CN204138731U - A kind of rare-earth extracting tank continuous saponification device - Google Patents
A kind of rare-earth extracting tank continuous saponification device Download PDFInfo
- Publication number
- CN204138731U CN204138731U CN201420495475.8U CN201420495475U CN204138731U CN 204138731 U CN204138731 U CN 204138731U CN 201420495475 U CN201420495475 U CN 201420495475U CN 204138731 U CN204138731 U CN 204138731U
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- CN
- China
- Prior art keywords
- mixing section
- rare
- settling tank
- continuous saponification
- extracting tank
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Abstract
The utility model relates to rare earth manufacture field, particularly a kind of rare-earth extracting tank continuous saponification device.Comprise opening for feed and water supplement port, it is characterized in that: comprise more than three groups mixing sections, more than three groups clarifying chambers, whipping appts is provided with in the middle of described mixing section, water eliminator and oil weir is also provided with between described mixing section and clarifying chamber, last group of described mixing section connects except Ca groove, except Ca groove connects settling tank, this settling tank is provided with pipeline and is connected with water supplement port.As preferably, opening for feed is provided with dosing system, intelligent further, reduces the export of labor of operating personnel.The utility model provides simple, the convenient and practical rare-earth extracting tank continuous saponification device of a kind of structure, at interval, a mixing section place arranges acidic substance return-flow structure, is also provided with settling tank in terminal, both improve saponification degree, also reduce the consumption of the material such as acid, alkali, greatly reducing production cost, and device achieves lasting extraction saponification work.
Description
Technical field
The utility model relates to rare earth manufacture field, particularly a kind of extraction tank device for saponifying.
Background technology
The separating device of solvent extration has mixer-settler, centrifugal extractor etc., purification rare earth extraction agent used has: the cation extractant taking acid phosphoric acid ester as representative, as P204 rare-earth extractant, P507 rare-earth extractant, take amine as the anionresin liquid N1923 of representative and the solvent extraction agent three kinds that is representative with neutral phosphates such as TBP, P350.The viscosity of these extraction agents and proportion are all very high, not easily separated with water.Usual kerosene equal solvent is diluted to be used again.
General extraction process is, first solid soap agent loaded in mixing tank, saponifying agent solution is made in the stirring that adds water, and then carries out saponification reaction by extraction agent and saponifying agent solution loading saponification tank.In the industrial production, efficiency is very low, and not only quality is likely affected and also there is certain potential safety hazard for the saponification reaction of this discontinuity.
Summary of the invention
The purpose of this utility model is exactly solve above-mentioned technical problem, the rare-earth extracting tank providing a kind of structure simple, convenient and practical and can the device of continuous saponification.
Technical problem of the present utility model is solved mainly through following technical proposals:
A kind of rare-earth extracting tank continuous saponification device, comprise opening for feed and water supplement port, it is characterized in that: comprise more than three groups mixing sections, more than three groups clarifying chambers, whipping appts is provided with in the middle of described mixing section, water eliminator and oil weir is also provided with between described mixing section and clarifying chamber, last group of described mixing section connects except Ca groove, and except Ca groove connects settling tank, this settling tank is provided with pipeline and is connected with water supplement port.As preferably, opening for feed is provided with dosing system, intelligent further, reduces the export of labor of operating personnel.
Concrete, described mixing section the 3rd group is provided with reflux line and is connected with first group, and described mixing section the 4th group is provided with reflux line and is connected with second group, by that analogy, by acidic substance recirculate mixing, and decreasing pollution, save energy.
Concrete, described clarifying chamber often organizes and all organizes clarifying chamber with last and be connected.
Concrete, described water eliminator is located at a mixing section side bottom adjacent with clarifying chamber, and described oil weir is located at a mixing section side roof part adjacent with clarifying chamber, leaves space between the two, and water eliminator vertex is higher than oil weir nadir, ensures technique effect further.
Concrete, described except being provided with filter screen between Ca groove and settling tank.
Concrete, be provided with slag-drip opening bottom described settling tank, easy cleaning settling tank.
The beneficial effects of the utility model are: at interval, a mixing section place arranges acidic substance return-flow structure, is also provided with settling tank in terminal this device, both improve saponification degree, also reduce the consumption of the material such as acid, alkali, greatly reducing production cost, and device achieves lasting extraction saponification work.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 11-13. mixing section; 21-23. clarifying chamber; 3. water eliminator; 4. oil weir; 5. filter screen; 6. opening for feed; 7. water supplement port; 8. except Ca groove; 9. settling tank; 91. slag-drip openings; 10. reflux line.
Embodiment
Below by embodiment, and by reference to the accompanying drawings, the technical solution of the utility model is described in further detail.Wherein mixing section is more than three groups, identifies from 11,12,13 in figure ... analogize; Clarifying chamber is all more than three groups, identifies from 21,22,23 in figure ... analogize.
