CN204051229U - A kind of purification impurity elimination system - Google Patents
A kind of purification impurity elimination system Download PDFInfo
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- CN204051229U CN204051229U CN201420493580.8U CN201420493580U CN204051229U CN 204051229 U CN204051229 U CN 204051229U CN 201420493580 U CN201420493580 U CN 201420493580U CN 204051229 U CN204051229 U CN 204051229U
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- chromatographic column
- settling tank
- column group
- pipeline
- supercentrifuge
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Abstract
The utility model relates to the technical field that material is purified, especially a kind of purification impurity elimination system, it comprises the material pot, coarse filter device, settling tank and the chromatographic column group that utilize pipeline to connect successively, wherein chromatographic column group is made up of some chromatography column in series, it is characterized in that: the pipeline between coarse filter device and settling tank is provided with condenser, condenser inside is provided with independently condensate water circulatory system, also connects supercentrifuge is housed between described settling tank with chromatographic column group; The utility model by setting up condenser and supercentrifuge in material purification impurity elimination system, not only greatly reduce the temperature of material, shorten the sedimentation time of material, prevent the fermentation of material to go bad, and greatly reduce the turbidity of material, reduce the loss to chromatographic column.
Description
Technical field
The utility model relates to the technical field that material is purified, especially a kind of purification impurity elimination system.
Background technology
At present, general employing such as lower device carries out purification impurity elimination to the material after plant extract: the material pot utilizing pipeline to connect successively, coarse filter device, settling tank and chromatographic column group, wherein chromatographic column group is made up of some chromatography column in series, forms a kind of purification impurity elimination system of hairdo of connecting thus.Operationally, be stored in material (counter-flow extraction liquid) in material pot after coarse filter device, enter into settling tank and carry out precipitate and separate, and then the supernatant liquor among settling tank after being separated is carried out further separating-purifying by chromatographic column group, thus the product needed for obtaining.
But existing extraction system does not consider the temperature problem of material.Generally speaking, enter the temperature of the material in material pot at about 60 DEG C, in order to precipitate and separate more convenient in settling tank, often material to be placed in settling tank more than 8 hours, it is made naturally to cool, to reach the effect being separated impurity elimination, so not only length consuming time, affect manufacturing schedule, and the material be placed in settling tank easily ferments rotten.
Meanwhile, the turbidity of the material obtained after existing extraction system is purified is undesirable.Although what adopt when entering chromatographic column group is supernatant liquor in settling tank, but the turbidity of supernatant liquor is 60NTU, wherein still there is impurity tiny in a large number and part oil, when therefore adopting chromatographic column to carry out separating-purifying to current material, the loss ratio of impurity in material to chromatographic column is larger, simultaneously in order to improve the clarity of material, a large amount of chromatographic columns often to be adopted to connect successively repeatedly to purify to material, and the life cycle of chromatographic column is short, substantially increase Productive statistics cost.
Summary of the invention
When the purpose of this utility model will solve exactly and adopt existing purification impurity elimination system to purify to material, temperature of charge is high, the sedimentation time is long, so that easily fermentation is rotten, the problem that the turbidity of material obtained after simultaneously purifying is undesirable, there is provided a kind of purification efficiency high, the desirable purification impurity elimination system that also can effectively prevent material fermentation rotten of the turbidity of material after purifying for this reason.
Concrete scheme of the present utility model is: a kind of purification impurity elimination system, comprise material pot, coarse filter device, settling tank and the chromatographic column group of connecting successively with pipeline, wherein chromatographic column group is made up of some chromatography column in series, it is characterized in that: the pipeline between coarse filter device and settling tank is provided with condenser, condenser inside is provided with independently condensate water circulatory system, also connects supercentrifuge is housed between described settling tank with chromatographic column group.
Tank skin on the upside of settling tank described in the utility model is provided with discharge nozzle, discharge nozzle is connected with the charging aperture of supercentrifuge, the discharging opening of supercentrifuge connects with chromatographic column group, and the tank skin on the downside of described settling tank is provided with blow-off pipe, and blow-off pipe is provided with control valve.
The pipeline of material pot described in the utility model and coarse filter device is provided with control valve, and the pipeline between described condenser, settling tank and supercentrifuge and chromatographic column group is equipped with control valve and product pump.
In the group of chromatographic column described in the utility model, the pipeline between two chromatographic columns of series connection is mutually provided with control valve and product pump.
Specific works mode of the present utility model is as follows: the material (counter-flow extraction liquid) be stored in material pot is filtered for the first time by coarse filter device, material after filtering is before entering settling tank, cooling process is carried out through condenser, the temperature of material is reduced within 10 DEG C by 60 DEG C, then in settling tank, precipitate and separate is carried out, get the supernatant liquor in settling tank afterwards, centrifugation purification is carried out by supercentrifuge, the material obtained of centrifugation being purified carries out further precision processing by chromatographic column group, finally obtains product.
