CN203900494U - Nano-zinc particle preparation device - Google Patents

Nano-zinc particle preparation device Download PDF

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Publication number
CN203900494U
CN203900494U CN201420335593.2U CN201420335593U CN203900494U CN 203900494 U CN203900494 U CN 203900494U CN 201420335593 U CN201420335593 U CN 201420335593U CN 203900494 U CN203900494 U CN 203900494U
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CN
China
Prior art keywords
nano
importer
zinc
reaction promoter
particle preparation
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CN201420335593.2U
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Chinese (zh)
Inventor
徐良
李韵秋
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Nanjing pioneer synergy Nanometer Technology Co., Ltd.
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JIANGSU KAISHANG ENERGY SAVING TECHNOLOGY Co Ltd
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Abstract

The utility model discloses a nano-zinc particle preparation device. The nano-zinc particle preparation device comprises a program control ultrasonic generator, an ultrasonic reaction tank body, a gas importer and a reaction promoter importer, wherein the program control ultrasonic generator is arranged in the center position right above the ultrasonic reaction tank body, and the gas importer and the reaction promoter importer are arranged in the edge position above the ultrasonic reaction tank body; the gas importer and the reaction promoter importer are respectively arranged in symmetrical positions of two sides of the program control ultrasonic generator; importing pipes of the gas importer and the reaction promoter importer are both electric telescopic importing pipes and can be returned to sleeves in a shrinking way after the importing of reaction promoter and gas is carried out. According to the nano-zinc particle preparation device disclosed by the utility model, the design is novel, the operation is simple and easy, the production maintenance cost is low, nano-zinc particles which are prepared by utilizing the nano-zinc particle preparation device are used for sterilization and disinfection, compared with a traditional technology, the effect of the nano-zinc particles is 20 times stronger than that of nano-zinc oxide, and the effect of sterilizing 99.9% of bacteria, fungus and the like can be achieved just by a very low dose.

