CN203894183U - Hemispherical emittance tester based on balanced-state heat meter measurement method - Google Patents
Hemispherical emittance tester based on balanced-state heat meter measurement method Download PDFInfo
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- 238000000034 method Methods 0.000 claims abstract description 29
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- 238000010438 heat treatment Methods 0.000 claims abstract description 25
- 238000001816 cooling Methods 0.000 claims abstract description 19
- 238000009792 diffusion process Methods 0.000 claims description 24
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 14
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- 238000005485 electric heating Methods 0.000 description 1
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Abstract
一种稳态量热计法半球发射率测试仪,包括真空室、试样加热组件、抽真空装置、恒温冷却装置以及数据测量与处理装置;真空室包括真空罩以及固设在真空罩内壁上的热沉;试样加热组件设置在真空室对试样进行加热,包括主加热器;抽真空装置与该真空室的真空测试空间连通;恒温冷却装置与真空室的冷却介质通道连通;数据测量与处理装置采集试样温度、热沉温度、真空室内真空度以及主加热器的功率,并计算出试样的半球发射率。克服了测试过程对材料导热系数与比热容的苛刻要求,测试精度高,测试温区宽,可以测试材料在不同温度条件下尤其是在低温下的半球发射率。利用该测试装置的测试结果,可方便地计算出材料的半球发射率,测试与计算较简单。
A steady-state calorimeter hemispherical emissivity tester, comprising a vacuum chamber, a sample heating component, a vacuum device, a constant temperature cooling device, and a data measurement and processing device; the vacuum chamber includes a vacuum cover and is fixed on the inner wall of the vacuum cover The heat sink; the sample heating component is set in the vacuum chamber to heat the sample, including the main heater; the vacuum device is connected with the vacuum test space of the vacuum chamber; the constant temperature cooling device is connected with the cooling medium channel of the vacuum chamber; the data measurement The temperature of the sample, the temperature of the heat sink, the vacuum degree in the vacuum chamber and the power of the main heater are collected with the processing device, and the hemispherical emissivity of the sample is calculated. It overcomes the strict requirements of the test process on the thermal conductivity and specific heat capacity of the material. It has high test accuracy and a wide test temperature range. It can test the hemispherical emissivity of materials under different temperature conditions, especially at low temperatures. Using the test results of the test device, the hemispherical emissivity of the material can be conveniently calculated, and the test and calculation are relatively simple.
Description
技术领域technical field
本实用新型涉及半球发射率测试仪领域,尤其是一种稳态量热计法半球发射率测试仪。The utility model relates to the field of hemispherical emissivity testers, in particular to a hemispherical emissivity tester with a steady-state calorimeter method.
背景技术Background technique
半球发射率是固体材料的一个重要物理性能参数,它体现了材料在特定温度下相对黑体的辐射能力。材料半球发射率的测试方法包括卡计法和光学方法。其中卡计法又包括瞬态卡计法和稳态卡计法(稳态量热计法)。瞬态卡计法能在较短的时间内连续测量试样在不同温度条件下的发射率,但在测试中要求试样的导热性好,以保证在冷却过程中试样内部没有温度梯度。因而,用其测试低热导率材料的半球发射率较为困难。此外,采用瞬态卡计法需获取材料在不同温度下的比热容,然而许多新型功能材料热控材料的热力学参数非常缺乏,这也限制了瞬态卡计法的应用。Hemispherical emissivity is an important physical performance parameter of solid materials, which reflects the radiation ability of materials relative to black bodies at specific temperatures. The test methods for material hemispherical emissivity include card meter method and optical method. The calorimeter method includes the transient calorimeter method and the steady-state calorimeter method (steady-state calorimeter method). The transient card meter method can continuously measure the emissivity of the sample under different temperature conditions in a short period of time, but it requires good thermal conductivity of the sample during the test to ensure that there is no temperature gradient inside the sample during the cooling process. Therefore, it is difficult to use it to test the hemispherical emissivity of low thermal conductivity materials. In addition, the specific heat capacity of materials at different temperatures needs to be obtained by using the transient calorimetric method. However, the thermodynamic parameters of many new functional materials and thermal control materials are very scarce, which also limits the application of the transient calorimetric method.
实用新型内容Utility model content
为了满足热辐射材料特别是隔热涂料在不同温度条件下尤其是低温下热发射率的测量要求,本实用新型合理设计了一台基于稳态量热计法的半球发射率测试仪。In order to meet the measurement requirements of heat radiation materials, especially heat insulation coatings, under different temperature conditions, especially at low temperatures, the utility model rationally designs a hemispherical emissivity tester based on the steady-state calorimeter method.
为了达到上述目的,本实用新型采用以下技术方案:一种稳态量热计法半球发射率测试仪,包括真空室、试样加热组件、抽真空装置、恒温冷却装置以及数据测量与处理装置;In order to achieve the above object, the utility model adopts the following technical solutions: a steady-state calorimeter method hemispherical emissivity tester, including a vacuum chamber, a sample heating component, a vacuum device, a constant temperature cooling device, and a data measurement and processing device;
所述真空室包括真空罩以及固设在真空罩内壁上呈半包围状的热沉;所述热沉朝内的一面构成真空测试空间,朝外的一面与真空罩的内壁之间留有一条冷却介质通道;所述冷却介质通道内设有一冷却介质入口与冷却介质出口;The vacuum chamber includes a vacuum cover and a semi-enclosed heat sink fixed on the inner wall of the vacuum cover; the inner side of the heat sink constitutes a vacuum test space, and a line is left between the outer side and the inner wall of the vacuum cover. A cooling medium channel; the cooling medium channel is provided with a cooling medium inlet and a cooling medium outlet;
所述试样加热组件设置在真空室的真空测试空间内对试样进行加热,包括主加热器;所述主加热器与一标准电阻以及直流电源构成串联回路;The sample heating assembly is arranged in the vacuum test space of the vacuum chamber to heat the sample, including a main heater; the main heater forms a series circuit with a standard resistor and a DC power supply;
所述抽真空装置通过管道与该真空室的真空测试空间连通;The vacuum pumping device communicates with the vacuum test space of the vacuum chamber through a pipeline;
所述恒温冷却装置通分别过管道与冷却介质通道的冷却介质入口和冷却介质出口连通;The constant temperature cooling device communicates with the cooling medium inlet and the cooling medium outlet of the cooling medium passage through pipes respectively;
所述数据测量与处理装置采集试样温度、热沉温度、真空室内真空度以及主加热器的功率;当数据测量与处理装置检测到真空室内的压力达到1.0X10-3Pa以下,且试样温度达到所设定的温度时,该数据测量与处理装置根据试样温度、热沉温度、主加热器的功率以及试样的辐射表面积计算出试样的半球发射率。The data measurement and processing device collects the temperature of the sample, the temperature of the heat sink, the vacuum degree in the vacuum chamber and the power of the main heater; when the data measurement and processing device detects that the pressure in the vacuum chamber reaches below 1.0X10 -3 Pa, and the sample When the temperature reaches the set temperature, the data measuring and processing device calculates the hemispherical emissivity of the sample according to the sample temperature, the heat sink temperature, the power of the main heater and the radiation surface area of the sample.
相比于现有技术,本实用新型的一种稳态量热计法半球发射率测试仪包括真空室、恒温冷却装置、试样加热组件、抽真空装置以及数据测量与处理装置,通过稳态量热计法,克服了测试过程对材料导热系数与比热容的苛刻要求,测试精度较高,测试温区宽,应用较为广泛,可以测试材料在不同温度条件下尤其是在低温下的半球发射率。利用该测试装置的测试结果,可方便地计算出材料的半球发射率,测试与计算较简单。Compared with the prior art, a steady-state calorimeter method hemispherical emissivity tester of the present invention includes a vacuum chamber, a constant temperature cooling device, a sample heating assembly, a vacuum device, and a data measurement and processing device. The calorimeter method overcomes the strict requirements on the thermal conductivity and specific heat capacity of the material during the test process. It has high test accuracy, wide test temperature range, and is widely used. It can test the hemispherical emissivity of materials under different temperature conditions, especially at low temperatures. . Using the test results of the test device, the hemispherical emissivity of the material can be conveniently calculated, and the test and calculation are relatively simple.
进一步,所述数据测量与处理装置包括第一温测单元、第二温测单元、第三温测单元、第四温测单元、第一电压计、第二电压计以及处理单元;所述第一温测单元设置在试样上,测量试样温度;第二温测单元设置在热沉上;所述第三温测单元设置在冷却介质入口处;所述第四温测单元设置在冷却介质出口处;所述第一电压计与该主加热器并联,测量主加热器的电压;所述第二电压计并联在该标准电阻上,测量标准电阻的电压;所述处理单元根据第一电压计与第二电压计的数值以及标准电阻的阻值计算主加热器的功率。Further, the data measurement and processing device includes a first temperature measurement unit, a second temperature measurement unit, a third temperature measurement unit, a fourth temperature measurement unit, a first voltmeter, a second voltmeter, and a processing unit; A temperature measurement unit is set on the sample to measure the temperature of the sample; the second temperature measurement unit is set on the heat sink; the third temperature measurement unit is set at the inlet of the cooling medium; the fourth temperature measurement unit is set at the cooling medium outlet; the first voltmeter is connected in parallel with the main heater to measure the voltage of the main heater; the second voltmeter is connected in parallel with the standard resistance to measure the voltage of the standard resistance; the processing unit according to the first The values of the voltmeter and the second voltmeter and the resistance of the standard resistor are used to calculate the power of the main heater.
进一步,所述抽真空装置包括油扩散泵、储气罐以及机械泵;真空室、油扩散泵、储气罐以及机械泵依次通过管道连通;该真空室与该油扩散泵之间的管道上设有高真空阀。Further, the vacuum pumping device includes an oil diffusion pump, an air storage tank, and a mechanical pump; the vacuum chamber, the oil diffusion pump, the air storage tank, and the mechanical pump are connected through pipelines in sequence; on the pipeline between the vacuum chamber and the oil diffusion pump Equipped with high vacuum valve.
进一步,所述抽真空装置还包括一个三通阀;该三通阀包括一个主端口与两个选择端口;该主端口通过管道与该机械泵连通;其中一选择端口通过管道与该储气罐连通,另一个选择端口通过管道与该真空室直接连通;该数据测量与处理装置还包括高真空计、第一低真空计和第二低真空计;所述高真空计设置在高真空阀与油扩散泵之间的管道上;所述第一低真空计设置在三通阀与机械泵之间的管道上;所述第二低真空计设置在三通阀与真空室之间的管道上。高真空机构与低真空机构共用一个机械泵,并可通过三通阀切换,简化了管路连接,省去了成本。Further, the vacuum pumping device also includes a three-way valve; the three-way valve includes a main port and two selection ports; the main port communicates with the mechanical pump through a pipeline; one of the selection ports communicates with the gas storage tank through a pipeline The other selection port is directly communicated with the vacuum chamber through a pipeline; the data measurement and processing device also includes a high vacuum gauge, a first low vacuum gauge and a second low vacuum gauge; the high vacuum gauge is arranged between the high vacuum valve and the On the pipeline between the oil diffusion pump; the first low vacuum gauge is set on the pipeline between the three-way valve and the mechanical pump; the second low vacuum gauge is set on the pipeline between the three-way valve and the vacuum chamber . The high-vacuum mechanism and the low-vacuum mechanism share a mechanical pump, which can be switched through a three-way valve, which simplifies the pipeline connection and saves costs.
进一步,该试样加热组件包括主加热器和辅助加热器;该辅助加热器呈半包围状,该主加热器设置在该辅助加热器的半包围空间内。该辅助加热器用于对试样温度补偿。Further, the sample heating assembly includes a main heater and an auxiliary heater; the auxiliary heater is semi-enclosed, and the main heater is arranged in the semi-enclosed space of the auxiliary heater. The auxiliary heater is used for sample temperature compensation.
进一步,该试样加热组件还包括一均热板,该均热板设置在该主加热器上。使试样均匀加热。Further, the sample heating assembly also includes a soaking plate, and the soaking plate is arranged on the main heater. Heat the sample evenly.
进一步,还包括与真空罩固定连接的升降销轴,该升降销轴配有动力单元以及与该动力单元电连接的控制按钮,该动力单元驱动该升降销轴上下移动。通过控制按钮控制升降销轴上下移动,带动真空罩打开或闭合,提高劳动效率。Further, it also includes a lifting pin fixedly connected with the vacuum cover, the lifting pin is equipped with a power unit and a control button electrically connected with the power unit, and the power unit drives the lifting pin to move up and down. Control the lifting pin shaft to move up and down through the control button to drive the vacuum cover to open or close, improving labor efficiency.
进一步,所述恒温冷却装置为循环冷却水装置或液氮罐。Further, the constant temperature cooling device is a circulating cooling water device or a liquid nitrogen tank.
进一步,所述热沉的朝向真空测试空间的一面涂覆有无光黑漆。Further, the side of the heat sink facing the vacuum test space is coated with matt black paint.
进一步,所述测试仪还包括测试主机;该测试主机包括显示屏、真空压力表、温度显示仪以及控制面板;该真空压力表显示第一低真空计、第二低真空计以及高真空计所测得的数值;所述温度显示仪显示第一温测单元与第二温测单元的所测得的数值;所述控制面板上设有多个控制按钮。Further, the tester also includes a test host; the test host includes a display screen, a vacuum pressure gauge, a temperature display and a control panel; the vacuum pressure gauge displays the first low vacuum gauge, the second low vacuum gauge and the high vacuum gauge. The measured values; the temperature display device displays the measured values of the first temperature measuring unit and the second temperature measuring unit; the control panel is provided with a plurality of control buttons.
附图说明Description of drawings
图1是本实用新型的一种稳态量热计法半球发射率测试仪的装置连接图Fig. 1 is a device connection diagram of a steady-state calorimeter method hemispherical emissivity tester of the present utility model
图2是图1中真空1的的内部结构示意图Fig. 2 is a schematic diagram of the internal structure of the vacuum 1 in Fig. 1
图3是图2中的主加热器31与辅助加热器32的电路图Fig. 3 is a circuit diagram of the main heater 31 and the auxiliary heater 32 in Fig. 2
下面参见附图及具体实施例,对本实用新型作进一步说明。Referring to the accompanying drawings and specific embodiments below, the utility model will be further described.
具体实施方式Detailed ways
采用稳态卡计法测量材料半球发射率的原理如下:假设试样的半球发射率εH等于半球吸收率,当试样温度T达到热平衡时,有如下关系式:The principle of measuring the hemispherical emissivity of the material by the steady-state card meter method is as follows: Assume that the hemispherical emissivity ε H of the sample is equal to the hemispherical absorptivity, when the temperature T of the sample reaches thermal equilibrium, the following relationship is expressed:
式中σ为斯蒂芬-波尔兹曼常数;A为试样的表面积;T和T0分别为试样与测试室内壁的温度;Q为加热器的加热功率;Qw为试样通过引线的热损;Qg为测试室内由残余气体引起的热损;Qr为试样与测试室内壁多次反射试样吸收的能量。In the formula, σ is the Stephen-Boltzmann constant; A is the surface area of the sample; T and T 0 are the temperature of the sample and the inner wall of the test chamber; Q is the heating power of the heater; Heat loss; Q g is the heat loss caused by residual gas in the test chamber; Q r is the energy absorbed by the sample and the test chamber wall for multiple reflections.
在测试过程中,测试室内维持高真空,且测试室内表面积远大于试样表面积,因而,Qg与Qr可以忽略不计;由于采用的加热丝及引线直径都较细,故可忽略引线的热损Qw。即公式(1)等价为During the test, the test chamber maintains a high vacuum, and the surface area of the test chamber is much larger than the surface area of the sample, so Q g and Q r can be ignored; since the heating wire and the diameter of the lead wire are small, the heat of the lead wire can be ignored. Loss of Q w . That is, formula (1) is equivalent to
故通过测量加试热器的加热功率Q、样温度T与测试室内壁温度T0以及试样的表面积A,即可计算出试样的半球发射率εH。Therefore, the hemispherical emissivity ε H of the sample can be calculated by measuring the heating power Q of the test heater, the temperature T of the sample, the temperature T 0 of the inner wall of the test chamber, and the surface area A of the sample.
请参阅图1与图2,图1是本实用新型的一种稳态量热计法半球发射率测试仪的装置连接图,图2是图1中真空室1的内部结构示意图。本实用新型的一种稳态量热计法半球发射率测试仪,包括真空室1、恒温冷却装置2、试样加热组件3、抽真空装置4、数据测量与处理装置5以及测试主机。所述真空室1包括真空罩11、设置在真空罩底部的法兰12以及固设在真空罩11内壁上呈半包围状的热沉13;所述热沉13朝内的一面与法兰12构成真空测试空间,朝外的一面与真空罩11的内壁之间留有一条冷却介质通道14。所述恒温冷却装置2与该真空室1的冷却介质通道14通过管道连通,其产生冷却介质并与所述热沉热交换以恒定热沉的温度。该试样加热组件3设置在该真空室1内,需测试的试样放置在该试样加热组件3上,由该试样加热组件3对其加热。该抽真空装置4与该真空室1的真空测试空间连通,用于对真空室1抽真空。该数据测量与处理装置5用于测量测试仪运行的数据,当试样温度T达到预设定的温度且真空室1内处于热稳定状态,计算出试样的半球发射率εH。Please refer to Fig. 1 and Fig. 2, Fig. 1 is a device connection diagram of a steady-state calorimeter hemispherical emissivity tester of the present invention, and Fig. 2 is a schematic diagram of the internal structure of the vacuum chamber 1 in Fig. 1 . The utility model relates to a hemispherical emissivity tester with a steady-state calorimeter method, comprising a vacuum chamber 1, a constant temperature cooling device 2, a sample heating component 3, a vacuuming device 4, a data measurement and processing device 5 and a test host. The vacuum chamber 1 includes a vacuum cover 11, a flange 12 arranged at the bottom of the vacuum cover, and a heat sink 13 fixed on the inner wall of the vacuum cover 11 in a semi-enclosed shape; A vacuum test space is formed, and a cooling medium channel 14 is left between the outward facing side and the inner wall of the vacuum cover 11 . The constant temperature cooling device 2 communicates with the cooling medium passage 14 of the vacuum chamber 1 through a pipeline, which generates cooling medium and exchanges heat with the heat sink to keep the temperature of the heat sink constant. The sample heating assembly 3 is arranged in the vacuum chamber 1 , the sample to be tested is placed on the sample heating assembly 3 and is heated by the sample heating assembly 3 . The vacuuming device 4 communicates with the vacuum testing space of the vacuum chamber 1 for evacuating the vacuum chamber 1 . The data measuring and processing device 5 is used to measure the running data of the tester, and calculate the hemispherical emissivity ε H of the sample when the sample temperature T reaches a preset temperature and the vacuum chamber 1 is in a thermally stable state.
该真空罩11的外壁上固定有一升降销轴15,该升降销轴15与一动力单元连接,该动力单元分别与上升按钮以及下降按钮电连接;操作员通过控制上升按钮或下降按钮对升降销轴15进行操控,从而控制真空罩11的上下移动,提高劳动效率;该动力单元优选为电机。该热沉13朝内的一面涂覆有无光黑漆。该冷却介质通道14内设有冷却介质入口16与冷却介质出口17。该冷却介质入口16与该冷却介质出口17分别与该恒温冷却装置2通过管道连通;冷却介质从该恒温冷却装置2产生后,通过冷却介质入口16进入冷却介质通道14,与热沉13热交换以维持热沉13的温度,并通过冷却介质出口17回流到恒温冷却装置2重新制冷。A lifting pin 15 is fixed on the outer wall of the vacuum cover 11, and the lifting pin 15 is connected with a power unit, and the power unit is electrically connected with the up button and the down button respectively; The shaft 15 is manipulated to control the up and down movement of the vacuum cover 11 and improve labor efficiency; the power unit is preferably a motor. The inwardly facing side of the heat sink 13 is painted with matt black paint. The cooling medium passage 14 is provided with a cooling medium inlet 16 and a cooling medium outlet 17 . The cooling medium inlet 16 and the cooling medium outlet 17 are respectively communicated with the constant temperature cooling device 2 through pipelines; after the cooling medium is generated from the constant temperature cooling device 2, it enters the cooling medium channel 14 through the cooling medium inlet 16, and exchanges heat with the heat sink 13 To maintain the temperature of the heat sink 13, and return to the constant temperature cooling device 2 through the cooling medium outlet 17 for re-refrigeration.
该恒温冷却装置2为循环冷却水装置或液氮罐。The constant temperature cooling device 2 is a circulating cooling water device or a liquid nitrogen tank.
该试样加热组件3包括主加热器31、辅助加热器32以及均热板33。该主加热器31用于将试样A加热至预定温度。如图3所示,其是图2中的主加热器31与辅助加热器32的电路图。该主加热器31与一标准电阻以及直流电源串联构成主加热回路。该均热板33放置在该主加热器31上。试样A放置在该均热板33上,使试样A均匀受热。该辅助加热器32呈半包围状,试样A、均热板33以及主加热器31放置在该辅助加热器32内,且通过一盖板34将试样A与辅助加热器32之间的缝隙封盖住,使主加热器31所产生的热全部提供给试样A。该辅助加热器32内置有线圈,通过接交流电来使线圈发热。辅助加热器32作为补偿加热,使主加热器31产生的热量全部供给试样A,并使试样温度恒定。The sample heating assembly 3 includes a main heater 31 , an auxiliary heater 32 and a vapor chamber 33 . The main heater 31 is used to heat the sample A to a predetermined temperature. As shown in FIG. 3 , it is a circuit diagram of the main heater 31 and the auxiliary heater 32 in FIG. 2 . The main heater 31 is connected in series with a standard resistor and a DC power supply to form a main heating circuit. The vapor chamber 33 is placed on the main heater 31 . The sample A is placed on the vapor chamber 33 so that the sample A is evenly heated. The auxiliary heater 32 is in a semi-enclosed shape, and the sample A, vapor chamber 33 and main heater 31 are placed in the auxiliary heater 32, and the space between the sample A and the auxiliary heater 32 is sealed by a cover plate 34. The gap was closed so that all the heat generated by the main heater 31 was supplied to the sample A. The auxiliary heater 32 has a built-in coil, and the coil is heated by receiving an alternating current. The auxiliary heater 32 supplies all the heat generated by the main heater 31 to the sample A as compensation heating, and keeps the temperature of the sample constant.
该抽真空装置4包括三通阀41、挡油器42、油扩散泵43与储气罐44以及机械泵45;所述三通阀41包括一个主端口、第一选择端口与第二选择端口。该主端口通过管道与该机械泵45连通,且该管道上设有一电磁阀46;该电磁阀46与该机械泵45联动,机械泵45打开时,电磁阀46打开,从而机械泵45与三通阀41之间通断。第一选择端口通过管道与真空室1连通。真空室1、挡油器42、油扩散泵43、储气罐44以及第二选择端口依次通过管道连通;该油扩散泵43与该真空室1之间的管道上设有高真空阀47。该三通阀41上设有一手柄,手柄可外拉至死点位置,或往里推至死点位置。当该三通阀41处于往里推至死点位置时,第二选择端口与该主端口连通;当该三通阀41处于向外拉至死点位置时,第一选择端口与主端口连通。该三通阀41的功能相当于一个选择器,选择机械泵45工作的管路。The vacuum device 4 includes a three-way valve 41, an oil retainer 42, an oil diffusion pump 43, an air tank 44, and a mechanical pump 45; the three-way valve 41 includes a main port, a first selection port and a second selection port . The main port communicates with the mechanical pump 45 through a pipeline, and the pipeline is provided with a solenoid valve 46; The through valve 41 is on-off. The first selection port communicates with the vacuum chamber 1 through a pipe. The vacuum chamber 1 , the oil retainer 42 , the oil diffusion pump 43 , the gas storage tank 44 and the second selection port are connected through pipelines in sequence; a high vacuum valve 47 is arranged on the pipeline between the oil diffusion pump 43 and the vacuum chamber 1 . This three-way valve 41 is provided with a handle, and the handle can be pulled out to the dead point position, or pushed inward to the dead point position. When the three-way valve 41 is in the position of pushing in to the dead point, the second selection port communicates with the main port; when the three-way valve 41 is in the position of pulling out to the dead point, the first selection port communicates with the main port . The function of the three-way valve 41 is equivalent to a selector, which selects the pipeline in which the mechanical pump 45 works.
