CN203909021U - Quinoline insoluble tester and quinoline insoluble testing device - Google Patents
Quinoline insoluble tester and quinoline insoluble testing device Download PDFInfo
- Publication number
- CN203909021U CN203909021U CN201420288414.4U CN201420288414U CN203909021U CN 203909021 U CN203909021 U CN 203909021U CN 201420288414 U CN201420288414 U CN 201420288414U CN 203909021 U CN203909021 U CN 203909021U
- Authority
- CN
- China
- Prior art keywords
- bottle
- quinoline
- toluene
- water bath
- pump
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn - After Issue
Links
Abstract
The utility model discloses a quinoline insoluble tester which comprises a thermostatic water bath, a toluene bottle, a quinoline bottle and a dissolution bottle which are arranged in the thermostatic water bath, a toluene pump, a quinoline pump, an extraction bottle communicated with the dissolution bottle, a suction filtration bottle arranged below the extraction bottle, a vacuumizing device connected with the suction filtration bottle, and a control device which is electrically connected with the thermostatic water bath, the toluene pump, the quinoline pump and the vacuumizing device. The utility model also discloses a quinoline insoluble testing device which comprises a box body, wherein the quinoline insoluble tester is arranged in the box body; an adsorption device for adsorbing toxic gases is arranged in the box body; and a door is arranged on the box body. According to the quinoline insoluble tester in the utility model, measurement of quinoline insoluble samples can be automatically finished, related standard requirements in the experimental process are met, and errors brought by manual operations are avoided. According to the quinoline insoluble testing device, harm of the toxic gases on a human body is eliminated, the measurement precision is high, and the data reproducibility is high.
Description
Technical field
The utility model belongs to quinoline insolubles detection technique field, particularly a kind of quinoline insolubles analyzer and quinoline non-soluble object measuring device.
Background technology
The domestic standard of measuring for coking asphalt product quinoline insolubles is GB/T2293-2008, and this standard has been stipulated test method and solvent temperature and consumption, washing times etc.At present domestic equipment is all manual operation, though solvent temperature, solvent load, dissolution time, washing times have standard-required, because operator's difference can vary with each individual.And these factors have determined the accuracy of measuring; Operating personnel work under poisonous and bad smell environment simultaneously, to health, can cause serious harm.
Existing quinoline insolubles determination techniques, is that dissolving bottle is put into water bath with thermostatic control, pours function funnel bottle into and fills in row vacuum filtration, then carry out repeatedly quinoline washing and toluene wash after artificial stirring and dissolving.Dissolution time, cleansing solution consumption are all rule of thumb determined by experimenter, therefore cause test findings to vary with each individual.
Utility model content
The utility model provides a kind of quinoline insolubles analyzer on the one hand, can automatically complete quinoline insolubles assay;
The utility model provides a kind of quinoline non-soluble object measuring device, the Health cost of operator being brought effectively to reduce toxic gas on the other hand.
In order to solve the problems of the technologies described above, the technical solution adopted in the utility model is:
A quinoline insolubles analyzer, comprising:
Water bath with thermostatic control;
Be arranged on toluene bottle, the quinoline bottle in described water bath with thermostatic control and dissolve bottle;
Extracting bottle, the top that it is arranged on described toluene bottle, quinoline bottle and dissolves bottle, is communicated with described dissolving bottle;
Toluene pump, it is for drawing toluene to extracting bottle from described toluene bottle;
Quinoline pump, it is for drawing quinoline to dissolving bottle from described quinoline bottle;
Be arranged on the bottle,suction of described extracting bottle below;
The vacuum extractor being connected with described bottle,suction;
With the control device that described water bath with thermostatic control, toluene pump, quinoline pump and vacuum extractor are electrically connected to, described control device is used for controlling lysate consumption, dissolution time, cleansing solution consumption, washing times and vacuum tightness.
Preferably, described control device comprises: proportion integration differentiation temperature controller and power regulator, described water bath with thermostatic control realizes thermostatic control by described proportion integration differentiation temperature controller and power regulator.
Preferably, described water bath with thermostatic control, comprising:
Stirrer, it is arranged on described water bath with thermostatic control bottom, and the rotating speed of described stirrer is controlled by described control device;
Well heater, it is arranged in described water bath with thermostatic control;
On described well heater, be provided with stationary barrier, be provided with the perforate for placing described toluene bottle, quinoline bottle and dissolving bottle on described stationary barrier, sidewall and the bottom of described water bath with thermostatic control are provided with insulation construction.
Preferably, described stirrer is magnetic stirring apparatus.
Preferably, the top of toluene bottle, quinoline bottle and dissolving bottle is provided with funnel bottle stopper.
