CN204051066U - A kind of chromatographic column agitating device - Google Patents
A kind of chromatographic column agitating device Download PDFInfo
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- CN204051066U CN204051066U CN201420493624.7U CN201420493624U CN204051066U CN 204051066 U CN204051066 U CN 204051066U CN 201420493624 U CN201420493624 U CN 201420493624U CN 204051066 U CN204051066 U CN 204051066U
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- agitating device
- cylinder
- tubular shell
- shaft
- chromatographic column
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Abstract
The utility model relates to the technical field that feed separation is purified, especially a kind of chromatographic column agitating device, it has cylinder, cylinder forms closed structure by tubular shell and upper and lower two hemispherical lids, particulate resins is filled with in cylinder, the two ends up and down of tubular shell are respectively equipped with charging aperture and discharging opening, it is characterized in that: in cylinder, be also provided with the agitating device for stirring particles shape resin, the lid of cylinder upper end is equipped with and forms with agitating device the drive unit driving and be connected, described agitating device has the shaft arranged along tubular shell central axis, shaft has been welded some pusher propeller leaves, the upper end of shaft is rotated by bearing and is fixed on a support member, support member is fixed on the upper end of tubular shell, the utility model structure is simple, design ingenious, the stirring up and down that can realize column body resin is loosened, reach developing result of just turning one's coat, increase the adsorbance of resin, improve output and purification efficiency.
Description
Technical field
The utility model relates to the technical field that feed separation is purified, especially a kind of chromatographic column agitating device.
Background technology
Current, in Chemical Manufacture, consider and expand the scale of production, usually adopt jumbo chromatographic column to carry out separating-purifying to material.Because the loading amount of the resin of chromatographic column cylinder inside is larger, in use, resin punching does not wash clean, easily lumps, thus affects the sorption and desorption effect of material, reduces the quality of product.
Application number is: disclose a kind of chromatographic column in the patent document of 201210284654.2, sordid problem is rinsed for solving column body adsorbent (being particulate resins in this patent document), a kind of agitating device is disclosed, agitating device has the shaft arranged along cylinder length direction, the axle body of shaft is provided with and stirs loose paddle for carrying out adsorbent, wherein paddle is arranged along interval, shaft axial length direction.
Although agitating device disclosed in above patent document efficiently solves the problem that adsorbent punching does not wash clean and easily lumps to a certain extent, but the comparison of resistance of this agitating device suffered by whipping process is large, greatly increase the live load of drive motors, this agitating device can only accomplish the loose stirring in horizontal direction to adsorbent simultaneously, the stirring of vertical direction can not be accomplished, cause the adsorbance of adsorbent little; During flushing, agitating device must lengthen mixing time, impurity just can be made fully to be deposited to the bottom of chromatographic column, thus discharged by discharging opening, so greatly reduces operating efficiency and the load of chromatographic column.
Summary of the invention
The purpose of this utility model is exactly to solve the above problem existing for current chromatographic column agitating device, provides a kind of stirring resistance little, greatly can improve the chromatographic column agitating device of output and separating-purifying efficiency.
Concrete scheme of the present utility model is: a kind of chromatographic column agitating device, there is cylinder, cylinder forms closed structure by tubular shell and upper and lower two hemispherical lids, particulate resins is filled with in cylinder, the two ends up and down of tubular shell are respectively equipped with charging aperture and discharging opening, it is characterized in that: in cylinder, be also provided with the agitating device for stirring particles shape resin, the lid of cylinder upper end is equipped with and forms with agitating device the drive unit driving and be connected, described agitating device has the shaft arranged along tubular shell central axis, shaft has been welded some pusher propeller leaves, the upper end of shaft is rotated by bearing and is fixed on a support member, support member is fixed on the upper end of tubular shell.
Drive unit described in the utility model has the motor of vertical, and the output of motor consists of to drive reduction gear box and shaft and is connected.
The tubular shell of cylinder described in the utility model is provided with three mirror mouth, and three mirror mouth are arranged on same vertical straight line.
The outer wall of the lid of the upper end of cylinder described in the utility model is provided with three reinforcements, two wherein adjacent reinforcements above horizontal plane all in 120 ° of angles.