The utility model adds condenser and supercentrifuge in existing material purification impurity elimination system, has the following advantages:
(1) in the utility model, the temperature of material is reduced within 10 DEG C by 60 DEG C by condenser, and material of being more convenient for carries out precipitate and separate in settling tank, and within the sedimentation time is reduced to 4h by 8h, the fermentation that effectively prevent material is gone bad.
(2) the utility model high speed centrifuge effectively eliminates the fine impurities and part oil that exist in settling tank supernatant liquor, after this centrifugation, the turbidity of material is reduced to 20NTU by original 60NTU, and then carry out further precision processing by chromatographic column group, within turbidity can being reduced in 5NTU.
(3) the utility model improves the operating efficiency of whole purifying technique, according to actual conditions, can increase the life cycle of chromatographic column in appropriate amount simultaneously, reduces production cost and drops into.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1-material pot, 2-coarse filter device, 3-settling tank, 4-chromatographic column group, 5-condenser, 6-condensate water circulatory system, 7-supercentrifuge, 8-discharge nozzle, 9-blow-off pipe, 10-control valve, 11-product pump.
Detailed description of the invention
See Fig. 1, the utility model comprises material pot 1, coarse filter device 2, settling tank 3 and the chromatographic column group 4 of connecting successively with pipeline, wherein chromatographic column group 4 is made up of some chromatography column in series, pipeline between described coarse filter device 2 and settling tank 3 is provided with condenser 5, condenser 5 inside is provided with independently condensate water circulatory system 6, and described settling tank 3 is equipped with supercentrifuge 7 with also connecting between chromatographic column group 4.
Tank skin on the upside of settling tank 3 described in the present embodiment is provided with discharge nozzle 8, discharge nozzle 8 is connected with the charging aperture of supercentrifuge 7, the discharging opening of supercentrifuge 7 connects with chromatographic column group 4, and the tank skin on the downside of described settling tank 3 is provided with blow-off pipe 9, and blow-off pipe 9 is provided with control valve 10.
The pipeline of material pot 1 described in the present embodiment and coarse filter device 2 is provided with control valve 10, and the pipeline between described condenser 5, settling tank 3 and supercentrifuge 7 and chromatographic column group 4 is equipped with control valve 10 and product pump 11.
In the group of chromatographic column described in the present embodiment 4, the pipeline between two chromatographic columns of series connection is mutually provided with control valve 10 and product pump 11.
Claims (4)
1. a purification impurity elimination system, comprise material pot, coarse filter device, settling tank and the chromatographic column group of connecting successively with pipeline, wherein chromatographic column group is made up of some chromatography column in series, it is characterized in that: the pipeline between coarse filter device and settling tank is provided with condenser, condenser inside is provided with independently condensate water circulatory system, also connects supercentrifuge is housed between described settling tank with chromatographic column group.
2. a kind of purification impurity elimination system according to claim 1, it is characterized in that: the tank skin on the upside of described settling tank is provided with discharge nozzle, discharge nozzle is connected with the charging aperture of supercentrifuge, the discharging opening of supercentrifuge connects with chromatographic column group, tank skin on the downside of described settling tank is provided with blow-off pipe, and blow-off pipe is provided with control valve.
3. a kind of purification impurity elimination system according to claim 1, it is characterized in that: the pipeline of described material pot and coarse filter device is provided with control valve, the pipeline between described condenser, settling tank and supercentrifuge and chromatographic column group is equipped with control valve and product pump.
4. a kind of purification impurity elimination system according to claim 1, is characterized in that: in described chromatographic column group, and the pipeline between two chromatographic columns of series connection is mutually provided with control valve and product pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420493580.8U CN204051229U (en) | 2014-08-29 | 2014-08-29 | A kind of purification impurity elimination system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420493580.8U CN204051229U (en) | 2014-08-29 | 2014-08-29 | A kind of purification impurity elimination system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204051229U true CN204051229U (en) | 2014-12-31 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201420493580.8U Expired - Fee Related CN204051229U (en) | 2014-08-29 | 2014-08-29 | A kind of purification impurity elimination system |
Country Status (1)
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| CN (1) | CN204051229U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105688442A (en) * | 2016-01-21 | 2016-06-22 | 中国科学院过程工程研究所 | Column chromatography and membrane filtration integration system |
| CN113121674A (en) * | 2021-04-19 | 2021-07-16 | 酒泉大得利制药股份有限公司 | Chorionic gonadotrophin processing system and chorionic gonadotrophin processing technology |
-
2014
- 2014-08-29 CN CN201420493580.8U patent/CN204051229U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105688442A (en) * | 2016-01-21 | 2016-06-22 | 中国科学院过程工程研究所 | Column chromatography and membrane filtration integration system |
| CN113121674A (en) * | 2021-04-19 | 2021-07-16 | 酒泉大得利制药股份有限公司 | Chorionic gonadotrophin processing system and chorionic gonadotrophin processing technology |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141231 Termination date: 20180829 |
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| CF01 | Termination of patent right due to non-payment of annual fee |