Preferably, described toluene pump is connected with extracting bottle with described toluene bottle respectively by sebific duct; Described quinoline pump is connected with dissolving bottle with described quinoline bottle respectively by sebific duct; Described extracting bottle is also connected with described dissolving bottle by sebific duct; Described bottle,suction is connected with described vacuum extractor by plastic tube.
Preferably, described vacuum means is set to vacuum pump.
A kind of quinoline non-soluble object measuring device, comprise casing, quinoline insolubles analyzer described in above-mentioned any one is installed in described casing, is provided with for adsorbing the adsorbent equipment of toxic gas in described casing, described casing opens the door towards being provided with on the panel of quinoline insolubles analyzer.
Preferably, described adsorbent equipment comprises body, is provided with multilayer insulating panel groove on described body, is inserted with the dividing plate that activated charcoal or efficient solvent adsorbent are housed in every layer of septalium.
Preferably, on opening the door described in, lockset is housed.
Thereby the quinoline insolubles analyzer of the utility model embodiment is realized and is automatically completed the measurement of quinoline non-soluble matter sample to detecting the control of utensil by control device, and guarantees that experimentation meets relevant criterion requirement, the error of having avoided manual operation to bring.In addition, in the utility model, in the casing of quinoline non-soluble object measuring device, add adsorbent equipment, eliminated the harm of toxic gas to human body, promoted the security of this quinoline non-soluble object measuring device.
Accompanying drawing explanation
The schematic diagram of the quinoline insolubles analyzer that Fig. 1 provides for the utility model embodiment;
The schematic diagram of water bath with thermostatic control in the quinoline insolubles analyzer that Fig. 2 provides for the utility model embodiment;
The schematic diagram of the quinoline non-soluble object measuring device that Fig. 3 provides for the utility model embodiment;
The schematic diagram of adsorbent equipment in the quinoline non-soluble object measuring device that Fig. 4 provides for the utility model embodiment.
In figure, Reference numeral is: casing 10, toluene pump 31, quinoline pump 32, extracting bottle 33, funnel bottle stopper 34, toluene bottle 35, quinoline bottle 36, dissolving bottle 37, control device 38, water bath with thermostatic control 51, stationary barrier 52, well heater 53, stirrer 54, body 61, dividing plate 62.
Embodiment
Below in conjunction with the drawings and specific embodiments, the utility model is described in further detail:
The utility model embodiment provides a kind of quinoline insolubles analyzer, and as shown in Figure 1, this analyzer structure is as follows:
Water bath with thermostatic control 51, it can be existing water bath with thermostatic control, also can be improved existing water bath with thermostatic control, water bath with thermostatic control in the present embodiment 51 as shown in Figure 2, comprise: the stirrer 54 that is arranged on water bath with thermostatic control 51 bottoms, stirrer 54 is not more than 50mm apart from the distance of water bath with thermostatic control 51 bottoms, the preferred magnetic stirring apparatus of this stirrer 54, and the rotating speed of stirrer 54 is controlled by following control device 38.The interior well heater 53 that arranges of water bath with thermostatic control 51, is provided with stationary barrier 52 on well heater 53, be provided with the perforate for placing toluene bottle 35, quinoline bottle 36 and dissolving bottle 37 on stationary barrier 52, and sidewall and the bottom of water bath with thermostatic control 51 are provided with insulation construction.In water bath with thermostatic control 51, thermostatic control represents differentiation-differential by proportion integration differentiation temperature controller in following control device 38 (PID temperature controller, P represents that proportion-ratio, I represent integration-integration), D) and power regulator realize thermostatic control.
Toluene bottle 35, quinoline bottle 36 and dissolving bottle 37, volume is 50～200ml, by quartz glass, is made, and is placed in the perforate of described water bath with thermostatic control 51.Extracting bottle 33 is also 50～200ml for volume, is also to be made by quartz glass.
Toluene pump 31 is connected with extracting bottle 33 with toluene bottle 35 respectively by sebific duct; Quinoline pump 32 is connected with dissolving bottle 37 with quinoline bottle 36 respectively by sebific duct; Extracting bottle 33 is also connected with dissolving bottle 37 by sebific duct.Toluene pump 31 is for drawing toluene to extracting bottle 33 from toluene bottle 35; Quinoline pump 32 is for drawing quinoline to dissolving bottle 37 from quinoline bottle 36.The top of toluene bottle 35, quinoline bottle 36 and dissolving bottle 37 is provided with funnel bottle stopper 34, and funnel bottle stopper 34 facilitates adding of solution.The pump capacity of toluene pump 31 and quinoline pump 32 is 1～300ml/min, and feed control accuracy is 0.1～0.5ml/ time.
Extracting bottle 33 belows are provided with bottle,suction (not shown), and this bottle,suction is connected with vacuum extractor by plastic tube (preferably pvc pipe).The preferred vacuum pump (not shown) of vacuum extractor in the present embodiment, it can be also other vacuum extractor.Lysate and cleansing solution pump into after extracting bottle, then put into bottle,suction.