Description

A kind of Nano-Zinc particle preparation facilities
Technical field
The utility model relates to nano metal material technical field, discloses a kind of Nano-Zinc particle preparation facilities.
Background technology
Nano-Zinc material Heat stability is good, can adsorb, one direct sum is killed bacterium, there is good anti-bacterial effect, timeliness is long, safe, the features such as price competition, through general notary (SOCIETE GENERALE DE SURVEILLANCE S.A., SGS) in oral anxious toxicity, skin irritatin, in sensitivity experiments, confirm, product has tight security and antimicrobial long-acting ability, can be applicable to food future, medicine, health products, cosmetics, articles for daily use, textile fabric, fish livestock-raising, the industries such as agricultural planting, prepare the various sterilizations that have, the product of antibacterial and antibacterial action.
Tradition nano metal (zinc) powder is scattered in cold coating, conventionally need disperse by mechanical lapping, and its nano-milled dispersion machine, exists the shortcomings such as cost is high, loss is high, maintenance cost is high, and therefore, the application of Nano metal powder has certain difficulty degree.The Nano-Zinc of conventional art, very easily oxidation, i.e. nano zine oxide (former Nano-Zinc powder, surface has changed its active structure, be converted to oxidation state, passivation and deactivated zinc oxide), have that sterilizing rate is low, persistence is poor, high in cost of production situation, be difficult to realize industrial applicability.
Utility model content
The utility model provides a kind of Nano-Zinc particle preparation facilities, easy and simple to handle, production maintenance cost is low, and the Nano-Zinc particle of preparation is easy to disperse, easy to use.
In order to reach above technique effect, the technical solution of the utility model is as follows:
A Nano-Zinc particle preparation facilities, comprises program control supersonic generator, ultrasonic response cell body, gas inducting device, reaction promoter inducting device.
Described program control supersonic generator is arranged at center directly over ultrasonic response cell body, and described gas inducting device and reaction promoter inducting device are arranged at ultrasonic response cell body top edges position.
Further, described gas inducting device and reaction promoter inducting device are placed in respectively the bilateral symmetry position of supersonic generator.
Preferably, the ingress pipe of described gas inducting device and reaction promoter inducting device is electric telescopic ingress pipe, after executing importing reaction promoter and gas, in collapsible time sleeve pipe.
This practical using method is as follows:
First-selection utilizes Nano-Zinc predecessor to add solvent, is configured to Nano-Zinc particle precursor liquid, inserts ultrasonic response cell body, opens supersonic generator and carries out ultrasonic irradiation, opens gas inducting device to produce cavitation erosion effect simultaneously; Reaction is carried out in process, can open reaction promoter inducting device in reaction hot-zone, add polymer electrolyte interfacial agent, reducing agent and stabilization agent with guarantee reaction continue carry out; After reaction finishes, collect the zinc particles that abovementioned steps is peeled off generation, import vacuum high-temperature baking oven and carry out recrystallization, can obtain be easy to disperse, Nano-Zinc particle easy to use.
Apply a kind of Nano-Zinc particle preparation facilities of the present utility model, there is following technique effect: the utility model is novel in design, operate simple and easy, production maintenance cost is low, the Nano-Zinc particle that utilizes the utility model to prepare, for sterilization sterilizing, effect is stronger 20 times than the nano zine oxide of conventional art, only need very low dose can reach the killing effect to bacterium, fungi etc. 99.9%, in process of production, without any waste water or generation of waste materials, production cost is low, there is high activity simultaneously, overcome the unstability of traditional Nano-Zinc or easily lost its sterilizing ability.The Nano-Zinc particle that the utility model technology is prepared, is easy to diffusion, on all types of coating adds, with simple and easy mixing plant, can complete.The utility model not only can use identical operation and technology to prepare other metal nanoparticles for the preparation of Nano-Zinc particle, also has fabulous effect.
Accompanying drawing explanation
Accompanying drawing described herein is used to provide further understanding of the present utility model, forms the application's a part, does not form to improper restriction of the present utility model, in the accompanying drawings:
Fig. 1 is the utility model structural representation.
The specific embodiment
Below in conjunction with accompanying drawing and specific embodiment, describe the utility model in detail, in this illustrative examples of the present utility model and explanation, be used for explaining the utility model, but not as to restriction of the present utility model.
Embodiment 1:
The present embodiment provides a kind of Nano-Zinc particle preparation facilities, and structure as shown in Figure 1, comprises program control supersonic generator 1, ultrasonic response cell body 2, gas inducting device 3, reaction promoter inducting device 4.
Described program control supersonic generator 1 is arranged at center directly over ultrasonic response cell body 2, and described gas inducting device 3 and reaction promoter inducting device 4 are arranged at ultrasonic response cell body 2 top edges positions; Described gas inducting device 3 and reaction promoter inducting device 4 are placed in respectively the bilateral symmetry position of supersonic generator 1; The ingress pipe 5 of described gas inducting device 3 and reaction promoter inducting device 4 is electric telescopic ingress pipe, after executing importing reaction promoter and gas, in collapsible time sleeve pipe 6.
A kind of Nano-Zinc particle preparation facilities of the present embodiment, its using method is as follows:
First-selection utilizes Nano-Zinc predecessor to add solvent, is configured to Nano-Zinc particle precursor liquid, inserts in ultrasonic response cell body 2, opens supersonic generator 1 and carries out ultrasonic irradiation, opens gas inducting device 3 to produce cavitation erosion effect simultaneously; Reaction is carried out in process, can open reaction promoter inducting device 4 in reaction hot-zone, add polymer electrolyte interfacial agent, reducing agent and stabilization agent with guarantee reaction continue carry out; After reaction finishes, collect the zinc particles that abovementioned steps is peeled off generation, import vacuum high-temperature baking oven and carry out recrystallization, can obtain be easy to disperse, Nano-Zinc particle easy to use.
The utility model is novel in design, operate simple and easyly, production maintenance cost is low, the Nano-Zinc particle that utilizes the utility model to prepare, for sterilization sterilizing, effect is stronger 20 times than the nano zine oxide of conventional art, only needs very low dose can reach the killing effect to bacterium, fungi etc. 99.9%, in process of production, without any waste water or generation of waste materials, production cost is low, has high activity simultaneously, has overcome the unstability of traditional Nano-Zinc or has easily lost its sterilizing ability.The Nano-Zinc particle that the utility model technology is prepared, is easy to diffusion, on all types of coating adds, with simple and easy mixing plant, can complete.The utility model not only can use identical operation and technology to prepare other metal nanoparticles for the preparation of Nano-Zinc particle, also has fabulous effect.
The above is preferred embodiment of the present utility model; it should be pointed out that for those skilled in the art, do not departing under the prerequisite of the utility model principle; can also make some improvements and modifications, these improvements and modifications are also considered as protection domain of the present utility model.

