CN204161889U - A kind of storage tank anti-clogging breather apparatus - Google Patents
A kind of storage tank anti-clogging breather apparatus Download PDFInfo
- Publication number
- CN204161889U CN204161889U CN201420600826.7U CN201420600826U CN204161889U CN 204161889 U CN204161889 U CN 204161889U CN 201420600826 U CN201420600826 U CN 201420600826U CN 204161889 U CN204161889 U CN 204161889U
- Authority
- CN
- China
- Prior art keywords
- breather
- drying chamber
- tank
- clogging
- storage tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000001035 drying Methods 0.000 claims abstract description 38
- 239000002245 particle Substances 0.000 claims abstract description 27
- 238000007689 inspection Methods 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract description 20
- 239000007789 gas Substances 0.000 abstract description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 7
- 239000000741 silica gel Substances 0.000 abstract description 7
- 229910002027 silica gel Inorganic materials 0.000 abstract description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract description 6
- 239000002274 desiccant Substances 0.000 abstract description 6
- 238000010438 heat treatment Methods 0.000 abstract description 6
- 230000029058 respiratory gaseous exchange Effects 0.000 abstract description 5
- 241001062009 Indigofera Species 0.000 abstract description 3
- 238000005260 corrosion Methods 0.000 abstract description 3
- 230000007797 corrosion Effects 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000007599 discharging Methods 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 description 18
- 238000010521 absorption reaction Methods 0.000 description 12
- 239000000463 material Substances 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 239000001117 sulphuric acid Substances 0.000 description 2
- 235000011149 sulphuric acid Nutrition 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000005530 etching Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
Landscapes
- Drying Of Solid Materials (AREA)
Abstract
A kind of storage tank anti-clogging breather apparatus, comprise breather tank and drying chamber, breather tank and drying chamber are interconnected.The beneficial effects of the utility model are: the tourie that the utility model is arranged can absorb titanium tetrachloride gases in expiratory air by actv., the gas of discharging breather apparatus is made to meet emission request, meanwhile, titanium tetrachloride product can be collected further, improve the production efficiency of titanium tetrachloride.Drying chamber prevents moisture in outside air to contact with the titanium tetrachloride gases in pipeline, reduces the corrosion of hydrochloric acid to equipment, and the situation simultaneously avoiding breathing pipeline to block occurs.Inspection door can be used for the color change of discolour silica gel particle.When silica gel particle color is reddened by indigo plant, in heating coil, pass into steam, control steam supply amount by humidostat, to remove the moisture that desiccant absorbs, enable desiccant repeated usage, decrease the replacing frequency of desiccant, reduce labour intensity and the replacement cost of workman.
Description
Technical field
The utility model relates to a kind of for the breather apparatus in titanic chloride production process, especially a kind of storage tank anti-clogging breather apparatus.
Background technology
In titanium tetrachloride is produced, in order to keep the pressure stability in each storage tank (technique groove tank), making the pressure of whole system be in state of equilibrium, usually breather apparatus can be set on each groove tank.When output material enters tank body, the gas in tank is discharged from tank body in time by breather apparatus; Discharge when storing material in tank, tank internal pressure is lower than tank external pressure, and the air outside tank or the material in breather apparatus then can be back in storage tank, to balance the pressure in tank body.
Titanium tetrachloride enters a small amount of titanium tetrachloride smoke of carrying secretly in the material of each technology groove tank and to be mixed in tank in gas when producing, therefore it directly can not be discharged into outside tank body, the moisture that simultaneously titanium tetrachloride runs in air reaction can produce hydrated titanium dioxide and hydrochloric acid rapidly, blocking breathing pipeline etching apparatus.At present, usually can arrange the concentrated sulphuric acid or titanium tetrachloride absorption liquid are housed in titanium tetrachloride is produced.When using titanium tetrachloride absorption liquid, often there is breathing pipeline blockage problem.When using concentrated sulphuric acid absorption liquid, require higher to the resistance to corrosion of equipment, when occurring building the pressure and emitting groove, the personnel that also easily cause injure.Therefore need to invent these problems that a kind of new breather apparatus solves existing installation existence.
