CN204154602U - A kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument - Google Patents

A kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument Download PDF

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Publication number
CN204154602U
CN204154602U CN201420569474.3U CN201420569474U CN204154602U CN 204154602 U CN204154602 U CN 204154602U CN 201420569474 U CN201420569474 U CN 201420569474U CN 204154602 U CN204154602 U CN 204154602U
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China
Prior art keywords
photoelectricity
container
coefficient
base
viscosity
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Expired - Fee Related
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CN201420569474.3U
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Chinese (zh)
Inventor
刘家菊
洪炜宁
钱良存
李满兰
袁兴红
吴志鹏
解彬彬
张凌峰
杨文超
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Anhui Agricultural University AHAU
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Anhui Agricultural University AHAU
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Abstract

The utility model discloses a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, include coefficient of viscosity tester, thermostatic control water tank, photoelectricity gate control circuit; Coefficient of viscosity tester includes base of measuring equipment, interconnective DC voltage-stabilizing module, photoelectricity gate control circuit are installed in base of measuring equipment, the middle part of base of measuring equipment is provided with the container, the spirit-leveling instrument that hold testing liquid, the stopper of container top is inserted with temperature-sensing probe in container, and the stopper circle centre position of container top has a circular hole; The base of measuring equipment being positioned at the both sides of container is installed respectively the support indicating millimeter scale, two stands is provided with the transmitting terminal of photoelectricity door one, two and the receiving end of photoelectricity door one, two respectively by the vernier scale of 50 calibration.The utility model uses the vernier caliper measurement small ball working time of 50 calibration, uses photoelectricity door to trigger millisecond meter and carries out timing, avoid people to be the error caused, substantially increase the degree of accuracy of experiment.

Description

A kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument
Technical field
The utility model relates generally to Experiment of College Physics device field, particularly relates to a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument.
Background technology
When there being relative motion in liquid between each several part, there is internal friction between surface of contact, hinder the relative motion of liquid, this character is called the glutinousness of liquid, and the internal friction of liquid is called viscous force.The size of viscous force is directly proportional to the velocity gradient at surface of contact area and surface of contact place, and scale-up factor η is called viscosity (or coefficient of viscosity).
To the research of fluid viscosity at fluid mechanics, chemical, medical treatment, the fields such as water conservancy are all widely used, such as, with will according to the flow of conveying liquid during Cemented filling liquid, pressure differential, fed distance and liquid viscosity, the bore of design conveyance conduit.Measure liquid viscosity and can use falling ball method, capillary tube technique, the methods such as rotating-cylinder method, wherein falling ball method is applicable to measure the higher liquid of viscosity.The size of viscosity depends on character and the temperature of liquid, and temperature raises, and viscosity will reduce rapidly.Such as castor oil, near room temperature temperature change 1 DEG C, viscosity number changes about 10%.Therefore, measuring liquid has very large practical significance in the viscosity of different temperatures, for the viscosity of Measurement accuracy liquid, and must liquid with precise control temperature.
Utility model content
The utility model object is exactly the defect in order to make up prior art, provides a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument.
The utility model is achieved through the following technical solutions:
A kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, is characterized in that: include coefficient of viscosity tester, thermostatic control water tank, photoelectricity gate control circuit, described coefficient of viscosity tester includes base of measuring equipment, interconnective DC voltage-stabilizing module is installed in base of measuring equipment, photoelectricity gate control circuit, base of measuring equipment upper surface is provided with power switch, with the power supply base one of fuse, digital display timer, with power supply base one and the DC voltage-stabilizing model calling of fuse, the middle part of base of measuring equipment is provided with the container holding testing liquid, spirit-leveling instrument, container upper, the sidewall of lower end is respectively equipped with water inlet, water delivering orifice, the stopper of container top is inserted with temperature-sensing probe in container, the stopper circle centre position of container top has a circular hole, the base of measuring equipment being positioned at the both sides of container is installed respectively the support indicating millimeter scale, two stands is equipped with the track moved up and down for photoelectricity door one, two, two stands is respectively equipped with the transmitting terminal of photoelectricity door one, two and the receiving end of photoelectricity door one, two, transmitting terminal, the receiving end place of photoelectricity door one, two are arranged on corresponding support respectively by the vernier scale of 50 calibration, described photoelectricity gate control circuit includes CD4011 chip, the voltage input end of DC voltage-stabilizing module connects the transformer that 220V becomes 6V, the voltage output end photoelectricity door one in parallel of DC voltage-stabilizing module, photoelectricity door two, photoelectricity door one, two and digital display timer are connected with CD4011 chip respectively, described thermostatic control water tank is provided with filler, the front panel of thermostatic control water tank is provided with gauge glass, two binding posts, temperature detect switch (TDS), the rear panel of thermostatic control water tank is provided with water delivering orifice, water inlet, gap, power supply base two with fuse, radiator fan, high power voltage stabilized power source is provided with in thermostatic control water tank, master controller, heating plate, cooling piece, the signal input part of master controller is connected with temperature-sensing probe by two binding posts, the signal output part control linkage high power voltage stabilized power source of master controller, high power voltage stabilized power source and heating plate, cooling piece connects, the water inlet of described container, the water delivering orifice of water delivering orifice and thermostatic control water tank, water inlet connects.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, is characterized in that: described digital display timer is provided with timer reset key.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, is characterized in that: the pipeline between described container and constant temperature water tank is provided with water pump, forms circulation waterway.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, it is characterized in that: the back side of described base of measuring equipment adopts dismountable panel, the lower surface of base of measuring equipment is provided with four adjustment screws, regulates four to adjust screw and makes tester be in vertical state.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, it is characterized in that: the Measuring Time scope 0.001s ~ 99.999s of described digital display timer, photoelectricity door one triggered timer is used to start timing, photoelectricity door two triggered timer time out, the time of digital display timer display is the time interval that little firm ball warp crosses two photoelectricity doors.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, is characterized in that: the utilizing emitted light of the transmitting terminal of described photoelectricity door one, two is red visible laser, and utilizing emitted light aperture is 0.9mm, aligns with the vernier scale zero graduation of 50 calibration in the unthreaded hole center of circle.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, it is characterized in that: the receiving end of described photoelectricity door one, two is NPN open type, receiving end central point aligns with the vernier scale zero graduation of 50 calibration, and at receiving end, LED and hummer have been installed, LED is connected with CD4011 chip with hummer; When laser-correlation receiving end, LED is bright, and when receiving end is blocked, LED is gone out, buzzer call.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, is characterized in that: the described container holding testing liquid is double layer light transmission glass material container.
Described a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, is characterized in that: described Circularhole diameter is 2.2mm, is that the center of the small ball testing liquid in a reservoir of about 2mm falls for making diameter.
Photoelectricity gate control circuit of the present utility model, primarily of the circuit of the element welding such as transformer, DC voltage-stabilizing module, photoelectricity door one, photoelectricity door two, CD4011 chip, hummer, is used for controlling timer initiation timing and stopping timing.CD4011 chip is four identical Sheffer stroke gate compositions, controls timer, sound, phototiming instruction.Photoelectricity door one and photoelectricity door two are made up of transmitting terminal and receiving end, when bead is through photoelectricity door one, produce high level pulse triggered timer and start timing, LED is bright, and hummer rings, when bead is through photoelectricity door two, produce high level pulse triggered timer and stop timing, LED is bright, and hummer rings, read the time of timer display, be the time of bead through two photoelectricity door spacing.
The utility model has the advantages that:
The utility model uses the vernier caliper measurement small ball working time of 50 calibration, uses photoelectricity door to trigger millisecond meter and carries out timing, avoid people to be the error caused, substantially increase the degree of accuracy of experiment.
Accompanying drawing explanation
Fig. 1 is the structural representation of coefficient of viscosity tester of the present utility model.
Fig. 2 is the structural representation of thermostatic control water tank of the present utility model.
Fig. 3 is the structural representation of the rear panel of thermostatic control water tank of the present utility model.
Fig. 4 is the circuit diagram of photoelectricity gate control circuit of the present utility model.
Embodiment
As Figure 1-4, a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument, includes coefficient of viscosity tester, thermostatic control water tank 19, photoelectricity gate control circuit;
Coefficient of viscosity tester includes base of measuring equipment 3, interconnective DC voltage-stabilizing module 29 is installed in base of measuring equipment 3, photoelectricity gate control circuit, base of measuring equipment 3 upper surface is provided with power switch 1, with the power supply base 2 of fuse, digital display timer 6, power supply base 2 with fuse is connected with DC voltage-stabilizing module 29, the middle part of base of measuring equipment 3 is provided with the container 14 holding testing liquid, spirit-leveling instrument 5, container 14 upper, the sidewall of lower end is respectively equipped with water inlet 15, water delivering orifice 16, the stopper at container 14 top is inserted with temperature-sensing probe 17 in container, the stopper circle centre position at container 14 top has a circular hole 18, the base of measuring equipment 3 being positioned at the both sides of container 14 is installed respectively the support 8 indicating millimeter scale, two stands 8 is equipped with the track moved up and down for photoelectricity door one, two, two stands 8 is respectively equipped with the transmitting terminal 9,12 of photoelectricity door one, two and the receiving end 11,13 of photoelectricity door one, two, the transmitting terminal of photoelectricity door one, 29,12, receiving end 11,13 place is arranged on corresponding support 8 respectively by the vernier scale 10 of 50 calibration, described photoelectricity gate control circuit includes CD4011 chip 30, the voltage input end of DC voltage-stabilizing module 29 connects the transformer 31 that 220V becomes 6V, the voltage output end photoelectricity door 1 in parallel of DC voltage-stabilizing module 29, photoelectricity door 2 33, photoelectricity door 32,33 and digital display timer 6 are connected with CD4011 chip 30 respectively, described thermostatic control water tank 19 is provided with filler 20, the front panel of thermostatic control water tank 19 is provided with gauge glass 21, two binding posts 22, temperature detect switch (TDS) 23, the rear panel of thermostatic control water tank 19 is provided with water delivering orifice 25, water inlet 26, gap 27, power supply base 24 with fuse, radiator fan 28, high power voltage stabilized power source is provided with in thermostatic control water tank 19, master controller, heating plate, cooling piece, the signal input part of master controller is connected with temperature-sensing probe 17 by two binding posts 22, the signal output part control linkage high power voltage stabilized power source of master controller, high power voltage stabilized power source and heating plate, cooling piece connects, the water inlet 15 of described container 14, the water delivering orifice 25 of water delivering orifice 16 and thermostatic control water tank 19, water inlet 26 connects.
Digital display timer 6 is provided with timer reset key 7.
Pipeline between container 14 and constant temperature water tank 19 is provided with water pump, forms circulation waterway.
The back side of base of measuring equipment 3 adopts dismountable panel, and the lower surface of base of measuring equipment 3 is provided with four adjustment screws 4, regulates four to adjust screw 4 and makes tester be in vertical state.
The Measuring Time scope 0.001s ~ 99.999s of digital display timer 6, use photoelectricity door one triggered timer to start timing, photoelectricity door two triggered timer time out, the time of digital display timer display is the time interval that little firm ball warp crosses two photoelectricity doors.
The utilizing emitted light of the transmitting terminal 9,12 of photoelectricity door one, two is red visible laser, and utilizing emitted light aperture is 0.9mm, aligns with the vernier scale zero graduation of 50 calibration in the unthreaded hole center of circle.
