CN203976970U - Circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer - Google Patents
Circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer Download PDFInfo
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- CN203976970U CN203976970U CN201420275957.2U CN201420275957U CN203976970U CN 203976970 U CN203976970 U CN 203976970U CN 201420275957 U CN201420275957 U CN 201420275957U CN 203976970 U CN203976970 U CN 203976970U
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Abstract
The utility model relates to a kind of circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer, comprises solution circulating device, temperature controlling system and aluminium foil corrosion frame; The water side of described magnetic force driving recycle pump is connected on the two side that electrolyzer is relative with feed-water end; Described temperature controlling system comprises temperature sensor, U-shaped quartz heating-pipe and 51 single chip circuit plates; Described aluminium foil corrosion frame comprises Graphite Electrodes anchor and aluminium foil folder, and the height of aluminium foil corrosion frame is less than electrolyzer height 3-5cm; Described solution circulating device can avoid solution inside there are differences; Temperature controlling system can Real-Time Monitoring temperature and is automatically regulated temperature, allows temperature keep constant, reduces experimental error; And can be according to the difference of experimental program, can choose that two or three electrolyzers use simultaneously and separate, also can carry out classification and send out hole experiment.
Description
(1) technical field
The utility model relates to a kind of circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer, belongs to aluminium foil corrosion research field.
(2) background technology
Along with the development of electronic industry, electric equipment products are constantly to high-performance, miniaturization, integrated development.Electrolytic condenser is requisite element in modern electric equipment products, accounts for 40% of whole electronic component consumptions.At present, the volume of electrical condenser has become one of key restriction factors of electronic circuit miniaturization greatly.Therefore, research Fabrication of High Specific Capacitance electrode aluminium foil has great meaning for the high-tech development of electronic information and high people's expanding economy.
At present mainly adopt sample to carry out to the research of aluminium foil corrosion, sample aluminium foil corrosion equipment mostly is beaker.Beaker heat retaining property and cyclicity are poor, use in real time thermometer measure solution temperature in experimentation, so not only time-consuming but also require great effort and measuring error larger, be one of important factor seriously restricting corrosive aluminum foil performance.Therefore, study circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer and can finely realize temperature Real-Time Monitoring, solution insulation and solution circulated, lay the foundation for obtaining high specific capacitance electrode aluminium foil.Circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer have high insulating effect, solution circulated fully, working efficiency advantages of higher.
(3) summary of the invention
In order to address the above problem, the utility model provides a kind of circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer, and this groove can Real-Time Monitoring solution temperature, circulate soln, can provide good corrosive environment for etching process, the experimental result having obtained.
A kind of circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer, comprises solution circulating device, temperature controlling system and aluminium foil corrosion frame;
Described solution circulating device comprises magnetic force driving recycle pump and circulating line; The water side of described magnetic force driving recycle pump is connected on the two side that electrolyzer is relative with feed-water end, and water side and the feed-water end of magnetic force driving recycle pump are communicated with by circulating line; And the feed-water end of magnetic force driving recycle pump in the installation site of electrolyzer higher than the installation site of its water side.Described temperature controlling system comprises temperature sensor, U-shaped quartz heating-pipe and 51 single chip circuit plates, described U-shaped quartz heating-pipe is separately fixed at temperature sensor the both sides that electrolyzer is inner relative, two terminals of U-shaped quartz heating-pipe are all enclosed with bakelite, U-shaped quartz heating-pipe is connected on the 5V rly. on 51 single chip circuit plates, and temperature sensor is connected on the temperature sensor joint on 51 single chip circuit plates.51 single chip circuit plates are positioned at electrolyzer outside and are connected with 5V direct supply.
Described aluminium foil corrosion frame comprises Graphite Electrodes anchor and aluminium foil folder, and described Graphite Electrodes anchor comprises Graphite Electrodes anchor top board, Graphite Electrodes, graphite supporting plate and aluminium foil folder pallet; Described Graphite Electrodes anchor top board is provided with three parallel-grooves, and both sides parallel-groove is respectively vertically installed with a Graphite Electrodes, and the length of the length of both sides parallel-groove and width and Graphite Electrodes and width equate; Length and the width of the length of middle parallel-groove and width and aluminium foil folder equate; Described aluminium foil folder is used for placing aluminium foil sample; Each Graphite Electrodes lower end is respectively provided with a graphite supporting plate, and aluminium foil folder pallet is arranged between two graphite supporting plates; Described aluminium foil folder pallet be provided with six equal-sized liquid-through holes and therein heart position be provided with a draw-in groove, in the middle of aluminium foil folder upper end is vertically mounted on, in parallel-groove, its lower end is arranged in the draw-in groove in the middle of aluminium foil folder pallet; Graphite Electrodes anchor top board width is greater than electrolyzer width; The height of aluminium foil corrosion frame is less than electrolyzer height 3-5cm.
