CN203894090U - Jade nondestructive testing sample model - Google Patents
Jade nondestructive testing sample model Download PDFInfo
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- CN203894090U CN203894090U CN201420280815.5U CN201420280815U CN203894090U CN 203894090 U CN203894090 U CN 203894090U CN 201420280815 U CN201420280815 U CN 201420280815U CN 203894090 U CN203894090 U CN 203894090U
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- 239000010977 jade Substances 0.000 title claims abstract description 119
- 238000009659 non-destructive testing Methods 0.000 title claims abstract description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 239000011159 matrix material Substances 0.000 claims description 31
- 239000000203 mixture Substances 0.000 claims description 19
- 238000005516 engineering process Methods 0.000 abstract description 21
- 238000001514 detection method Methods 0.000 abstract description 20
- 238000011160 research Methods 0.000 abstract description 13
- 238000005520 cutting process Methods 0.000 abstract description 6
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 abstract description 2
- 239000010931 gold Substances 0.000 abstract description 2
- 229910052737 gold Inorganic materials 0.000 abstract description 2
- 238000009792 diffusion process Methods 0.000 abstract 1
- 230000001795 light effect Effects 0.000 abstract 1
- 239000000523 sample Substances 0.000 description 78
- 238000012360 testing method Methods 0.000 description 26
- 239000013078 crystal Substances 0.000 description 21
- 238000000034 method Methods 0.000 description 20
- 238000011161 development Methods 0.000 description 14
- 230000008569 process Effects 0.000 description 12
- 239000011435 rock Substances 0.000 description 12
- 239000000843 powder Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 9
- 238000004458 analytical method Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 8
- 238000005070 sampling Methods 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 230000000694 effects Effects 0.000 description 7
- 229910052500 inorganic mineral Inorganic materials 0.000 description 7
- 239000011707 mineral Substances 0.000 description 7
- 238000003776 cleavage reaction Methods 0.000 description 6
- 239000010437 gem Substances 0.000 description 6
- 230000003287 optical effect Effects 0.000 description 6
- 230000007017 scission Effects 0.000 description 6
- 238000001069 Raman spectroscopy Methods 0.000 description 5
- 241000304460 Sinocrassula yunnanensis Species 0.000 description 5
- 230000005540 biological transmission Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 5
- 208000007578 phototoxic dermatitis Diseases 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 238000004026 adhesive bonding Methods 0.000 description 4
- 230000013011 mating Effects 0.000 description 4
- 238000000862 absorption spectrum Methods 0.000 description 3
- 230000001066 destructive effect Effects 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 239000004593 Epoxy Substances 0.000 description 2
- 238000005481 NMR spectroscopy Methods 0.000 description 2
- 208000034189 Sclerosis Diseases 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000000295 complement effect Effects 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 229910001751 gemstone Inorganic materials 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 230000005477 standard model Effects 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 230000000007 visual effect Effects 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010835 comparative analysis Methods 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000001739 density measurement Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 238000001493 electron microscopy Methods 0.000 description 1
- 239000005338 frosted glass Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 125000001475 halogen functional group Chemical group 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000010978 jasper Substances 0.000 description 1
- 238000003475 lamination Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000005298 paramagnetic effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000011049 pearl Substances 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 238000012428 routine sampling Methods 0.000 description 1
- 238000005464 sample preparation method Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 229910052594 sapphire Inorganic materials 0.000 description 1
- 239000010980 sapphire Substances 0.000 description 1
- 238000004621 scanning probe microscopy Methods 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000010421 standard material Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/84—Systems specially adapted for particular applications
- G01N21/87—Investigating jewels
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3563—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/65—Raman scattering
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
The utility model discloses a jade nondestructive testing sample model which comprises a jade model plate, wherein a smooth plane area, a hopper-shaped thinning area, a concave thinning area, a concave gold film area, a concave carbon film area, a barrel-shaped thinning area, a transparency changing area, a light diffusion prism area, a raw material remaining area, a cutting and grinding remaining area, a color vector area, a special light effect area and a mark area are arranged on the jade model plate. According to the jade nondestructive testing sample model, a novel product and a novel technology are specially designed for jade identification and teaching researches, and the demands of rapid nondestructive scientific and technological identification teaching and researches researched and developed at the present stage of the unique jade theory in China are satisfied, as a result, the blank that all specified 15 items of national standard data and conclusions cannot be rapidly obtained on the premises of no cutting of the sample and no changing of the shape of the detected sample in the field of the teaching and researches of jade detection and identification at home and abroad is compensated.
Description
Technical field
The utility model belongs to jade detection technique field, is specifically related to a kind of jade Non-Destructive Testing instance model.
Background technology
(1) the current domestic jade sample that is not specifically designed to Non-Destructive Testing.
China is the country with unique jade culture few in number in the world, China's national standard has reached a variety of at the natural jade of row, because jade is worth expensive, in the process integrating with in social demand, harmless science and technology identifies that detection technique has more and more important meaning in practice, but so far,, China does not have to meet present stage development in science and technology to be detected and the jade Dynamic Non-Destruction Measurement system of applying, and also there is no to support the jade sample of this technological system.
(2) international and domestic industry development is needed badly for professional Nondestructive Identification material sample.
1, surging along with jade collecting craze, the development of scientific research and authenticate technology, sample size to be analyzed increases considerably.Jade fast detecting becomes objective requirement, and detection needs sample Quick Acquisition and basic appraising datum, and the standard substance sample of applicable fast restore country examination criteria data.
2, optical microscope is as the strong instrument of a kind of exploration microworld, be widely used in every scientific experiment, along with the calculate fast development for the treatment of technology and digital processing technology of computing machine, various spectrum and ray detection and analytical technology have progressively realized the automatic acquisition of online control, micro-image and have preserved and computer aided detection, and non-damaging detects the inexorable trend that becomes of robotization and intelligent development.
3, in today of computer and palm intelligent equipment universalness, on the small-size laboratory that founds a family, personalized sole, the imagination in laboratory, technically moves to maturity, and utilizes high-tech wide at popularization Identification of Jades technical prospect among the people.
4, for concept and the classification of jade, judge not directly perceived at present, indefinite, classification is differentiated and is difficult to unification, inspection body, dealer and consumer are widely different to the understanding and grasping of Khotan jade criteria for classification, cause the phenomenon of passing a fake product off as a genuine one, adulterate general, Identification of Jades often causes quality dispute, has also restricted the development of jade industry.Along with Chinese jade culture stretches out, around the international jade industry in Consumption of China market, form, be badly in need of material standard compound matter and standardization identification systems, and international joint.
(3) non-infringement detection technique can complete the index test that all GBs of jade require.
1, jewel is identified to entering instrumental analysis is main digitizing, standardization track abroad.Continuous progress along with science and technology, the development that material microstructure is learned and electron microscopy development are fast, scanning electron microscope, scanning probe microscopy, electron probe are micro-, infrared spectrometer, ultraviolet spectrometer (UVS), Raman spectrometer, electron paramagnetic nuclear magnetic resonance, the a large amount of non-damaging detecting instruments of technology that transmission electron microscope ray etc. is new are applied in the middle of jewels and jade evaluation, the Nondestructive Identification technology of growing up on this basis reaches its maturity, and constantly obtains new achievement.
2, comprehensively adopt current scientific analysis instrument, according to current technical merit, jade sample to be checked can damaging proterties and the form of the lossy samples such as granulation, powder crystal, powder, solution after sampling, jade sample retains under the constant prerequisite of original its naturally solid-state form basic, as long as being processed into, its form is applicable to corresponding various non-infringement detecting instrument needs, 15 individual events that just can obtain GB requirement detect data and content, complete the index test that all GBs of jade require.
3, current, although the most imports of above advanced instrument that China is being used, some core technologies form barrier, so price is high, domestic many laboratories are difficult to be equipped with, but along with some technology are captured, the quickening of production domesticization step detects in China in recent years, cost declines, and non-infringement jade, precious stones, pearls and jewelery detects and started to popularize.
(4) problem of existing similar sample and technology.
1, multiple proterties sample lack of standardization: do not detect sample because current China has the Khotan jade of State-level or the standard substance of other jades, existing evaluation detects word standard cannot be corresponding with material standard, can only detect sample comparative analysis according to raw material, jade product and jade speciality.
(1) former stone: form is irregular, observation and research cannot become more meticulous.
(2) jadeware: cannot meet the delineation of measuring hardness, and the measurement of special light efficiency etc., inlay individually with hollow out jadeware cannot density measurement etc. index.