所述数据测量与处理装置5包括第一温测单元、第二温测单元、第三温测单元、第四温测单元、第一电压计、第二电压计、高真空计51、第一低真空计52、第二低真空计53以及处理单元。所述第一温测单元设置在试样上,测量试样温度T。所述第二温测单元设置在热沉上,测量热沉温度T0。所述第三温测单元设置在冷却介质入口16处。所述第四温测单元设置在冷却介质出口17处。所述第一电压计与该主加热器31并联,测量主加热器31的端电压V。所述第二电压计并联在该标准电阻上,测量标准电阻的电压V1。所述高真空计51设置在高真空阀47与挡油器42之间。所述第一低真空计52设置在三通阀41与电磁阀46之间。所述第二低真空计53设置在三通阀41与真空室1之间。所述处理单元根据第一电压计与第二电压计的数值以及标准电阻的阻值R计算主加热器的功率Q。并且,若采用循环冷却水作为恒温装置时,热沉温度T0为第三、第四温测单元所检测值的平均值,即冷却介质入口16与冷却介质出口17的平均温度值;若采用液氮作为恒温装置,热沉温度T0为第二单元所检测的温度值。The data measurement and processing device 5 includes a first temperature measurement unit, a second temperature measurement unit, a third temperature measurement unit, a fourth temperature measurement unit, a first voltmeter, a second voltmeter, a high vacuum gauge 51, a first Rough gauge 52, second rough gauge 53 and processing unit. The first temperature measurement unit is arranged on the sample to measure the temperature T of the sample. The second temperature measuring unit is arranged on the heat sink to measure the temperature T 0 of the heat sink. The third temperature measuring unit is arranged at the cooling medium inlet 16 . The fourth temperature measuring unit is arranged at the cooling medium outlet 17 . The first voltmeter is connected in parallel with the main heater 31 to measure the terminal voltage V of the main heater 31 . The second voltmeter is connected in parallel with the standard resistance to measure the voltage V1 of the standard resistance. The high vacuum gauge 51 is arranged between the high vacuum valve 47 and the oil deflector 42 . The first rough vacuum gauge 52 is disposed between the three-way valve 41 and the solenoid valve 46 . The second rough vacuum gauge 53 is arranged between the three-way valve 41 and the vacuum chamber 1 . The processing unit calculates the power Q of the main heater according to the values of the first voltmeter and the second voltmeter and the resistance value R of the standard resistor. And, when using circulating cooling water as the constant temperature device, the heat sink temperature T0 is the average value of the values detected by the third and fourth temperature measuring units, that is, the average temperature value of the cooling medium inlet 16 and the cooling medium outlet 17; Liquid nitrogen is used as a constant temperature device, and the heat sink temperature T 0 is the temperature value detected by the second unit.
当试样温度T达到预设定的温度且真空室1内处于热稳定状态,所述数据测量与处理装置5根据试样温度T、热沉温度T0、主加热器的功率Q以及试样的辐射表面积S计算出试样的半球发射率εH。其中,
所述测试主机包括显示屏、真空压力表、温度显示仪以及控制面板;该真空压力表显示第一低真空计52、第二低真空计53以及高真空计51所测得的数值。所述温度显示仪显示第一温测单元、第二温测单元、第三温测单元以及第四温测单元的所测得的数值。所述控制面板上设有测试主机电源按钮、显示屏电源按钮、温度显示仪电源按钮、机械泵开关按钮、恒温冷却装置开关按钮、冷却水开关按钮、真空罩上升按钮、真空罩下降按钮、主加热器开关按钮以及辅助加热器开关按钮。The test host includes a display screen, a vacuum pressure gauge, a temperature indicator and a control panel; the vacuum pressure gauge displays the values measured by the first low vacuum gauge 52 , the second low vacuum gauge 53 and the high vacuum gauge 51 . The temperature display device displays the measured values of the first temperature measuring unit, the second temperature measuring unit, the third temperature measuring unit and the fourth temperature measuring unit. The control panel is provided with a test host power button, a display power button, a temperature indicator power button, a mechanical pump switch button, a constant temperature cooling device switch button, a cooling water switch button, a vacuum cover up button, a vacuum cover down button, and a main Heater switch button and auxiliary heater switch button.
进一步,该真空室1还另外通过管道与充气泵连通,真空室1与充气泵之间设有充气阀。Further, the vacuum chamber 1 is additionally communicated with the air pump through a pipeline, and an inflation valve is arranged between the vacuum chamber 1 and the air pump.
本实用新型的一种稳态量热计法半球发射率测试仪的测量原理:将一个被测试样放置在真空室1内,试样表面和真空室1之间只有辐射热交换,试样发出的热辐射全部投射到真空室1热沉表面上。对试样用电加热方式提供一个连续的加热功率,使试样加热到测定温度,试样通过热辐射与所处的冷却黑体空腔进行热交换。当试样与环境之间达到热平衡,通过数据测量与处理装置5采集加热器温度T、热沉温度T0、主加热器的端电压V和标准电阻的端电压V1的数据,再根据试样的表面积S,由计算机软件直接计算出试样的半球发射率εH。The measurement principle of a steady-state calorimeter method hemispherical emissivity tester of the utility model: a test sample is placed in the vacuum chamber 1, there is only radiation heat exchange between the sample surface and the vacuum chamber 1, and the sample emits All of the heat radiation is projected onto the heat sink surface of the vacuum chamber 1. The electric heating method is used to provide a continuous heating power to the sample, so that the sample is heated to the measurement temperature, and the sample conducts heat exchange with the cooling blackbody cavity in which it is located through thermal radiation. When the thermal balance between the sample and the environment is reached, the data of the heater temperature T, the heat sink temperature T 0 , the terminal voltage V of the main heater and the terminal voltage V1 of the standard resistor are collected by the data measuring and processing device 5, and then according to the sample The surface area S of the sample is directly calculated by the computer software to calculate the hemispherical emissivity ε H of the sample.