A kind of rare-earth extracting tank continuous saponification device, comprise opening for feed 6 and water supplement port 7, comprise more than three groups mixing section 11-13, more than three groups clarifying chamber 21-23, whipping appts is provided with in the middle of described mixing section 11-13, water eliminator 3 and oil weir 4 is also provided with between described mixing section 11-13 and clarifying chamber 21-23, last group of described mixing section 11-13 connects except Ca groove 8, and except Ca groove 8 connects settling tank 9, this settling tank 9 is provided with pipeline and is connected with water supplement port 7.As preferably, opening for feed 6 is provided with dosing system, intelligent further, reduces the export of labor of operating personnel.The combination of mixing section 11-13 and clarifying chamber 21-23 can from one group to up to a hundred groups, and accompanying drawing is only rough schematic, is not construed as limiting.
Concrete, described mixing section 11-13 the 3rd group is provided with reflux line 10 and is connected with first group, and described mixing section 11-13 the 4th group is provided with reflux line 10 and is connected with second group, by that analogy, by acidic substance recirculate mixing, and decreasing pollution, save energy.Described clarifying chamber 21-23 often organizes and all organizes clarifying chamber 21-23 with last and be connected.Described water eliminator 3 is located at mixing section 11 side bottom adjacent with clarifying chamber 21, described oil weir 4 is located at mixing section 11 side roof part adjacent with clarifying chamber 21, leave space between the two, and water eliminator 3 vertex is higher than oil weir 4 nadir, ensures technique effect further.Described except being provided with filter screen 5 between Ca groove 8 and settling tank 9.Slag-drip opening 91 is provided with, easy cleaning settling tank bottom described settling tank 9.
The present embodiment is the embodiment of the utility model example; for those skilled in the art; on the basis that the utility model discloses application method and principle; be easy to make various types of improvement or distortion; and the structure be not limited only to described by the above-mentioned embodiment of the utility model; therefore previously described mode is preferred version; and not there is restrictive meaning; every equivalence done according to the utility model changes and amendment, all in the scope protection domain of the utility model claims.
Claims (6)
1. a rare-earth extracting tank continuous saponification device, comprise opening for feed and water supplement port, it is characterized in that: comprise more than three groups mixing sections, more than three groups clarifying chambers, whipping appts is provided with in the middle of described mixing section, water eliminator and oil weir is also provided with between described mixing section and clarifying chamber, last group of described mixing section connects except Ca groove, and except Ca groove connects settling tank, this settling tank is provided with pipeline and is connected with water supplement port.
2. a kind of rare-earth extracting tank continuous saponification device according to claim 1, it is characterized in that: described mixing section the 3rd group is provided with reflux line and is connected with first group, described mixing section the 4th group is provided with reflux line and is connected with second group, by that analogy.
3. a kind of rare-earth extracting tank continuous saponification device according to claim 1, is characterized in that: described clarifying chamber often organizes and all organizes clarifying chamber with last and be connected.
4. a kind of rare-earth extracting tank continuous saponification device according to claim 1, it is characterized in that: described water eliminator is located at a mixing section side bottom adjacent with clarifying chamber, described oil weir is located at a mixing section side roof part adjacent with clarifying chamber, leave space between the two, and water eliminator vertex is higher than oil weir nadir.
5. a kind of rare-earth extracting tank continuous saponification device according to claim 1, is characterized in that: described except being provided with filter screen between Ca groove and settling tank.
6. a kind of rare-earth extracting tank continuous saponification device according to claim 1, is characterized in that: be provided with slag-drip opening bottom described settling tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420495475.8U CN204138731U (en) | 2014-08-29 | 2014-08-29 | A kind of rare-earth extracting tank continuous saponification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420495475.8U CN204138731U (en) | 2014-08-29 | 2014-08-29 | A kind of rare-earth extracting tank continuous saponification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204138731U true CN204138731U (en) | 2015-02-04 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420495475.8U Expired - Fee Related CN204138731U (en) | 2014-08-29 | 2014-08-29 | A kind of rare-earth extracting tank continuous saponification device |
Country Status (1)
| Country | Link |
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| CN (1) | CN204138731U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113403489A (en) * | 2021-06-17 | 2021-09-17 | 吉安鑫泰科技有限公司 | Calcium saponification organic phase clarification extraction process and equipment thereof |
-
2014
- 2014-08-29 CN CN201420495475.8U patent/CN204138731U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113403489A (en) * | 2021-06-17 | 2021-09-17 | 吉安鑫泰科技有限公司 | Calcium saponification organic phase clarification extraction process and equipment thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150204 Termination date: 20160829 |
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| CF01 | Termination of patent right due to non-payment of annual fee |