(3) powder: changed solid-state form originally.
(4) powder crystal: there is no smooth enough plane, measure refractive index, volume, density etc. too little.
(5) solution: can only supply composition Study.
(6) mating plate: the most just ores of existing observation mating plate are learned the common jade sheet of ore in field.
On June 1st, 2010, Xinjiang Administration of Quality and Technology Supervision of autonomous region issued one recommendatory but not be not with enforceable Khotan jade provincial standard, comprise < < Khotan jade material standard sample > >, the Khotan jade standard that is through with only has text description there is no the history of sample reference, domestic Khotan jade is identified and stepped forward major step, but this sample preparation method is simple, it is a bevelled wedge shape cube of tool, with this provincial standard sample, detect, must on detection sample piece, again sample sample preparation or processing again.
On Dec 17th, 2013 and in January, 2014, national standard GSB 16-3061-2013 < < Khotan jade material standard sample > > has been issued in CNS management committee and the approval of national standard model technical committee, this Khotan jade national standard sample in kind, with color classification, is divided into white jade, grey-white jade, sapphire, jasper, sugared jade and the large class of black jade six by Khotan jade.Think in the industry, this will play an important role for standard and guiding China jade industry, but, this specification is assembly long 3 centimetres, wide 2 centimetres, the rectangular parallelepiped jadeware sample of thick 1 centimetre, every class Khotan jade national standard in kind only represents the lowest limit of this jade kind color, there is no other special moulding implication and functions.It is only the standard substance that belongs in general sense " part for national standard ", according to the requirement of national standard material, Khotan jade national standard in kind should form correspondence with the word national standard having had, all the elements of utilizing this jade standard model can holographic acquisition national standard to enumerate, but also must on sample piece, again sample sample preparation or destructive processing again detecting.
(7) thin slice: at present China is not specifically designed to the jade thin slice of optical detection object, for a long time, can only be based upon geology and petrologic petrological Minerals And Rocks identifies that generally adopt petrographic thin section for optical detection object.Traditional key rock thin slice is based upon on mineralogy basis, utilizes light transmission and the reflective of rock forming mineral crystal, and the crystalline form of rock forming mineral, cleavage, every optical property are observed to evaluation, and then reaches the object to the evaluation of mineral.Under the instruments such as polarizing microscope, observe, first enough " thin ", is thinned to light and can penetrates sample, and general standard sheet thickness is 30 μ m, is equivalent to 0.003 centimeter.Manufacture difficulty is large, has again significant limitation in use procedure.
2, in general, at least need 6 procedures:
(1) cutting: the rock sample that field is gathered, first choose fresh not weathering part, then be cut into by diamond saw the suitable size that meets slide.
(2) polish: the rock sample sample cutting with want deadlocked slide, the silicon carbide powder with #600～#1000 grinds respectively, makes rock sample tangent plane become smooth plane.Check that whether smooth tangent plane is smooth, can, by rock sample towards light source, observe its reflection and whether well judge.
(3) gluing: the rock sample of finishing dealing with is adhered on frosted glass with epoxy (Epoxy), notes needing surface of contact before gluing clean with alcohol, and can not have Bubble formation between rock sample and glass when gluing, in order to avoid adhesion strength during impact section.It is upper that gluing is placed on stationary platform (Bonding jig), and with 50 ℃ of low-temperature bakes approximately 6～8 hours, so that fixed, sclerosis.
(4) section: sample is placed in to the thickness that cuts and wear into 100～150 μ m on thin slice cutting machine (Petro-thin) after glue sclerosis, because cutting machine rotating speed is too fast, so cannot cut into too thin sample.
(5) grind: with mircrometer gauge, make sample thickness, then utilize vacuum principle to be fixed on vacuum cup the thick rock sample sample of 100～150 μ m, then directly on thin slice abrasive disk (Lapping plate), be ground to standard thickness 30 μ m.
(6) Throwing light: if sample will be done micro-spy constituent analysis, need thin slice to carry out Throwing light with the aluminium powder Throwing light liquid of 0.3～0.05 μ m respectively.