Claims (3)

1. a Nano-Zinc particle preparation facilities, comprise program control supersonic generator, ultrasonic response cell body, gas inducting device, reaction promoter inducting device, it is characterized in that: described program control supersonic generator is arranged at center directly over ultrasonic response cell body, and described gas inducting device and reaction promoter inducting device are arranged at ultrasonic response cell body top edges position.
2. a kind of Nano-Zinc particle preparation facilities according to claim 1, is characterized in that: described gas inducting device and reaction promoter inducting device are placed in respectively the bilateral symmetry position of supersonic generator.
3. according to a kind of Nano-Zinc particle preparation facilities described in claim 1 or 2 any one, it is characterized in that: the ingress pipe of described gas inducting device and reaction promoter inducting device is electric telescopic ingress pipe, after executing importing reaction promoter and gas, in collapsible time sleeve pipe.
CN201420335593.2U 2014-06-23 2014-06-23 Nano-zinc particle preparation device Active CN203900494U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420335593.2U CN203900494U (en) 2014-06-23 2014-06-23 Nano-zinc particle preparation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420335593.2U CN203900494U (en) 2014-06-23 2014-06-23 Nano-zinc particle preparation device

Publications (1)

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CN203900494U true CN203900494U (en) 2014-10-29

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106587290A (en) * 2016-11-25 2017-04-26 北京科技大学 Method for improving sterilization efficiency of nanometer zinc oxide under ultrasonic action by additionally using atmospheric condition

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106587290A (en) * 2016-11-25 2017-04-26 北京科技大学 Method for improving sterilization efficiency of nanometer zinc oxide under ultrasonic action by additionally using atmospheric condition
CN106587290B (en) * 2016-11-25 2020-05-08 北京科技大学 Synergistic method for sterilizing nano zinc oxide under action of ultrasonic waves under atmosphere condition

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ASS Succession or assignment of patent right

Owner name: NANJING PENGTENG SCIENCE AND TRADE CO., LTD.

Free format text: FORMER OWNER: JIANGSU KAISHANG ENERGY SAVING TECHNOLOGY CO., LTD.

Effective date: 20150320

C41 Transfer of patent application or patent right or utility model
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Effective date of registration: 20150320

Address after: Horses Street Village in Qixia District of Nanjing city fruit market in Jiangsu province 210000

Patentee after: NANJING PANTENG TECHNOLOGY AND TRADE CO., LTD.

Address before: No. 18 Qixia Xianlin Avenue District of Nanjing City, Jiangsu province 210000

Patentee before: Jiangsu Kaishang Energy Saving Technology Co., Ltd.

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20161228

Address after: Pai Lou Xiang, Gulou District of Nanjing city in Jiangsu province 210029 No. 47 6 floor

Patentee after: Jiangsu Zhongxing surplus Trade Group Co., Ltd.

Address before: Horses Street Village in Qixia District of Nanjing city fruit market in Jiangsu province 210000

Patentee before: NANJING PANTENG TECHNOLOGY AND TRADE CO., LTD.

TR01 Transfer of patent right

Effective date of registration: 20171201

Address after: 210038 Jiangsu province Nanjing HENGFA economic and Technological Development Zone, Road No. 30-4 floor two

Patentee after: Nanjing pioneer synergy Nanometer Technology Co., Ltd.

Address before: Pai Lou Xiang, Gulou District of Nanjing city in Jiangsu province 210029 No. 47 6 floor

Patentee before: Jiangsu Zhongxing surplus Trade Group Co., Ltd.

TR01 Transfer of patent right