CN203971434U - A kind of device that reclaims benzinum in acidification oil sample of measuring - Google Patents
A kind of device that reclaims benzinum in acidification oil sample of measuring Download PDFInfo
- Publication number
- CN203971434U CN203971434U CN201420436147.0U CN201420436147U CN203971434U CN 203971434 U CN203971434 U CN 203971434U CN 201420436147 U CN201420436147 U CN 201420436147U CN 203971434 U CN203971434 U CN 203971434U
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- CN
- China
- Prior art keywords
- benzinum
- conical flask
- condenser pipe
- ground conical
- mouth glass
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- Investigating Or Analyzing Materials Using Thermal Means (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
A kind of device that reclaims benzinum in acidification oil sample of measuring, comprise heater, described heater is electric hot plate, on electric hot plate, place 500ml ground conical flask, 500ml ground conical flask connection standard mouth glass three-way, standard mouth glass three-way one end is provided with 500ml ground conical flask plug, and the other end connects condenser pipe, and condenser pipe output connects 500ml ground conical flask through standard mouth glass bend-head; Described condenser pipe one end is provided with emulsion tube and connects circulating water intake, and the other end is provided with emulsion tube and connects circulating water outlet; Described condenser pipe is arranged on cross clamp through condensing tube tongs, and cross clamp is arranged on iron stand.Use benzinum not change as principle as the amount of extractant benzinum before and after reaction, employing adds thermal distillation, condensation, recovery and directly obtains benzinum.Have easy and simple to handle, reclaim easy, with low cost, be easy to practical feature, and reduced testing cost, reduced environmental pollution, improved the security of operation.
Description
Technical field
The utility model relates to a kind of device that reclaims benzinum in acidification oil sample of measuring.
Background technology
Measuring in the process of acidification oil, add benzinum to be mainly used to extract the aliphatic acid in sample, then benzinum is evaporated, obtain the aliphatic acid oil content in sample.At present, we do not reclaim benzinum in the process that detects acidification oil, directly evaporate benzinum, have not only polluted environment, and have caused the wasting of resources, have increased the cost that detects acidification oil.And existing naked light electric furnace easily causes benzinum ignition.
Utility model content
Its object of the utility model is just to provide a kind of device that reclaims benzinum in acidification oil sample of measuring, use benzinum not change as principle as the amount of extractant benzinum before and after reaction, employing adds thermal distillation, condensation, recovery and directly obtains benzinum.Have easy and simple to handle, reclaim easy, with low cost, be easy to practical feature, and reduced testing cost, reduced environmental pollution, improved the security of operation.
The technical scheme that realizes above-mentioned purpose and take, comprise heater, described heater is electric hot plate, on electric hot plate, place 500ml ground conical flask, 500ml ground conical flask connection standard mouth glass three-way, standard mouth glass three-way one end is provided with 500ml ground conical flask plug, and the other end connects condenser pipe, and condenser pipe output connects 500ml ground conical flask through standard mouth glass bend-head; Described condenser pipe one end is provided with emulsion tube and connects circulating water intake, and the other end is provided with emulsion tube and connects circulating water outlet; Described condenser pipe is arranged on cross clamp through condensing tube tongs, and cross clamp is arranged on iron stand.
Compared with prior art the utlity model has following advantage.
1), easy and simple to handle, reclaim easy, with low cost, be easy to practicality;
2), there is certain economic worth and reduced testing cost;
3) reduce environmental pollution, improved the security of operation.
Brief description of the drawings
Below in conjunction with accompanying drawing, the utility model is described in further detail.
Fig. 1 is this apparatus structure schematic diagram.
Detailed description of the invention
Comprise heater, as shown in Figure 1, described heater is electric hot plate 1, on electric hot plate 1, place 500ml ground conical flask 2,500ml ground conical flask 2 connection standard mouth glass three-ways 3, standard mouth glass three-way 3 one end are provided with 500ml ground conical flask plug 4, and the other end connects condenser pipe 5, and condenser pipe 5 outputs connect 500ml ground conical flask 10 through standard mouth glass bend-head 9; Described condenser pipe 5 one end are provided with emulsion tube and connect circulating water intake 11, and the other end is provided with emulsion tube and connects circulating water outlet 12; Described condenser pipe 5 is arranged on cross clamp 7 through condensing tube tongs 6, and cross clamp 7 is arranged on iron stand 8.
Embodiment
Utilize while measuring acidification oil sample, use benzinum (30-60 DEG C of boiling ranges) as extractant, before and after reaction, the amount of benzinum does not change as principle.Employing adds thermal distillation, condensation, recovery and directly obtains benzinum (becoming liquid lower than 70 DEG C).
Heater replaces old-fashioned naked light electric furnace with electric hot plate, has avoided benzinum gas to meet the danger of naked light burning, improves the security of operation.
This device comprises electric hot plate 1,500ml ground conical flask 2, standard mouth glass three-way 3,500ml ground conical flask plug 4, condenser pipe 5, condensing tube tongs 6, cross clamp 7, iron stand 8, standard mouth glass bend-head 9,500ml ground conical flask 10, emulsion tube connects circulating water intake 11, and emulsion tube connects circulating water outlet 12.
1, with cross clamp 7, condensing tube tongs 6 is fixed on iron stand 8;
2, clamp condenser pipe 5 with condensing tube tongs 6;
3, the acidification oil sample with petroleum ether extraction is poured in 500ml ground conical flask 2, and flask is put on electric hot plate 1;
4, connect 500ml ground conical flask 2 and condenser pipe 5 with standard mouth glass three-way 3;
5, clog an outlet of standard mouth glass three-way 3 with 500ml ground conical flask plug 4;
6, connect another interface and the 500ml ground conical flask 10 of condenser pipe 5 with standard mouth glass bend-head 9;
7, connect circulating water intake 11 with emulsion tube;
8, open the heating of electric hot plate power supply.
Claims (1)
1. measure the device that reclaims benzinum in acidification oil sample for one kind, comprise heater, it is characterized in that, described heater is electric hot plate (1), the upper 500ml ground conical flask (2) of placing of electric hot plate (1), 500ml ground conical flask (2) connection standard mouth glass three-way (3), standard mouth glass three-way (3) one end is provided with 500ml ground conical flask plug (4), the other end connects condenser pipe (5), and condenser pipe (5) output connects 500ml ground conical flask (10) through standard mouth glass bend-head (9); Described condenser pipe (5) one end is provided with emulsion tube and connects circulating water intake (11), and the other end is provided with emulsion tube and connects circulating water outlet (12); It is upper that described condenser pipe (5) is arranged on cross clamp (7) through condensing tube tongs (6), and cross clamp (7) is arranged on iron stand (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420436147.0U CN203971434U (en) | 2014-08-05 | 2014-08-05 | A kind of device that reclaims benzinum in acidification oil sample of measuring |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420436147.0U CN203971434U (en) | 2014-08-05 | 2014-08-05 | A kind of device that reclaims benzinum in acidification oil sample of measuring |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203971434U true CN203971434U (en) | 2014-12-03 |
Family
ID=51968904
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420436147.0U Expired - Fee Related CN203971434U (en) | 2014-08-05 | 2014-08-05 | A kind of device that reclaims benzinum in acidification oil sample of measuring |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203971434U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
-
2014
- 2014-08-05 CN CN201420436147.0U patent/CN203971434U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110006774A (en) * | 2018-01-04 | 2019-07-12 | 中电电气(上海)太阳能科技有限公司 | A kind of cross linking degree tester of recyclable dimethylbenzene and its application |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141203 Termination date: 20160805 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |