished with between adjacent catalytic bed dividing plate (24).
2. in PVC production process according to claim 1 based on the C of acetylene 2h 3cl synthesizer, it is characterized in that, described conversion tube device comprises band ring pipe jaggy (21), multiple straight tube (22) is vertically connected on ring pipe (21), and be communicated with ring pipe (21), ring pipe (21) is communicated with escape pipe (16) by gaseous mixture air inlet pipe (25) simultaneously, the breach end of wherein said ring pipe (21) is closed with plug, the two ends of each straight tube (22) are also closed with plug, and ring pipe (21) and straight tube (22) are provided with the pore (23) being with stifled son.
3. in PVC production process according to claim 1 based on the C of acetylene 2h 3cl synthesizer, is characterized in that, be furnished with baffle plate (14) in described mixed gas storehouse (15), baffle plate (14) unsettled setting, just to the slot of skirt (13).
4. in PVC production process according to claim 1 based on the C of acetylene 2h 3cl synthesizer, it is characterized in that, described main gas inlet pipe (11) and skirt (13) respectively have two, two skirts (13) are positioned opposite on mixed gas storehouse (15), slot end is all just to baffle plate (14), and the bottom in mixed gas storehouse (15) is provided with deslagging outlet (17).
5. in PVC production process according to claim 1 based on the C of acetylene 2h 3cl synthesizer, it is characterized in that, described main gas inlet pipe (11) and skirt (13) respectively have multiple, are distributed in the same side of mixed gas storehouse (15), and the slot end of each skirt (13) is all just to baffle plate (14).
6. in PVC production process according to claim 1 based on the C of acetylene 2h 3cl synthesizer, is characterized in that, the outlet conduit of described auxiliary gas generator is provided with air pump.
CN201420582315.7U 2014-10-09 2014-10-09 Based on the C of acetylene in a kind of PVC production process 2h 3cl synthesizer Active CN204208540U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109772236A (en) * 2017-11-14 2019-05-21 中国石油化工股份有限公司 A kind of fluid distributor, reaction unit and its application

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109772236A (en) * 2017-11-14 2019-05-21 中国石油化工股份有限公司 A kind of fluid distributor, reaction unit and its application
KR20200085863A (en) * 2017-11-14 2020-07-15 차이나 페트로리움 앤드 케미컬 코포레이션 Fluid distributors, reaction devices and applications thereof
CN109772236B (en) * 2017-11-14 2022-08-12 中国石油化工股份有限公司 Fluid distributor, reaction device and application thereof
US11571673B2 (en) 2017-11-14 2023-02-07 China Petroleum & Chemical Corporation Fluid distributor, reaction device and application thereof
TWI800556B (en) * 2017-11-14 2023-05-01 大陸商中國石油化工科技開發有限公司 A kind of fluid distributor, reaction device and application thereof
KR102536047B1 (en) 2017-11-14 2023-05-23 차이나 페트로리움 앤드 케미컬 코포레이션 Fluid distributor, reaction device and application thereof

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