本实用新型的一种稳态量热计法半球发射率测试仪的具体操作流程如下:The concrete operating procedure of a kind of steady-state calorimeter method hemispherical emissivity tester of the present utility model is as follows:
按真空罩上升按钮,通过上升销轴将真空罩11升至合适的高度,将制备好的被测试样用导热硅脂固定在真空室1的均热板33上,并用压板34压好,然后按真空罩下降按钮,将真空罩11降至最低处,使真空罩11与底法兰的密封圈负压压紧。先对真空室1进行预抽低真空:将三通阀41往外拉至死点位置,并保持高真空阀47的关闭状态。在控制面板上打开如下按钮:测试主机电源按钮、显示屏电源按钮、温度显示仪电源按钮、机械泵开关按钮。当真空室1的压力小于或等于10Pa时,对挡油器42、油扩散泵43进行抽真空:将三通阀41的手柄往里推至死点位置,并保持高真空阀47处于关闭状态,当油扩散泵43的压力达到约6Pa以下时,打开冷却水开关按钮以接通油扩散泵43的冷却水,对油扩散泵43加热,并开启恒温水或液氮,若是使用液氮,则直接旋开液氮瓶的减压阀,使其压力控制在0.05-0.1MPa。对油扩散泵43加热40min后,把三通阀41往外拉至死点位置,再次对真空室1抽低真空至10Pa以下时:将三通阀41往里推至死点位置,把高真空阀47打开,在控制面板上按下如下按钮:主加热器开关按钮、辅助加热器开关按钮,对试样开始加热升温。试样温度T达到预设定的温度且真空室1内处于热稳定状态(在20min内,试样温度波动不大于0.1℃)时,连续3次测量试样温度T、热沉温度T0、主加热器31的端电压V和标准电阻的端电压V1;其中,热沉温度T0为当试样温度T达到检测的温度时冷却介质入口15和冷却介质出口16的温度的平均值。通过数据测量与处理装置5进行数据采集,再根据试样的表面积S,由计算机软件直接计算出试样的半球发射率εH。Press the vacuum cover up button, raise the vacuum cover 11 to a suitable height through the lifting pin, fix the prepared test sample on the soaking plate 33 of the vacuum chamber 1 with thermal conductive silicone grease, and press it with the pressure plate 34, and then Press the down button of the vacuum cover to lower the vacuum cover 11 to the lowest point, so that the vacuum cover 11 and the sealing ring of the bottom flange are compressed under negative pressure. Pre-pump the vacuum chamber 1 to low vacuum: pull the three-way valve 41 outward to the dead point, and keep the high vacuum valve 47 closed. Open the following buttons on the control panel: test host power button, display power button, temperature display instrument power button, mechanical pump switch button. When the pressure of the vacuum chamber 1 is less than or equal to 10Pa, vacuumize the oil retainer 42 and the oil diffusion pump 43: push the handle of the three-way valve 41 to the dead point, and keep the high vacuum valve 47 in a closed state , when the pressure of the oil diffusion pump 43 reaches below about 6Pa, turn on the cooling water switch button to connect the cooling water of the oil diffusion pump 43, heat the oil diffusion pump 43, and turn on the constant temperature water or liquid nitrogen. If liquid nitrogen is used, Then unscrew the pressure reducing valve of the liquid nitrogen bottle directly to control the pressure at 0.05-0.1MPa. After heating the oil diffusion pump 43 for 40 minutes, pull the three-way valve 41 outward to the dead point position, and then evacuate the vacuum chamber 1 below 10 Pa: push the three-way valve 41 inward to the dead point position, and turn the high vacuum Valve 47 is opened, and the following buttons are pressed on the control panel: the main heater switch button and the auxiliary heater switch button, and the sample starts to be heated and heated. When the sample temperature T reaches the preset temperature and the vacuum chamber 1 is in a thermally stable state (within 20 minutes, the sample temperature fluctuation is not greater than 0.1°C), measure the sample temperature T, heat sink temperature T 0 , The terminal voltage V of the main heater 31 and the terminal voltage V1 of the standard resistor; wherein, the heat sink temperature T 0 is the average value of the temperatures of the cooling medium inlet 15 and the cooling medium outlet 16 when the sample temperature T reaches the detected temperature. The data is collected by the data measuring and processing device 5, and then according to the surface area S of the sample, the hemispherical emissivity ε H of the sample is directly calculated by computer software.
测试完毕后,关闭真空测量的电源,停止油扩散泵43加热,关闭高真空阀。打开充气阀,使真空罩11内充气。将真空罩11上升,取出试样后,使真空罩11下降,封闭好后,关充气阀,将三通阀41拉出至死点,对真空罩11抽低真空3-5min。当油扩散泵43冷却至室温后,再停机械泵45,保证油扩散泵43本机保持真空。关闭油扩散泵43的冷却水及电源,全部工作结束。After the test is completed, turn off the power supply for vacuum measurement, stop the oil diffusion pump 43 for heating, and close the high vacuum valve. Open the inflation valve to inflate the vacuum cover 11. Raise the vacuum cover 11, take out the sample, lower the vacuum cover 11, close the inflation valve, pull out the three-way valve 41 to the dead point, and vacuum the vacuum cover 11 for 3-5 minutes. After the oil diffusion pump 43 is cooled to room temperature, stop the mechanical pump 45 again to ensure that the oil diffusion pump 43 keeps the vacuum. Turn off the cooling water and the power supply of the oil diffusion pump 43, and all work ends.
