CN203904312U - Extraction and purification device for effective components in essential oil of fresh gingers - Google Patents
Extraction and purification device for effective components in essential oil of fresh gingers Download PDFInfo
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- CN203904312U CN203904312U CN201420302368.9U CN201420302368U CN203904312U CN 203904312 U CN203904312 U CN 203904312U CN 201420302368 U CN201420302368 U CN 201420302368U CN 203904312 U CN203904312 U CN 203904312U
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Abstract
The utility model provides an extraction and purification device for effective components in essential oil of fresh gingers. An ultrasound enzyme fermentation extraction device (1), a horizontal screw-discharge sedimentation centrifugal device (2), an ultrafiltration membrane separation device (3), a nanofiltration membrane separation device (4), a silica gel column separation device (5), a macroporous resin purification device (6), a molecular distillation device (7) and a high-speed countercurrent chromatography preparation device (8) are artfully combined through serial connection to extract, concentrate and purify components such as gingerol and the like in the fresh gingers, and extraction, concentration, purification and separation are integrated, so that the equipment is simplified, the process flow is greatly simplified, the extraction and purification efficiencies are greatly increased, the energy consumption and the cost are reduced, and the extraction and purification device is convenient to operate; and in addition, the extraction and purification device is safe and reliable in production and is a better continuous extraction and purification device for the effective components in the essential oil of the fresh gingers.
Description
Technical field
The utility model belongs to the extraction and separation technology field of effective ingredients in plant in pharmaceutical engineering, particularly a kind of device for extracts active ingredients purifying such as ginger essential oil gingerols.
Background technology
Ginger refers to the rhizome of Zingiber herbaceous plant ginger, contains pungent and fragrance ingredient, is a kind of important tubers spices.It includes volatile oil, is mainly zingiberol, zingiberene, phellandrene, citral, phantol etc.; Containing pungency component gingerol, can decompose and generate zingiberone, ginger ketenes etc. again.In addition, also contain asparagine, L-glutamic acid, aspartic acid, Serine, glycine, Threonine, L-Ala etc., have medicinal and edibleness concurrently.
At present, on market is mainly to utilize ginger oil volatility and water-fast characteristic for ginger essential oil material active ingredient extraction equipment, adopt steam distillation, utilize steam generator, distiller and condenser etc., by after ginger oil distillation, cooling, oily water separation, obtain finished product Oils, Zingiber officinale, have the defects such as the second-rate or effective constituent separating effect of product is bad, therefore must find better isolation technique.
Summary of the invention
For the shortcoming of prior art, the purpose of this utility model is to provide in a kind of ginger the effective constituent such as gingerol in ginger essential oil and extracts continuously purification devices, substep extracts continuously purification devices effective constituents such as gingerols in ginger essential oil in ginger and extracts, and carry out purification process, not high to overcome DNA purity, the problem that the wasting of resources is large has solved complex operation and inefficiency simultaneously, realizes the maximization of the utilization of resources.
For achieving the above object, the technical solution of the utility model is: a kind of ginger essential oil extracts active ingredients purification devices, by ultrasonic wave fermentation, extraction device (1), horizontal spiral discharge sedimentation centrifugal device (2), ultrafiltration membrane separating device (3), nanofiltration membrane separation device (4), silicagel column tripping device (5), macroporous resin purification device (6), molecular distillation apparatus (7), high speed adverse current chromatogram preparation facilities (8) composition, it is characterized in that ultrasonic wave fermentation, extraction device (1) is connected with horizontal spiral discharge sedimentation centrifugal device (2) by pipeline, horizontal spiral discharge sedimentation centrifugal device (2) is connected with ultrafiltration membrane separating device (3) by pipeline, ultrafiltration membrane separating device (3) is connected with nanofiltration membrane separation device (4) by pipeline, nanofiltration membrane separation device (4) is connected with silicagel column tripping device (5) by pipeline, silicagel column tripping device (5) is connected with macroporous resin purification device (6) and molecular distillation apparatus (7) by pipeline, molecular distillation apparatus (7) is connected with high speed adverse current chromatogram preparation facilities (8) by pipeline.
Concrete, above-described a kind of ginger essential oil extracts active ingredients purification devices, is characterized in that: described ultrasonic wave fermentation, extraction device (1) is provided with ultrasonic generator, temperature regulator, pressure controller, whipping appts.