The receiving end 11,13 of photoelectricity door one, two is NPN open type, and receiving end central point aligns with the vernier scale zero graduation of 50 calibration, and has installed LED 34 and hummer 35 at receiving end, and LED 34 is connected with CD4011 chip 30 with hummer 35; When laser-correlation receiving end, LED 34 is bright, and when receiving end is blocked, LED 34 is gone out, and hummer 35 pipes.
The container 14 holding testing liquid is double layer light transmission glass material container.
Circular hole 18 diameter is 2.2mm, is that the center of the small ball testing liquid in a reservoir of about 2mm falls for making diameter.
Following explanation is further made respectively for each device of the present utility model:
Tester device figure (Fig. 1)
1, power switch, controls the break-make of coefficient of viscosity tester power supply.
2, with the power supply base of fuse, directly plug about 220V civil power, export 5V D.C. regulated power supply through DC voltage-stabilizing module, power to tester.
3, base of measuring equipment, base table top is made by metal material, and install the circuit (Fig. 4) such as DC voltage-stabilizing module, photoelectricity gate control circuit below table top, base back surface uses dismountable panel.
4, adjust screw, regulate four screws to make tester be in vertical state.
5, spirit-leveling instrument.
6, digital display millisecond timer, Measuring Time scope 0.001s ~ 99.999s, use photoelectricity door one triggered timer to start timing, photoelectricity door two triggered timer time out, the time of timer display is the time interval that little firm ball warp crosses two photoelectricity doors.
7, timer reset key, by record time reset, again writing time numerical value.
8, indicate the support of millimeter scale, support is provided with track, facilitates photoelectricity door to move up and down.
9, the transmitting terminal of photoelectricity door one, transmitting terminal is red visible laser, the advantage such as laser-correlation stable performance, fast response time, shock resistance, vibration resistance, interference are little.Utilizing emitted light aperture is 0.9mm, and aliging with the vernier zero graduation of 50 calibration in the unthreaded hole center of circle, and is fixed on vernier scale.
10, the vernier scale of 50 calibration, setting nut makes vernier scale move up and down in bracket track.
11, the receiving end of photoelectricity door one, receiving end is NPN open type, receiving end central point aligns with vernier scale zero graduation, installed LED and hummer at receiving end, when laser-correlation receiving end, LED is bright, when small ball is through photoelectricity door, when receiving end is blocked, LED is gone out, and the hummer sound that " ticks " pipes.
12, the transmitting terminal of photoelectricity door two, configures identical with photoelectricity door one.
13, the receiving end of photoelectricity door two, configures identical with photoelectricity door one.
14, the container of testing liquid is held, double layer light transmission glass material container.
15, water inlet, testing liquid carries out the temperature control that heats or freeze, and by carrying out temperature control to the water in double container interlayer, reaching fluid temperature balance, being connected with the water delivering orifice 25 of water tank.
16, water delivering orifice, is connected with the water inlet 26 of water tank.
17, temperature-sensing probe, is placed in container filled with water and carries out temperature-sensitive, by NTC temperature sensor, temperature ascending, descending is converted into the device of electric signal switching, realizes the accurate temperature control of testing liquid.
18, circular hole, container stopper circle centre position is provided with 2.2mm circular hole, makes diameter be that the little firm ball of about 2mm falls in the center of testing liquid.
Thermostatic control water tank (Fig. 2)
19, thermostatic control water tank, casing is by high power voltage stabilized power source, heating plate, cooling piece, and the compositions such as water pump, water tank, the temperature control decorum, realize heating liquid and freezing.
20, filler, when needing experiment, by filler injection experiments water.
21, gauge glass, installs gauge glass in casing front end, and is provided with lowest water level and peak level stand by lamp
22, two reserved binding posts, in order to connect NTC temperature sensor.