The utility model adopts the agitating device with pusher propeller leaf to replace the agitating device of existing interval layout paddle on shaft, has the following advantages:
(1) in the utility model, pusher propeller leaf is for paddle, and overall mechanical strength is larger, stirs resistance little, long service life;
(2) the utility model can realize particulate resins up and down comprehensive carry out upset loosen, efficiently avoid resin caking, increase the adsorption effect of resin;
(3) the utility model can realize particulate resins positive backwash up and down, and effectively can precipitate and discharge the impurity be mixed in resin, improve separating-purifying efficiency, the purity of material is promoted to 80%-85% by 60%-70% simultaneously.
Accompanying drawing explanation
Fig. 1 is schematic front view of the present utility model;
Fig. 2 is the schematic top plan view of Fig. 1;
Fig. 3 is the structural representation of the utility model middle column body.
In figure: 1-cylinder, 2-tubular shell, 3-lid, 4-charging aperture, 5-discharging opening, 6-shaft, 7-pusher propeller leaf, 8-support member, 9-motor, 10-reduction gear box, 11-mirror mouth, 12-reinforcement, 13-particulate resins.
Detailed description of the invention
See Fig. 1-3, the utility model has cylinder 1, cylinder 1 forms closed structure by tubular shell 2 and upper and lower two hemispherical lids 3, particulate resins 13 is filled with in cylinder 1, the two ends up and down of tubular shell 2 are respectively equipped with charging aperture 4 and discharging opening 5, particularly, the agitating device for stirring particles shape resin 13 is also provided with in cylinder 1, the lid 3 of cylinder 1 upper end is equipped with and forms with agitating device the drive unit driving and be connected, described agitating device has the shaft 6 arranged along tubular shell 2 central axis, shaft 6 has been welded some (being specially 7-8 sheet) pusher propeller leaves 7, the upper end of shaft 6 is rotated by bearing and is fixed on a support member 8, support member 8 is fixed on the upper end of tubular shell 2.
Drive unit described in the present embodiment has the motor 9 of vertical, and the output of motor 9 consists of to drive with shaft 6 reduction gear box 10 and is connected, see Fig. 1.
See Fig. 3, the tubular shell 2 of cylinder 1 described in the present embodiment is provided with three mirror mouth, 11, three mirror mouth 11 and is arranged on same vertical straight line.
The outer wall of the lid 3 of the upper end of cylinder 1 described in the present embodiment is provided with three reinforcements 12, two wherein adjacent reinforcements 12 above horizontal plane all in 120 ° of angles.
Chromatographic column described in the present embodiment is carbon steel line with rubber resin column, and the external diameter of cylinder 1 is 1000mm, and length is 3000mm.
The length of shaft 6 described in the present embodiment is 2700mm, and the diameter of axle is 100mm, and the width of pusher propeller leaf 7 is 500mm, and pitch is 300mm.
Claims (4)
1. a chromatographic column agitating device, there is cylinder, cylinder forms closed structure by tubular shell and upper and lower two hemispherical lids, particulate resins is filled with in cylinder, the two ends up and down of tubular shell are respectively equipped with charging aperture and discharging opening, it is characterized in that: in cylinder, be also provided with the agitating device for stirring particles shape resin, the lid of cylinder upper end is equipped with and forms with agitating device the drive unit driving and be connected, described agitating device has the shaft arranged along tubular shell central axis, shaft has been welded some pusher propeller leaves, the upper end of shaft is rotated by bearing and is fixed on a support member, support member is fixed on the upper end of tubular shell.
2. a kind of chromatographic column agitating device according to claim 1, is characterized in that: described drive unit has the motor of vertical, and the output of motor consists of to drive reduction gear box and shaft and is connected.
3. a kind of chromatographic column agitating device according to claim 1, is characterized in that: the tubular shell of described cylinder is provided with three mirror mouth, and three mirror mouth are arranged on same vertical straight line.