Concrete, above-described a kind of ginger essential oil extracts active ingredients purification devices, is characterized in that: the rotating speed of described horizontal spiral discharge sedimentation centrifugal device (2) is 4000r/min.
Concrete, above-described a kind of ginger essential oil extracts active ingredients purification devices, is characterized in that: described ultrafiltration membrane separating device (3) adopts the modification ps hollow fiber uf membrane assembly of molecular weight cut-off 6000.
Concrete, above-described a kind of ginger essential oil extracts active ingredients purification devices, is characterized in that: described nanofiltration membrane separation device (4) adopts the hollow fiber nanofiltration membrane assembly of molecular weight cut-off 1000.
[0010]a kind of ginger essential oil extracts active ingredients purification devices described in the utility model, it adopts ultrasonic wave fermentation, extraction device (1), horizontal spiral discharge sedimentation centrifugal device (2), ultrafiltration membrane separating device (3), nanofiltration membrane separation device (4), silicagel column tripping device (5), macroporous resin purification device (6), molecular distillation apparatus (7), high speed adverse current chromatogram preparation facilities (8) series combination carries out the extraction of the effective constituent such as gingerol in ginger essential oil in ginger, concentrated, purifying, greatly improve extraction, purification efficiency, save energy consumption, reduce cost, easy to operate, and production safety is reliable, it is ginger essential oil in a kind of ginger preferably, gingerol extracts purification devices continuously.
Brief description of the drawings
Below in conjunction with drawings and Examples, the utility model is further illustrated.
Fig. 1 is the structural representation of a kind of ginger essential oil extracts active ingredients of the utility model purification devices;
Accompanying drawing is detailed as follows: 1, ultrasonic wave fermentation, extraction device, 2, horizontal spiral discharge sedimentation centrifugal device, 3, ultrafiltration membrane separating device, 4, nanofiltration membrane separation device, 5, silicagel column tripping device, 6, macroporous resin purification device, 7, molecular distillation apparatus, 8, high speed adverse current chromatogram preparation facilities.
Embodiment
Below preferred embodiment of the present utility model is described, should be appreciated that preferred embodiment described herein is only for description and interpretation the utility model, and be not used in restriction the utility model.
Embodiment 1
As shown in Fig. 1, a kind of ginger essential oil extracts active ingredients purification devices, comprises successively connected ultrasonic wave fermentation, extraction device (1), horizontal spiral discharge sedimentation centrifugal device (2), ultrafiltration membrane separating device (3), nanofiltration membrane separation device (4), silicagel column tripping device (5), macroporous resin purification device (6), molecular distillation apparatus (7), high speed adverse current chromatogram preparation facilities (8).
Described ultrasonic wave fermentation, extraction device (1) is connected with horizontal spiral discharge sedimentation centrifugal device (2) by pipeline.Described horizontal spiral discharge sedimentation centrifugal device (2) is connected with ultrafiltration membrane separating device (3) by pipeline.Described ultrafiltration membrane separating device (3) is connected with nanofiltration membrane separation device (4) by pipeline.Described nanofiltration membrane separation device (4) is connected with silicagel column tripping device (5) by pipeline.Described silicagel column tripping device (5) is connected with macroporous resin purification device (6) and molecular distillation apparatus (7) by pipeline.Described molecular distillation apparatus (7) is connected with high speed adverse current chromatogram preparation facilities (8) by pipeline.
Described ultrasonic wave fermentation, extraction device (1) is provided with ultrasonic generator, temperature regulator, pressure controller, whipping appts.The rotating speed of described horizontal spiral discharge sedimentation centrifugal device (2) is 4000r/min.Described ultrafiltration membrane separating device (3) adopts the modification ps hollow fiber uf membrane assembly of molecular weight cut-off 6000.Described nanofiltration membrane separation device (4) adopts the hollow fiber nanofiltration membrane assembly of molecular weight cut-off 1000.
First adopt ultrasonic wave fermentation, extraction device (1) to extract the dry ginger after pulverizing, after extraction, entering horizontal spiral discharge sedimentation centrifugal device (2) separates, parting liquid is after ultrafiltration membrane separating device (3) and nanofiltration membrane separation device (4) are processed, enter silicagel column tripping device (5) and carry out chromatographic separation, adopt normal hexane: ethyl ester ethyl ester (volume ratio 2:1) carries out wash-out one time, elutriant enters macroporous resin purification device (6) to carry out purifying and obtains gingerol.Adopt sherwood oil to carry out secondary wash-out, elutriant enters molecular distillation apparatus (7) and separates, and enters high speed adverse current chromatogram preparation facilities (8) and carries out separation and purification.