When use by U-shaped quartz heating-pipe and the temperature sensor relative both sides of stationary electrolysis groove inside respectively, aluminium foil corrosion frame is put into electrolyzer inside, Graphite Electrodes anchor top board is placed on electrolyzer two lateral walls upper end, because the height of aluminium foil corrosion frame is less than electrolyzer height 3-5cm, so graphite supporting plate and bottom of electrolytic tank have certain spacing; Electrolyzer is filled etchant solution, magnetic force driving recycle pump switches on power, 51 single chip circuit plates are received on 5V power supply, set the bound of the required temperature value of experiment, the temperature of temperature sensor senses corrosive fluid, and sending temperature to 51 micro-chips, the U-shaped quartz heating-pipe of 51 micro-chip control heats etchant solution and is incubated.Magnetic force driving recycle pump impels circulation of elecrolyte to flow, and keeps the temperature of electrolytic solution to be consistent; According to the difference of experimental program, can choose that two electrolyzers use simultaneously and separate, hole electrolyzer is sent out in a conduct, and one as reaming electrolyzer; Also can choose that three electrolyzers use simultaneously and separate, hole electrolyzer is sent out in a conduct, and two as reaming electrolyzer.Also can carry out classification and send out hole experiment.
The utility model can avoid solution internal temperature there are differences, and has designed solution recycle system, and the power providing by magnetic force driving recycle pump fully stirs the liquid in groove, makes the solution various piece temperature in groove identical.
The utility model can be worked in the bad environment of heat retaining property, and heat-insulation system can Real-Time Monitoring temperature and automatically regulated temperature, reaches heat insulation effect.
Solution recycle system of the present utility model can avoid solution inside there are differences; Heat-insulation system can Real-Time Monitoring temperature and is automatically regulated temperature, allows temperature keep constant, reduces experimental error.When using simultaneously, two electrolyzers can greatly increase work efficiency.
(4) brief description of the drawings
Fig. 1 the utility model one-piece construction figure;
Fig. 2 solution circulating device annexation figure;
Fig. 3 aluminium foil sample corrosion rack front view;
Fig. 4 aluminium foil sample corrosion rack vertical view;
Fig. 5 single chip circuit schematic diagram;
The U-shaped quartz heating-pipe of (1) magnetic force driving recycle pump (2) (3) aluminium foil corrosion frame (4) temperature sensor (5) etching tank (6) circulating line (7) Graphite Electrodes (8) aluminium foil folder (9) aluminium foil folder pallet (10) liquid-through hole (11) aluminium foil folder pallet draw-in groove in figure
(5) embodiment
The utility model is mainly used in the corrosion of aluminium foil sample, explains together experimentation in conjunction with pattern.Taking high-voltage aluminum foil corrosion as example, adopt two electrolyzers below, one in order to send out a hole electrolyzer, one for reaming electrolyzer, the magnetic force driving recycle pump that the utility model uses is commercial product, and the model of magnetic force driving recycle pump is not limit.But be not limited to use range of the present utility model:
Case study on implementation:
After the utility model installs into solution circulating device, temperature controlling system, aluminium foil corrosion frame, power pack, two electrolyzers and be emitted on desk, hole electrolyzer is sent out in a conduct, and one as reaming electrolyzer; In two electrolyzers, all pile etchant solution, the magnetic force driving recycle pump (MP-10RN) of each electrolyzer is switched on power, corrosive fluid circulates.Terminals of U-shaped quartz heating-pipe are connected on the 5V rly. off (output terminal) on 51 single chip circuit plates and are drawn and be connected to U-shaped quartz heating-pipe plug one side by com (communication ends) again, and another terminals of U-shaped quartz heating-pipe are connected to the opposite side of U-shaped quartz heating-pipe plug; After 51 single chip circuit plates switch on power, by test the bound of needed temperature value in 51 single chip circuit plates by key assignments.The etchant solution temperature value that temperature sensor is surveyed feeds back in 51 singlechip chips, test with setting the temperature value comparison needing, if etchant solution temperature value reaches the upper 5V rly. in limited time disconnection of setting the needed temperature value of experiment, U-shaped quartz heating-pipe stops heating, if etchant solution temperature value reaches the lower 5V relay closes in limited time of setting the needed temperature value of experiment, U-shaped quartz heating-pipe starts heating.Finally, Graphite Electrodes is connected on the negative electrode of corrosion power supply, within temperature remains on the scope needing, aluminium foil sample complete pre-treatment is put into after aluminium foil folder, put into aluminium foil corrosion frame.Aluminium foil sample is connected on corrosion power anode, open aluminium foil corrosion power supply and send out hole experiment, sending out the complete later aluminium foil in hole washes, wash after three minutes, corrosion folder is put in the corrosion rack in reaming electrolyzer again, aluminium foil sample is connected on corrosion power anode, opens aluminium foil corrosion power supply and carries out reaming experiment.Electrolyzer temperature keeps constant temperature, can test continuously, improves conventional efficient.