4. a kind of chromatographic column agitating device according to claim 1, is characterized in that: the outer wall of the lid of described cylinder upper end is provided with three reinforcements, two wherein adjacent reinforcements above horizontal plane all in 120 ° of angles.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420493624.7U CN204051066U (en) | 2014-08-29 | 2014-08-29 | A kind of chromatographic column agitating device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420493624.7U CN204051066U (en) | 2014-08-29 | 2014-08-29 | A kind of chromatographic column agitating device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204051066U true CN204051066U (en) | 2014-12-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420493624.7U Expired - Fee Related CN204051066U (en) | 2014-08-29 | 2014-08-29 | A kind of chromatographic column agitating device |
Country Status (1)
| Country | Link |
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| CN (1) | CN204051066U (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104606920A (en) * | 2015-01-06 | 2015-05-13 | 四川省林业科学研究院 | Method for loading sample onto column, stirring device, and devices utilizing stirring device to load sample onto column |
| CN106267901A (en) * | 2016-08-31 | 2017-01-04 | 朱小琼 | Adjustable resin column |
| CN106267900A (en) * | 2016-08-31 | 2017-01-04 | 朱小琼 | Resin column device |
| CN106345144A (en) * | 2016-08-31 | 2017-01-25 | 朱小琼 | Resin column with adjustable resin compactness |
| CN106345143A (en) * | 2016-08-31 | 2017-01-25 | 朱小琼 | Automatic separation device |
| CN106362436A (en) * | 2016-08-31 | 2017-02-01 | 朱小琼 | Separator based on controller |
| CN106390516A (en) * | 2016-08-31 | 2017-02-15 | 朱小琼 | Intelligent separation device |
| CN111672158A (en) * | 2020-07-24 | 2020-09-18 | 河北宝晟新型材料有限公司 | Alumina adsorption tower |
| CN112794394A (en) * | 2020-12-21 | 2021-05-14 | 安徽国星生物化学有限公司 | Intelligently controlled reaction kettle for treating acetaldehyde wastewater through resin adsorption and control method |
| CN113289379A (en) * | 2021-06-17 | 2021-08-24 | 合肥工业大学 | Soy lecithin adsorbs stirring purification equipment |
-
2014
- 2014-08-29 CN CN201420493624.7U patent/CN204051066U/en not_active Expired - Fee Related
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104606920A (en) * | 2015-01-06 | 2015-05-13 | 四川省林业科学研究院 | Method for loading sample onto column, stirring device, and devices utilizing stirring device to load sample onto column |
| CN106267901A (en) * | 2016-08-31 | 2017-01-04 | 朱小琼 | Adjustable resin column |
| CN106267900A (en) * | 2016-08-31 | 2017-01-04 | 朱小琼 | Resin column device |
| CN106345144A (en) * | 2016-08-31 | 2017-01-25 | 朱小琼 | Resin column with adjustable resin compactness |
| CN106345143A (en) * | 2016-08-31 | 2017-01-25 | 朱小琼 | Automatic separation device |
| CN106362436A (en) * | 2016-08-31 | 2017-02-01 | 朱小琼 | Separator based on controller |
| CN106390516A (en) * | 2016-08-31 | 2017-02-15 | 朱小琼 | Intelligent separation device |
| CN106362436B (en) * | 2016-08-31 | 2018-09-18 | 朱小琼 | Separator based on controller |
| CN106345144B (en) * | 2016-08-31 | 2018-12-07 | 朱小琼 | The resin column of adjustable resin compactness |
| CN106345143B (en) * | 2016-08-31 | 2019-01-01 | 靳琦 | The separator of automation |
| CN106267900B (en) * | 2016-08-31 | 2019-04-12 | 靳琦 | Resin column device |
| CN111672158A (en) * | 2020-07-24 | 2020-09-18 | 河北宝晟新型材料有限公司 | Alumina adsorption tower |
| CN112794394A (en) * | 2020-12-21 | 2021-05-14 | 安徽国星生物化学有限公司 | Intelligently controlled reaction kettle for treating acetaldehyde wastewater through resin adsorption and control method |
| CN113289379A (en) * | 2021-06-17 | 2021-08-24 | 合肥工业大学 | Soy lecithin adsorbs stirring purification equipment |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141231 Termination date: 20180829 |