Described a kind of ginger essential oil extracts active ingredients purification devices of the present utility model, by ultrasonic wave fermentation, extraction device (1), horizontal spiral discharge sedimentation centrifugal device (2), ultrafiltration membrane separating device (3), nanofiltration membrane separation device (4), silicagel column tripping device (5), macroporous resin purification device (6), molecular distillation apparatus (7), high speed adverse current chromatogram preparation facilities (8) dexterously series combination carries out the extraction of the composition such as gingerol in ginger essential oil in ginger, concentrated, purifying, treasury is got, separate, concentrated, purifying is integrated, simplify equipment, greatly simplify technical process, greatly improve extraction, purification efficiency, save energy consumption, reduce cost, easy to operate, and production safety is reliable, be in a kind of ginger preferably in ginger essential oil the composition such as gingerol extract continuously purification devices.
Claims (5)
1. a ginger essential oil extracts active ingredients purification devices, by ultrasonic wave fermentation, extraction device (1), horizontal spiral discharge sedimentation centrifugal device (2), ultrafiltration membrane separating device (3), nanofiltration membrane separation device (4), silicagel column tripping device (5), macroporous resin purification device (6), molecular distillation apparatus (7), high speed adverse current chromatogram preparation facilities (8) composition, it is characterized in that ultrasonic wave fermentation, extraction device (1) is connected with horizontal spiral discharge sedimentation centrifugal device (2) by pipeline, horizontal spiral discharge sedimentation centrifugal device (2) is connected with ultrafiltration membrane separating device (3) by pipeline, ultrafiltration membrane separating device (3) is connected with nanofiltration membrane separation device (4) by pipeline, nanofiltration membrane separation device (4) is connected with silicagel column tripping device (5) by pipeline, silicagel column tripping device (5) is connected with macroporous resin purification device (6) and molecular distillation apparatus (7) by pipeline, molecular distillation apparatus (7) is connected with high speed adverse current chromatogram preparation facilities (8) by pipeline.
2. a kind of ginger essential oil extracts active ingredients purification devices according to claim 1, is characterized in that: described ultrasonic wave fermentation, extraction device is provided with ultrasonic generator, temperature regulator, pressure controller, whipping appts.
3. a kind of ginger essential oil extracts active ingredients purification devices according to claim 1, is characterized in that: the rotating speed of described horizontal spiral discharge sedimentation centrifugal device is 4000r/min.
4. a kind of ginger essential oil extracts active ingredients purification devices according to claim 1, is characterized in that: described ultrafiltration membrane separating device (3) adopts the modification ps hollow fiber uf membrane assembly of molecular weight cut-off 6000.
5. a kind of ginger essential oil extracts active ingredients purification devices according to claim 1, is characterized in that: described nanofiltration membrane separation device (4) adopts the hollow fiber nanofiltration membrane assembly of molecular weight cut-off 1000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420302368.9U CN203904312U (en) | 2014-06-09 | 2014-06-09 | Extraction and purification device for effective components in essential oil of fresh gingers |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420302368.9U CN203904312U (en) | 2014-06-09 | 2014-06-09 | Extraction and purification device for effective components in essential oil of fresh gingers |
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| CN203904312U true CN203904312U (en) | 2014-10-29 |
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| CN201420302368.9U Expired - Fee Related CN203904312U (en) | 2014-06-09 | 2014-06-09 | Extraction and purification device for effective components in essential oil of fresh gingers |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105748580A (en) * | 2016-03-15 | 2016-07-13 | 中国科学院过程工程研究所 | Low-temperature extraction device and method of active ingredients of natural products |
| CN108244151A (en) * | 2017-12-26 | 2018-07-06 | 刘志刚 | A kind of extracting method of clove bud oil for mite killing |
-
2014
- 2014-06-09 CN CN201420302368.9U patent/CN203904312U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105748580A (en) * | 2016-03-15 | 2016-07-13 | 中国科学院过程工程研究所 | Low-temperature extraction device and method of active ingredients of natural products |
| CN108244151A (en) * | 2017-12-26 | 2018-07-06 | 刘志刚 | A kind of extracting method of clove bud oil for mite killing |
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| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141029 Termination date: 20190609 |