23, temperature detect switch (TDS), primarily of LCDs and button composition, on display screen, display current room temperature and set temperature, button is: " setting ", " ← ", " → ", " ▲ ", " ▼ "
Press " setting " key, the numeral of the temperature arranged starts to flash, by the position of " ← ", " → " mobile Temperature numerical arranged, again by the size of " ▲ ", " ▼ " set temperature, judged by temperature control system, when " set temperature < Current Temperatures ", start cooling piece work, until " set temperature=Current Temperatures " cooling piece quits work, when " set temperature > Current Temperatures ", start heating plate work, until " set temperature=Current Temperatures " heating plate quits work, so repeat said process.The temperature of testing liquid remain near to fixed temperature one among a small circle in, substantially reach the object that constant temperature controls automatically.
The rear panel (Fig. 3) of casing
24, be with fuse power supply base, directly plug about 220V civil power, power to experimental box.
25, water delivering orifice, is connected with the water inlet 15 of container.
26, water inlet, is connected with the water delivering orifice 16 of container.
27, gap, when being added water to container by filler, when exceeding maximum water level, water is overflowed by gap automatically.
28, radiator fan, when cooling piece works, fan dispels the heat outside casing.
Principle of work of the present utility model:
The viscosity experimental provision of research liquid using falling ball, serviceability temperature sensing switch controls heating or refrigerating plant work, reaches testing liquid accurate temperature controlling.Use the distance that the vernier caliper measurement bead of 50 scale division values at the uniform velocity falls, use photoelectricity door to survey the time of bead whereabouts, comparatively traditional means of experiment, measuring error reduces greatly.At traditional viscosity test device, when carrying out the coefficient of viscosity measurement of different temperatures, be only limited to liquid under the state of room temperature, heat, cannot carry out studying the measurement lower than the room temperature liquid coefficient of viscosity.This device uses multiple cooling piece to freeze to testing liquid, the coefficient of viscosity of research different temperatures.
Radius is the smooth, spherical solid of r, is ρ in density 0the coefficient of viscosity is η and liquid level is when move with speed V in unlimited broad viscous fluid, if speed not quite, do not produce eddy current in less, the liquid of ball, then the viscous force that bead is subject to is
F=6πηrV
Make bead fall in limited circle oil cylinder during experiment, liquid is not unlimited broad, considers the impact of cylinder wall, and reply Stokes formula is revised,
&eta; = 1 18 ( &rho; - &rho; 0 ) gd 2 18 V ( 1 + 2.4 d D )
When measuring coefficient of viscosity by falling ball method, ρ, ρ 0, g is the degree of accuracy of definite value, η, the precision measured by d, D, V determines, traditional experimental measurement method, d measures and uses milscale, and D measures and uses vernier caliper, but V measures and uses meter ruler to survey little firm ball operation distance, and artificial start the watch timing, introduces systematic error and accidental error is larger, this experimental provision, uses the vernier caliper measurement bead working time of 50 scale division values, uses photoelectricity door to trigger millisecond meter and carries out timing, avoid people to be the error caused, substantially increase the degree of accuracy of experiment.

