CN203922756U - A kind of reactive tank exhaust heat-energy recycling system - Google Patents

A kind of reactive tank exhaust heat-energy recycling system Download PDF

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Publication number
CN203922756U
CN203922756U CN201420314124.2U CN201420314124U CN203922756U CN 203922756 U CN203922756 U CN 203922756U CN 201420314124 U CN201420314124 U CN 201420314124U CN 203922756 U CN203922756 U CN 203922756U
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CN
China
Prior art keywords
sulfuric acid
falling
hydrochloric acid
tank
circulation groove
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420314124.2U
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Chinese (zh)
Inventor
沙德宏
叶国华
刘新生
季新峰
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JIANGSU RUIHE FERTILIZER CO Ltd
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JIANGSU RUIHE FERTILIZER CO Ltd
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Priority to CN201420314124.2U priority Critical patent/CN203922756U/en
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Publication of CN203922756U publication Critical patent/CN203922756U/en
Expired - Fee Related legal-status Critical Current
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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Abstract

The utility model relates to a kind of reactive tank exhaust heat-energy recycling system, belt scale is arranged at conversion tank top, Repone K hopper is arranged at directly over belt scale, described sub-cylinder steam is through pipeline communication conversion tank, sulfuric acid preheater is shell shell and tube heat exchanger, the outlet of sulfuric acid storage tank is connected with conversion tank through sulfuric acid preheater shell side, conversion tank connects the input terminus of falling-film absorber through the tube side of sulfuric acid preheater, the output terminal of falling-film absorber connects hydrochloric acid circulation groove, hydrochloric acid circulation groove connects the input terminus of falling-film absorber through salt acid circulating pump, the output terminal of hydrochloric acid circulation groove connects hydrochloric acid storage tank through salt acid circulating pump.Native system has been recycled the heat energy of sulfuric acid and Repone K conversion reaction tail gas, reduces steam consumption, reduces coal consumption, power consumption.

Description

A kind of reactive tank exhaust heat-energy recycling system
Technical field
The utility model relates to a kind of fertilizer production equipment field, is specifically related to a kind of reactive tank exhaust heat-energy recycling system.
Background technology
Produce S-based compound fertilizer and generally first carry out after conversion reaction generates sal enixum slip delivering to subsequent handling with sulfuric acid and Repone K, also discharge the tail gas that contains hydrogen chloride gas simultaneously, after cooling absorbs, become salt acid product, instead of directly discharge.Although conversion reaction process is micro-heat release, but because hot slip and the tail gas that contains hydrogen chloride gas need constantly to discharge and take away a large amount of heat energy, easily reduce conversion reaction temperature and cannot normally produce, conventionally using steam heating to keep conversion reaction temperature, guaranteeing to reach the transformation efficiency index of regulation.In theory every production 1000kg S-based compound fertilizer need to consume 150kg(pressure be 0.8MPa) steam, the steam of supply produces with bunker coal.Outflow temperature is that the exhaust heat-energy of 100 DEG C is not utilized, and generally draws through the hydrochloric acid that falling-film absorber is lowered the temperature and circulation absorption production concentration is 31% then up to standard emptying by cigarette fontanel with induced draft fan.Therefore existing conversion reaction, in having consumed a large amount of coals and water resources, has been wasted again a large amount of utilized heat energy, and has coal-fired environmental pollution and the resource consumption causing.
Summary of the invention
For solving deficiency of the prior art, the purpose of this utility model is to provide a kind of chemical fertilizers production device of recycling reactive tank exhaust heat-energy.
For reaching above object, the technical scheme that the utility model is taked is:
A kind of reactive tank exhaust heat-energy recycling system comprises Repone K hopper, belt electronic scale, reactive tank, sub-cylinder steam, sulfuric acid storage tank, sulfuric acid preheater, falling-film absorber, hydrochloric acid circulation groove, salt acid circulating pump, hydrochloric acid storage tank and induced draft fan, described belt scale is arranged at conversion tank top, Repone K hopper is arranged at directly over belt scale, described sub-cylinder steam is through pipeline communication conversion tank, described sulfuric acid preheater is shell shell and tube heat exchanger, described sulfuric acid storage tank outlet is connected with conversion tank through sulfuric acid preheater shell side, described conversion tank connects the input terminus of falling-film absorber through the tube side of sulfuric acid preheater, the output terminal of described falling-film absorber connects hydrochloric acid circulation groove, described hydrochloric acid circulation groove connects the input terminus of falling-film absorber through salt acid circulating pump, the output terminal of described hydrochloric acid circulation groove connects hydrochloric acid storage tank through salt acid circulating pump.
Further, between the tube side of described falling-film absorber and sulfuric acid preheater, be provided with induced draft fan.
Further, between described falling-film absorber and sulfuric acid circulation groove, be provided with induced draft fan.
Again further, the open to atmosphere induced draft fan of the external company of described sulfuric acid circulation groove upper space.
Take after above technical scheme, the beneficial effects of the utility model are:
Utilize induced draft fan to introduce in sulfuric acid well heater sulfuric acid preheating passing into high-temperature tail gas in the conversion tank of high-temperature steam, reduced steam, effectively utilized the heat energy of tail gas; The tail gas of gas containing hydrogen chloride enters falling-film absorber after heat exchange cooling, has reduced the consumption of the water coolant passing in falling-film absorber.
The utility model has been recycled the heat energy of sulfuric acid and Repone K conversion reaction tail gas, reduce the steam consumption in conversion reaction process, reduce the coal consumption of follow-up baking operation, the power consumption of recirculated cooling water in induced draft and hydrogen chloride gas absorption process, stablize technic index, improve output and quality, reduced cost and environmental pollution.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model;
In figure: Repone K hopper 1, belt electronic scale 2, reactive tank 3, sub-cylinder steam 4, sulfuric acid storage tank 5, sulfuric acid preheating 6, falling-film absorber 7, hydrochloric acid circulation groove 8, hydrochloric acid circulation 9, hydrochloric acid storage tank 10, induced draft fan 11.
Embodiment
Below in conjunction with accompanying drawing, embodiment of the present utility model is further described:
As shown in the figure, a kind of chemical fertilizers production device of recycling reactive tank exhaust heat-energy comprises Repone K hopper 1, belt electronic scale 2, reactive tank 3, sub-cylinder steam 4, sulfuric acid storage tank 5, sulfuric acid preheater 6, falling-film absorber 7, hydrochloric acid circulation groove 8, hydrochloric acid circulation 9, hydrochloric acid storage tank 10 and induced draft fan 11.Repone K in Repone K hopper 1 enters in groove through reactive tank 3 its top feed mouths after 2 meterings of belt electronic scale, take over and enter in groove by reactive tank 3 tops after sulfuric acid preheater 6 preheating temperatures reach 50 DEG C in the sulfuric acid under the normal temperature state in sulfuric acid storage tank 5, the steam of 0.8MPa is taken over the 3 tops adapters of connection reactive tank by sub-cylinder steam 4 tops and is entered in groove, sulfuric acid and Repone K carry out conversion reaction and generate the tail gas of temperature at 120 DEG C of sal enixum slips and 100 DEG C of gas containing hydrogen chlorides, draw and sulfuric acid heat exchange in tube side and sulfuric acid preheater 6 shell sides of sulfuric acid preheater 6 through induced draft fan 11 at tail gas autoreaction groove 3 tops, temperature is down to 65 DEG C of left and right and by entering falling-film absorber 7 communicating pipe.Dilute hydrochloric acid in while hydrochloric acid circulation groove 8 is delivered to falling-film absorber 7 tops through salt acid circulating pump 9 and is mixed further absorbing hydrogen chloride gas with the tail gas of gas containing hydrogen chloride, sends in hydrochloric acid storage tank when concentration of hydrochloric acid reaches more than 31%.