As shown in Figure 1, in quinoline insolubles analyzer, also comprise the control device 38 being electrically connected to water bath with thermostatic control 51, toluene pump 31, quinoline pump 32 and vacuum extractor, control device 38 is for controlling lysate consumption, dissolution time, cleansing solution consumption, washing times and vacuum tightness, this control device 38 can comprise the existing logic controller of single-chip microcomputer or Programmable Logic Controller or other, if aforementioned this control device 38 is for controlling rotating speed and the thermostatic control to water bath with thermostatic control 51 of water bath with thermostatic control 51 stirrers 54.This control device 38 comprises PID temperature controller and power regulator, and the thermostatic control of water bath with thermostatic control 51 is realized by PID temperature controller and power regulator exactly.
The operation of quinoline insolubles analyzer, strictly observe standard GB/T2293-2008, according to 38 pairs of lysate consumptions of this standard control device, dissolution time, cleansing solution consumption, washing times and vacuum tightness, controlled, when needs quinoline washs, control device 38 is controlled quinoline pump 32 and is extracted quinoline washing dissolving bottle 37, carries out suction filtration simultaneously.When needs toluene wash, control device 38 is controlled toluene pump extraction toluene and is washed to dissolving bottle 37 through extracting bottle 33, and whole process has been avoided personnel's direct control.
The utility model embodiment also provides a kind of quinoline non-soluble object measuring device, as shown in Figure 3, this device comprises casing 10, and above-mentioned quinoline insolubles analyzer is installed in casing 10, casing 10 opens the door towards being provided with L-type on the panel of quinoline insolubles analyzer, on opening the door, lockset is housed.In casing 10, be also provided with for adsorbing the adsorbent equipment of toxic gas.In experimentation, be convenient to experimental implementation when door is opened, door is shut rear assurance experimentation toxic gas by effectively suction filtration and absorption.
In the present embodiment, preferably, adsorbent equipment can adopt structure as shown in Figure 4, comprise body 61, it is packed in the side that casing 10 opens the door dorsad, on body 61, be provided with 10 layers of septalium (septalium be 5～10 layers more suitable), be inserted with the dividing plate 62 that activated charcoal is housed in every layer of septalium, septalium and dividing plate 62 junctions seal with sealing strip.Except activated charcoal, also can select other efficient solvent adsorbents.
Certainly, in actual applications, described adsorbent equipment also can be selected high efficiency particle air filter (High efficiency particulate air Filter is called for short HEPA), can also select other efficient adsorption devices, to this utility model, embodiment does not limit.
In sum, content of the present utility model is not limited in the above-described embodiments, and those skilled in the art can propose other embodiment easily according to guiding theory of the present utility model, within these embodiments are all included in scope of the present utility model.
Claims (10)
1. a quinoline insolubles analyzer, is characterized in that, comprising:
Water bath with thermostatic control (51);
Be arranged on toluene bottle (35), the quinoline bottle (36) in described water bath with thermostatic control (51) and dissolve bottle (37);
Extracting bottle (33), the top that it is arranged on described toluene bottle (35), quinoline bottle (36) and dissolves bottle (37), is communicated with described dissolving bottle (37);
Toluene pump (31), it is for drawing toluene to extracting bottle (33) from described toluene bottle (35);
Quinoline pump (32), it is for drawing quinoline to dissolving bottle (37) from described quinoline bottle (36);
Be arranged on the bottle,suction of described extracting bottle (33) below;
The vacuum extractor being connected with described bottle,suction;
With the control device (38) that described water bath with thermostatic control (51), toluene pump (31), quinoline pump (32) and vacuum extractor are electrically connected to, described control device (38) is for controlling lysate consumption, dissolution time, cleansing solution consumption, washing times and vacuum tightness.
2. quinoline insolubles analyzer according to claim 1, it is characterized in that: described control device (38) comprising: proportion integration differentiation temperature controller and power regulator, described water bath with thermostatic control (51) realizes thermostatic control by described proportion integration differentiation temperature controller and power regulator.
3. quinoline insolubles analyzer according to claim 1, is characterized in that: described water bath with thermostatic control (51) comprising:
Stirrer (54), it is arranged on described water bath with thermostatic control (51) bottom, and the rotating speed of described stirrer (54) is controlled by described control device (38);
Well heater (53), it is arranged in described water bath with thermostatic control (51);
On described well heater (53), be provided with stationary barrier (52), on described stationary barrier (52), be provided with the perforate for placing described toluene bottle (35), quinoline bottle (36) and dissolving bottle (37), sidewall and the bottom of described water bath with thermostatic control (51) are provided with insulation construction.