For convenient experiment needs to use by three electrolyzers simultaneously, between three electrolyzers, keep relatively independent, one is a hole electrolyzer, two is reaming electrolyzer; Also can send out hole experiment for classification, greatly improve experiment effect, improve conventional efficient, save manpower.
Claims (1)
1. a circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer, is characterized in that comprising solution circulating device, temperature controlling system and aluminium foil corrosion frame;
Described solution circulating device comprises magnetic force driving recycle pump and circulating line; The water side of described magnetic force driving recycle pump is connected on the two side that electrolyzer is relative with feed-water end, and water side and the feed-water end of magnetic force driving recycle pump are communicated with by circulating line; And the feed-water end of magnetic force driving recycle pump and the installation site of electrolyzer are higher than the installation site of its water side; Described temperature controlling system comprises temperature sensor, U-shaped quartz heating-pipe and 51 single chip circuit plates, and described U-shaped quartz heating-pipe is separately fixed at temperature sensor the both sides that electrolyzer is inner relative; Two terminals of described U-shaped quartz heating-pipe are all enclosed with bakelite; Described U-shaped quartz heating-pipe is connected on the 5V rly. on 51 single chip circuit plates; Described temperature sensor is connected on the temperature sensor joint on 51 single chip circuit plates; Described 51 single chip circuit plates are positioned at electrolyzer outside and are connected with 5V direct supply;
Described aluminium foil corrosion frame comprises Graphite Electrodes anchor and aluminium foil folder, and described Graphite Electrodes anchor comprises Graphite Electrodes anchor top board, Graphite Electrodes, graphite supporting plate and aluminium foil folder pallet; Described Graphite Electrodes anchor top board is provided with three parallel-grooves, and both sides parallel-groove is respectively vertically installed with a Graphite Electrodes, and the length of the length of both sides parallel-groove and width and Graphite Electrodes and width equate; Length and the width of the length of middle parallel-groove and width and aluminium foil folder equate; Described aluminium foil folder is used for placing aluminium foil sample; Each Graphite Electrodes lower end is respectively provided with a graphite supporting plate, and aluminium foil folder pallet is arranged between two graphite supporting plates; Described aluminium foil folder pallet be provided with six equal-sized liquid-through holes and therein heart position be provided with a draw-in groove, in the middle of aluminium foil folder upper end is vertically mounted on, in parallel-groove, its lower end is arranged in the draw-in groove in the middle of aluminium foil folder pallet; Graphite Electrodes anchor top board width is greater than electrolyzer width; The height of aluminium foil corrosion frame is less than electrolyzer height 3-5cm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420275957.2U CN203976970U (en) | 2014-05-28 | 2014-05-28 | Circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420275957.2U CN203976970U (en) | 2014-05-28 | 2014-05-28 | Circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer |
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| Publication Number | Publication Date |
|---|---|
| CN203976970U true CN203976970U (en) | 2014-12-03 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420275957.2U Expired - Fee Related CN203976970U (en) | 2014-05-28 | 2014-05-28 | Circulating automatic constant-temperature aluminium foil sample corrosion electrolyzer |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106868579A (en) * | 2017-04-27 | 2017-06-20 | 南通南辉电子材料股份有限公司 | A kind of corrosion hair engaging aperture device for improving aluminium foil corrosion specific volume |
| CN108660503A (en) * | 2018-07-27 | 2018-10-16 | 南通海星电子股份有限公司 | A kind of temperature control system of aluminium foil hair engaging aperture slot |
-
2014
- 2014-05-28 CN CN201420275957.2U patent/CN203976970U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106868579A (en) * | 2017-04-27 | 2017-06-20 | 南通南辉电子材料股份有限公司 | A kind of corrosion hair engaging aperture device for improving aluminium foil corrosion specific volume |
| CN106868579B (en) * | 2017-04-27 | 2018-12-14 | 南通南辉电子材料股份有限公司 | A kind of corrosion hair engaging aperture device improving aluminium foil corrosion specific volume |
| CN108660503A (en) * | 2018-07-27 | 2018-10-16 | 南通海星电子股份有限公司 | A kind of temperature control system of aluminium foil hair engaging aperture slot |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141203 Termination date: 20150528 |
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| EXPY | Termination of patent right or utility model |