Claims (4)

1. a reactive tank exhaust heat-energy recycling system, it is characterized in that, comprise Repone K hopper, belt electronic scale, reactive tank, sub-cylinder steam, sulfuric acid storage tank, sulfuric acid preheater, falling-film absorber, hydrochloric acid circulation groove, salt acid circulating pump, hydrochloric acid storage tank and induced draft fan, described belt scale is arranged at conversion tank top, Repone K hopper is arranged at directly over belt scale, described sub-cylinder steam is through pipeline communication conversion tank, described sulfuric acid preheater is shell shell and tube heat exchanger, described sulfuric acid storage tank outlet is connected with conversion tank through sulfuric acid preheater shell side, described conversion tank connects the input terminus of falling-film absorber through the tube side of sulfuric acid preheater, the output terminal of described falling-film absorber connects hydrochloric acid circulation groove, described hydrochloric acid circulation groove connects the input terminus of falling-film absorber through salt acid circulating pump, the output terminal of described hydrochloric acid circulation groove connects hydrochloric acid storage tank through salt acid circulating pump.
2. a kind of reactive tank exhaust heat-energy recycling system according to claim 1, is characterized in that, between the tube side of described falling-film absorber and sulfuric acid preheater, is provided with induced draft fan.
3. a kind of reactive tank exhaust heat-energy recycling system according to claim 1, is characterized in that, between described falling-film absorber and sulfuric acid circulation groove, is provided with induced draft fan.
4. a kind of reactive tank exhaust heat-energy recycling system according to claim 1, is characterized in that, the open to atmosphere induced draft fan of the external company of described sulfuric acid circulation groove upper space.
CN201420314124.2U 2014-06-13 2014-06-13 A kind of reactive tank exhaust heat-energy recycling system Expired - Fee Related CN203922756U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420314124.2U CN203922756U (en) 2014-06-13 2014-06-13 A kind of reactive tank exhaust heat-energy recycling system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420314124.2U CN203922756U (en) 2014-06-13 2014-06-13 A kind of reactive tank exhaust heat-energy recycling system

Publications (1)

Publication Number Publication Date
CN203922756U true CN203922756U (en) 2014-11-05

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Family Applications (1)

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CN (1) CN203922756U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104003426A (en) * 2014-06-13 2014-08-27 江苏瑞和化肥有限公司 System for recycling heat energy of tail gas in reaction tank
RU2616061C1 (en) * 2016-04-04 2017-04-12 Акционерное общество "Минерально-химическая компания "ЕвроХим" Installation for combined obtaining of phosphate salts and potassium sulphate

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104003426A (en) * 2014-06-13 2014-08-27 江苏瑞和化肥有限公司 System for recycling heat energy of tail gas in reaction tank
RU2616061C1 (en) * 2016-04-04 2017-04-12 Акционерное общество "Минерально-химическая компания "ЕвроХим" Installation for combined obtaining of phosphate salts and potassium sulphate
WO2017176164A1 (en) * 2016-04-04 2017-10-12 Акционерное общество "Минерально-химическая компания "ЕвроХим" Plant for the combined production of phosphate salts and potassium sulphate

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20141105

Termination date: 20180613