Claims (9)

1. a high precision temperature-change type liquid coefficient of viscosity measuring instrument, is characterized in that: include coefficient of viscosity tester, thermostatic control water tank, photoelectricity gate control circuit, described coefficient of viscosity tester includes base of measuring equipment, interconnective DC voltage-stabilizing module is installed in base of measuring equipment, photoelectricity gate control circuit, base of measuring equipment upper surface is provided with power switch, with the power supply base one of fuse, digital display timer, with power supply base one and the DC voltage-stabilizing model calling of fuse, the middle part of base of measuring equipment is provided with the container holding testing liquid, spirit-leveling instrument, container upper, the sidewall of lower end is respectively equipped with water inlet, water delivering orifice, the stopper of container top is inserted with temperature-sensing probe in container, the stopper circle centre position of container top has a circular hole, the base of measuring equipment being positioned at the both sides of container is installed respectively the support indicating millimeter scale, two stands is equipped with the track moved up and down for photoelectricity door one, two, two stands is respectively equipped with the transmitting terminal of photoelectricity door one, two and the receiving end of photoelectricity door one, two, transmitting terminal, the receiving end place of photoelectricity door one, two are arranged on corresponding support respectively by the vernier scale of 50 calibration, described photoelectricity gate control circuit includes CD4011 chip, the voltage input end of DC voltage-stabilizing module connects the transformer that 220V becomes 6V, the voltage output end photoelectricity door one in parallel of DC voltage-stabilizing module, photoelectricity door two, photoelectricity door one, two and digital display timer are connected with CD4011 chip respectively, described thermostatic control water tank is provided with filler, the front panel of thermostatic control water tank is provided with gauge glass, two binding posts, temperature detect switch (TDS), the rear panel of thermostatic control water tank is provided with water delivering orifice, water inlet, gap, power supply base two with fuse, radiator fan, high power voltage stabilized power source is provided with in thermostatic control water tank, master controller, heating plate, cooling piece, the signal input part of master controller is connected with temperature-sensing probe by two binding posts, the signal output part control linkage high power voltage stabilized power source of master controller, high power voltage stabilized power source and heating plate, cooling piece connects, the water inlet of described container, the water delivering orifice of water delivering orifice and thermostatic control water tank, water inlet connects.
2. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, is characterized in that: described digital display timer is provided with timer reset key.
3. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, is characterized in that: the pipeline between described container and constant temperature water tank is provided with water pump, forms circulation waterway.
4. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, is characterized in that: the back side of described base of measuring equipment adopts dismountable panel, and the lower surface of base of measuring equipment is provided with four adjustment screws.
5. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, it is characterized in that: the Measuring Time scope 0.001s ~ 99.999s of described digital display timer, photoelectricity door one triggered timer is used to start timing, photoelectricity door two triggered timer time out, the time of digital display timer display is the time interval that little firm ball warp crosses two photoelectricity doors.
6. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, it is characterized in that: the utilizing emitted light of the transmitting terminal of described photoelectricity door one, two is red visible laser, utilizing emitted light aperture is 0.9mm, aligns with the vernier scale zero graduation of 50 calibration in the unthreaded hole center of circle.
7. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, it is characterized in that: the receiving end of described photoelectricity door one, two is NPN open type, receiving end central point aligns with the vernier scale zero graduation of 50 calibration, and at receiving end, LED and hummer have been installed, LED is connected with CD4011 chip with hummer; When laser-correlation receiving end, LED is bright, and when receiving end is blocked, LED is gone out, buzzer call.
8. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, is characterized in that: the described container holding testing liquid is double layer light transmission glass material container.
9. a kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument according to claim 1, is characterized in that: described Circularhole diameter is 2.2mm, is that the center of the small ball testing liquid in a reservoir of about 2mm falls for making diameter.
CN201420569474.3U 2014-09-29 2014-09-29 A kind of high precision temperature-change type liquid coefficient of viscosity measuring instrument Expired - Fee Related CN204154602U (en)

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104297104A (en) * 2014-09-29 2015-01-21 安徽农业大学 High-accuracy temperature-variable liquid viscous coefficient measuring instrument
CN106840966A (en) * 2017-02-23 2017-06-13 中国石油大学(华东) Evaluate the device and method of polymer Efficient Adhesive Promotion in supercritical carbon dioxide
CN107247009A (en) * 2017-06-16 2017-10-13 内蒙古科技大学 A kind of pipe clamp photoelectricity door determines coefficient of viscosity experiment instrument

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104297104A (en) * 2014-09-29 2015-01-21 安徽农业大学 High-accuracy temperature-variable liquid viscous coefficient measuring instrument
CN106840966A (en) * 2017-02-23 2017-06-13 中国石油大学(华东) Evaluate the device and method of polymer Efficient Adhesive Promotion in supercritical carbon dioxide
CN107247009A (en) * 2017-06-16 2017-10-13 内蒙古科技大学 A kind of pipe clamp photoelectricity door determines coefficient of viscosity experiment instrument

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