Utility model content
Technical problem to be solved in the utility model is to provide a kind of storage tank anti-clogging breather apparatus, to solve the blocking of existing installation breathing pipe Louis, the low problem of safety.
The technical scheme of the utility model technical solution problem is: a kind of storage tank anti-clogging breather apparatus, and comprise breather tank and drying chamber, breather tank is provided with air inlet pipe, vent, and drying chamber is provided with upper vent, lower vent.Vent is positioned at the top of breather tank.Upper vent is positioned at the top of drying chamber, and lower vent is positioned at the bottom of drying chamber.The vent of breather tank and the upper vent of drying chamber are interconnected by connecting tube.
Air inlet pipe inserts from the top of breather tank and extends in breather tank, and bottom does not contact with breather tank.Breather tank is provided with outgate.Breather tank bottom is provided with discharge gate.
In connecting tube, ball valve is installed.
Be conical bottom drying chamber, lower vent is located at the side bottom cone.Bottom drying chamber, water back is housed, water back is connected with humidostat.Drying chamber is provided with inspection door.Drying chamber is built with dried particles.The bottom of drying chamber is provided with dried particles discharge gate.
The beneficial effects of the utility model are: the tourie that the utility model is arranged can absorb titanium tetrachloride gases in expiratory air by actv., the gas of discharging breather apparatus is made to meet emission request, meanwhile, titanium tetrachloride product can be collected further, improve the production efficiency of titanium tetrachloride.Drying chamber prevents moisture in outside air to contact with the titanium tetrachloride gases in pipeline, reduces the corrosion of hydrochloric acid to equipment, and the situation simultaneously avoiding breathing pipeline to block occurs.Inspection door can be used for the color change of discolour silica gel particle.When silica gel particle color is reddened by indigo plant, in heating coil, pass into steam, control steam supply amount by humidostat, to remove the moisture that desiccant absorbs, enable desiccant repeated usage, decrease the replacing frequency of desiccant, reduce labour intensity and the replacement cost of workman.
Accompanying drawing explanation
Fig. 1 is the utility model structural representation.
Description of reference numerals: 1 air inlet pipe, 2 vents, 3 material-feeding ports, 4 outgates, 5 discharge gates, 6 upper vents, 7 times vents, 8 dried particles add entrance, 9 dried particles discharge gates, 10 inspection doors, 11 heating coils, 12 humidostats, connecting tube 13, ball valve 14.
Detailed description of the invention
Below in conjunction with accompanying drawing 1, the utility model is described in further detail.
A kind of storage tank anti-clogging breather apparatus, comprising: breather tank, drying chamber, connecting tube 13.
Breather tank is installed on air inlet pipe 1, offers vent 2, material-feeding port 3, outgate 4, discharge gate 5.
In breather tank, absorption liquid is housed, absorption liquid is titanium tetrachloride liquid.Air inlet pipe 1 is inserted into from the top of breather tank in breather tank and also extends under absorption liquid liquid level always, does not contact with breather tank bottom air inlet pipe 1.Vent 2 is positioned at the top of breather tank.Outgate 4 is opened on the sidewall on breather tank, and outgate 4 is connected with liquid collection tank.Discharge gate 5 is opened in the position near bottom on the sidewall on breather tank, and discharge gate 5 is provided with manually-operated gate.The electrolyte level of absorption liquid will lower than outgate 4 height.
Drying chamber the first half is for conical bottom cylindrical, the latter half.Drying chamber is built with dried particles, and dried particles is calcium chloride and discolour silica gel particle.Dried particles is all positioned at drying chamber conical section.
Drying chamber offers upper vent 6, lower vent 7, dried particles add entrance 8, dried particles discharge gate 9, inspection door 10, heating coil 11 is installed.
Lower vent 7 and inspection door 10 are opened in the side of drying chamber conical portion.Dried particles discharge gate 9 is positioned at bottom drying chamber conical portion.Water back 11 is arranged on the inwall of drying chamber conical portion, can install the water back 11 that quantity is applicable to as required.Every bar water back 11 is all connected with humidostat 12.Upper vent 6, dried particles add the top that entrance 8 is positioned at drying chamber.
Two ports of connecting tube 13 are connected with vent 2, upper vent 6 respectively, are provided with ball valve 14 in connecting tube 13.