4. quinoline insolubles analyzer according to claim 3, is characterized in that: described stirrer (54) is magnetic stirring apparatus.
5. quinoline insolubles analyzer according to claim 1, is characterized in that: the top of toluene bottle (35), quinoline bottle (36) and dissolving bottle (37) is provided with funnel bottle stopper (34).
6. quinoline insolubles analyzer according to claim 1, is characterized in that: described toluene pump (31) is connected with extracting bottle (33) with described toluene bottle (35) respectively by sebific duct; Described quinoline pump (32) is connected with dissolving bottle (37) with described quinoline bottle (36) respectively by sebific duct; Described extracting bottle (33) is also connected with described dissolving bottle (37) by sebific duct; Described bottle,suction is connected with described vacuum extractor by plastic tube.
7. according to the quinoline insolubles analyzer described in any one in claim 1 to 6, it is characterized in that: described vacuum means is set to vacuum pump.
8. a quinoline non-soluble object measuring device, it is characterized in that: comprise casing (10), quinoline insolubles analyzer described in any one in claim 1 to 7 is installed in described casing (10), in described casing (10), be provided with for adsorbing the adsorbent equipment of toxic gas, described casing (10) opens the door towards being provided with on the panel of quinoline insolubles analyzer.
9. quinoline non-soluble object measuring device according to claim 8, it is characterized in that: described adsorbent equipment comprises body (61), described body is provided with multilayer insulating panel groove on (61), is inserted with the dividing plate (62) that activated charcoal or efficient solvent adsorbent are housed in every layer of septalium.
10. quinoline non-soluble object measuring device according to claim 8, is characterized in that: described in lockset is housed on opening the door.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420288414.4U CN203909021U (en) | 2014-05-30 | 2014-05-30 | Quinoline insoluble tester and quinoline insoluble testing device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420288414.4U CN203909021U (en) | 2014-05-30 | 2014-05-30 | Quinoline insoluble tester and quinoline insoluble testing device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203909021U true CN203909021U (en) | 2014-10-29 |
Family
ID=51783283
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201420288414.4U Withdrawn - After Issue CN203909021U (en) | 2014-05-30 | 2014-05-30 | Quinoline insoluble tester and quinoline insoluble testing device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203909021U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104062403A (en) * | 2014-05-30 | 2014-09-24 | 北京中仪励朗科技有限公司 | Quinoline insoluble tester and quinoline insoluble testing device |
-
2014
- 2014-05-30 CN CN201420288414.4U patent/CN203909021U/en not_active Withdrawn - After Issue
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104062403A (en) * | 2014-05-30 | 2014-09-24 | 北京中仪励朗科技有限公司 | Quinoline insoluble tester and quinoline insoluble testing device |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102539637B (en) | Environment testing device | |
| CN109596809B (en) | Simulation system for monitoring and analyzing dynamic release of pollutants in soil filler under leaching state | |
| CN101587031B (en) | Sealing gas sampling apparatus | |
| CN105823896A (en) | Multifunctional automatic sample injector | |
| CN107596865A (en) | A kind of charcoal absorption case for exhaust-gas treatment | |
| CN103344728B (en) | In-situ headspace sample injector | |
| CN203365398U (en) | In-situ headspace sample injector | |
| CN203909021U (en) | Quinoline insoluble tester and quinoline insoluble testing device | |
| CN203909023U (en) | Methylbenzene and quinoline insoluble measuring device | |
| CN104062403B (en) | Quinoline insolubles analyzer and quinoline non-soluble object measuring device | |
| CN206074605U (en) | A kind of petroleum components detection means | |
| CN109100259A (en) | A kind of shale gas generation resolver | |
| CN202362223U (en) | High-precision gas content tester | |
| CN111693652B (en) | Analysis method and treatment system for chlorine-containing waste gas generated by high-temperature water quenching of chlorination slag | |
| CN206161642U (en) | Extraction and desorption device | |
| CN107449930A (en) | A kind of liquid keeps sample sampler | |
| CN204789458U (en) | Chlorine ion content detection device | |
| CN110726640B (en) | Automatic determination device for coal sample gas adsorption constant | |
| CN114354324A (en) | Automatic cell wax block preparation instrument and method for preparing cell wax block based on same | |
| CN209656558U (en) | A kind of degradation gas analyzing apparatus | |
| CN105334072A (en) | Sealed faeces sample sampling container and sampling method | |
| CN103100363B (en) | Automatic derivatization reaction processing equipment and method | |
| CN207232111U (en) | A kind of easy to operate Oxygen bottle combustion device | |
| CN207164077U (en) | A kind of liquid keeps sample sampler | |
| CN205280635U (en) | Quick lime activity degree short -term test appearance that sintering used |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20141029 Effective date of abandoning: 20151216 |
|
| C25 | Abandonment of patent right or utility model to avoid double patenting |