在测试过程中,密封好真空容器后,必须先抽低真空,待真空抽低至6Pa后再开高真空阀,决不允许直接抽高真空,以免工作着的扩散泵油接触大气而使油氧化,破坏了扩散泵的性能。真空操作结束时必须首先切断真空测量,再关高真空阀,然后再打开充气阀,高真空测量未切断而充气,则电离管灯丝立即烧毁,高真空阀未关闭而充气,则扩散泵油即氧化,扩散泵就不能正常工作。工作过程中经常注意冷却水是否畅通,水温、流量是否正常。若遇突然停电,则立即切断真空测量并关高真空阀,将三通阀41往外拉至死点(冷却水不能断),来电后,待机械泵45工作2—3分钟后再将三通阀41往里推至死点,继续转入正常工作,若电源在30分钟内不能修复,应将扩散泵去热,尽可能地快速冷却。In the test process, after the vacuum container is sealed, the vacuum must be drawn down first, and the high vacuum valve should be opened after the vacuum has been drawn down to 6Pa. Oxidation, which destroys the performance of the diffusion pump. At the end of the vacuum operation, you must first cut off the vacuum measurement, then close the high vacuum valve, and then open the inflation valve. If the high vacuum measurement is not cut off and the gas is filled, the filament of the ionization tube will be burned immediately. If the high vacuum valve is not closed and the gas is filled, the diffusion pump oil will Oxidation, the diffusion pump will not work properly. During the working process, always pay attention to whether the cooling water is unblocked, whether the water temperature and flow are normal. In case of a sudden power failure, immediately cut off the vacuum measurement and close the high vacuum valve, pull the three-way valve 41 to the dead point (the cooling water cannot be cut off), after the power is turned on, wait for the mechanical pump 45 to work for 2-3 minutes before closing the three-way valve. Valve 41 is pushed inward to the dead point, and continues to turn into normal work, if the power supply cannot be repaired within 30 minutes, the diffusion pump should be deheated and cooled as fast as possible.
相比于现有技术,本实用新型的一种稳态量热计法半球发射率测试仪包括真空室1、恒温冷却装置2、试样加热组件3、抽真空装置4以及数据测量与处理装置5,通过稳态量热计法,克服了测试过程对材料导热系数与比热容的苛刻要求,测试精度较高,测试温区宽,应用较为广泛,可以测试材料在不同温度条件下尤其是在低温下的半球发射率。利用该测试装置的测试结果,可方便地计算出材料的半球发射率,测试与计算较简单。Compared with the prior art, a steady-state calorimeter hemispherical emissivity tester of the present invention includes a vacuum chamber 1, a constant temperature cooling device 2, a sample heating component 3, a vacuuming device 4, and a data measurement and processing device 5. Through the steady-state calorimeter method, it overcomes the strict requirements on the thermal conductivity and specific heat capacity of materials during the test process. The test accuracy is high, the test temperature range is wide, and the application is relatively wide. It can test materials under different temperature conditions, especially at low temperatures. Lower hemispheric emissivity. Using the test results of the test device, the hemispherical emissivity of the material can be conveniently calculated, and the test and calculation are relatively simple.
以上仅是本实用新型的优选实施方式,应当指出的是,上述优选实施方式不应视为对本实用新型的限制,本实用新型的保护范围应当以权利要求所限定的范围为准。对于本技术领域的普通技术人员来说,在不脱离本实用新型的精神和范围内,还可以做出若干改进和润饰,这些改进和润饰也应视为本实用新型的保护范围。The above are only preferred implementations of the present utility model. It should be pointed out that the above-mentioned preferred implementations should not be regarded as limitations on the present utility model, and the protection scope of the present utility model should be based on the scope defined by the claims. For those skilled in the art, without departing from the spirit and scope of the utility model, some improvements and modifications can also be made, and these improvements and modifications should also be regarded as the protection scope of the utility model.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103969291A (en) * | 2014-04-17 | 2014-08-06 | 广州特种承压设备检测研究院 | Test instrument for hemispherical emissivity adopting homeostasis calorimeter method |
CN115993379A (en) * | 2023-02-17 | 2023-04-21 | 北京中科科仪股份有限公司 | Coating heat dissipation testing device and testing method |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103969291A (en) * | 2014-04-17 | 2014-08-06 | 广州特种承压设备检测研究院 | Test instrument for hemispherical emissivity adopting homeostasis calorimeter method |
CN103969291B (en) * | 2014-04-17 | 2016-09-07 | 广州特种承压设备检测研究院 | A kind of stable state calorimeter method hemispherical emissivity tester |
CN115993379A (en) * | 2023-02-17 | 2023-04-21 | 北京中科科仪股份有限公司 | Coating heat dissipation testing device and testing method |
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