When storage tank charging, tidal air in tank enters into tourie by the air inlet pipe 1 on tourie, air inlet pipe 1 outlet extend into below titanium tetrachloride absorption liquid liquid level, after titanium tetrachloride gases in tidal air absorbs by the absorption liquid in tank, the vent 2 of residual gas on tourie enters drying chamber through connecting tube 13 from the upper vent 6 drying chamber, eventually passes through dried particles and is discharged in air from lower vent 7.
When storage tank discharge, the air outside tank, by the lower vent 7 bottom drying chamber, enters into drying chamber, after dewatering, from drying chamber upper vent 6 through connecting tube 13, enters tourie afterwards from the vent 2 tourie through dried particles.When absorption liquid liquid level exports higher than air inlet pipe 1, in tourie, titanium tetrachloride absorption liquid is pushed back in storage tank; When absorption liquid liquid level exports lower than air inlet pipe 1, tank outer air fills in storage tank in time.
When after dried particles water suction too much, the color relation of discolour silica gel particle wherein can be reddened by indigo plant, at this moment just needs to remove the moisture in dried particles.When dewatering, open dried particles and add entrance 8 start-up temperature adjusting apparatus 12 and control the temperature of heating pipe to 11, the temperature of heating pipe to 11 is remained between 200 to 260 degree.When discolour silica gel particle color relation can by red stain basket after, just illustrate that dried particles thoroughly dewaters, and can reuse.The color change of dried particles can pass through inspection door 10 real-time monitored.
Claims (10)
1. a storage tank anti-clogging breather apparatus, comprises breather tank and drying chamber, and described breather tank is provided with air inlet pipe, vent, and described drying chamber is provided with upper vent, lower vent, it is characterized in that: described vent (2) is positioned at the top of breather tank; Described upper vent (6) is positioned at the top of drying chamber, and described lower vent (7) is positioned at the bottom of drying chamber; The vent (2) of described breather tank and the upper vent (6) of drying chamber are interconnected by connecting tube (14).
2. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: described air inlet pipe (1) inserts from the top of breather tank and extends in breather tank, and bottom does not contact with breather tank.
3. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: described breather tank is provided with outgate (4).
4. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: described breather tank bottom is provided with discharge gate (5).
5. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: be provided with ball valve (13) in described connecting tube (14).
6. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: for conical bottom described drying chamber, described lower vent (7) is located at the side bottom cone.
7. a kind of storage tank anti-clogging breather apparatus according to claim 1, it is characterized in that: water back (11) is housed bottom described drying chamber, described water back (11) is connected with humidostat (12).
8. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: described drying chamber is provided with inspection door (10).
9. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: described drying chamber is built with dried particles.
10. a kind of storage tank anti-clogging breather apparatus according to claim 1, is characterized in that: the bottom of described drying chamber is provided with dried particles discharge gate (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420600826.7U CN204161889U (en) | 2014-10-17 | 2014-10-17 | A kind of storage tank anti-clogging breather apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420600826.7U CN204161889U (en) | 2014-10-17 | 2014-10-17 | A kind of storage tank anti-clogging breather apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204161889U true CN204161889U (en) | 2015-02-18 |
Family
ID=52535600
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420600826.7U Expired - Fee Related CN204161889U (en) | 2014-10-17 | 2014-10-17 | A kind of storage tank anti-clogging breather apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204161889U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105059771A (en) * | 2015-08-06 | 2015-11-18 | 安徽中创电子信息材料有限公司 | High-purity titanium tetrachloride storage device |
| CN110180364A (en) * | 2019-06-28 | 2019-08-30 | 金川集团股份有限公司 | A kind of device and its application method adjusting titanium tetrachloride reservoir pressure |
-
2014
- 2014-10-17 CN CN201420600826.7U patent/CN204161889U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105059771A (en) * | 2015-08-06 | 2015-11-18 | 安徽中创电子信息材料有限公司 | High-purity titanium tetrachloride storage device |
| CN110180364A (en) * | 2019-06-28 | 2019-08-30 | 金川集团股份有限公司 | A kind of device and its application method adjusting titanium tetrachloride reservoir pressure |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150218 |