Due to rock tool rigidity, thus above-mentioned manufacturing process be by sample be first fixed on slide, cut again thin, this and biologic slice first cut thin after, then the program being fixed on slide is just contrary.In to the research of jade and testing process, this thin slice of making of jade can be preferably for observing crystal structure.Thin slice is too thin, has limitation such as hardness in application, and refractive index, density etc. cannot be measured, and makes except relying on accurate instrument, also needs by dexterous both hands, and manufacture difficulty is large, and cost is high, and loss is large.Seldom, the scattered specialized laboratory that is distributed in, and can only using in laboratory, is difficult to promote socially domestic quantity.
3, qualification process is complicated:
According to traditional detection method, generally, the individual event that obtains 15 aspects of jade detects data and content, to utilize the detecting instrument of multiple difference in functionality respectively, and need be according to the different user demands of different instruments, repeatedly monoblock sampling or micro-damage sampling, then make above powder, powder crystal, particle, thin slice, mating plate, and the sample that is configured to the multiple difformities such as solution and form, can meet instrument and use.Modern jewels and jade identify learn based on modern mineralogy " the material performance of any mineral (and the macro property that comprises the physics categories such as mechanical property, optical property; and the micro-property etc. that comprises the multidisciplinary categories such as chemical property, biology performance); be all decided by the micromechanism that it is inner " theoretical foundation, what in mineralogy, extensively adopt at present is that to take mineralogical composition, crystal structure be foundation, has reflected to a certain extent the crystal chemistry classification schemes of native element in conjunction with rule.For the evaluation program of jewels and jade, be the detecting instrument that utilizes difference in functionality, by macrofeature, hold and to microscopic feature, hold that the direction of the transition that progressively becomes more meticulous carries out when identifying mineral.China's GB/T-16553-2010 national standard, with reference to general international standard, according to detecting instrument at that time, can reach high-tech level, listed investigation and detected different natural jades 15 aspects whether up to standard.Specifically as shown in Table 1:
Table one:
More than statistics shows, utilize traditional detection method, to the detection from a jade sample obtain described all 15 item number certificate and the indexs of GB, in 20 applicable steps of routine, have at least 10 steps need to carry out to sample the destructiveness processing of different samplings, there are 3 steps sometimes to need sample to carry out the destructivenesses processing of different samplings, only have 7 steps can destructive sample.Need to provide former stone or jade sample to be processed into the solids such as powder, powder crystal, thin slice, special mating plate, and a plurality of samples such as solvent.This will destroy jade sample, meanwhile, owing to also there is greatest differences in the composition of same jade different parts, so repeatedly sampling, also can the testing result that causes there is the possibility increase of dispute and error, affect test result accuracy and authority.
Sum up, do not having the standardized Khotan jade of State-level or the standard substance of other jades to detect under the prerequisite of sample, the defect of traditional detection technology is:,
(1) these samples are much disposable, have inspected rear disappearance or destruction, and the minimizing of jade sample quality and consumption lose sample exemplary value intuitively originally.
(2) request for utilization makes in teaching and research activity institute's sampling quantity many, and style is many, and specification is many, complex process, and Production Time is long.
(3) program link is many, and length expends time in.
(4) because jade price is high, if sample repeated detection and analysis will be scrapped completely, this has formed huge waste for expensive jade resource, and appraisal cost is large.
(5) because jade is a kind of heterogeneous body aggregate, different parts on same sample, jade composition and structure also often has larger difference, so, at different parts, repeatedly sample, must use different parts sample, and the difficult preservation such as powder, liquefied mixture, these factors all can cause testing result to exist the possibility of error to increase, and affect test result accuracy.
(6) cannot really rise to national standard aspect of material, thereby become corresponding relation with national word canonical form. the development of industry is played to guiding, standard and impetus.
Because above reason, existing all kinds of non-national standard samples cannot meet the requirement of scientific research and social Nondestructive Identification.Owing to there is no the material standard corresponding with national word standard, jade standard is carried out and floated on form, various places testing agency also cannot really require to implement one by one according to GB for the detection of jade, detect certificate and only mark the content that several of hardness, density, refractive indexes etc. etc. are utilized simple instrument naked-eye observation, weakened the authority of testing agency and test result, the development of modern detecting aspect Identification of Jades seriously lagged behind.
Utility model content
The purpose of this utility model is in order to solve technical matters of the prior art, provide that a kind of cost is low, technique is simple, easy to use, be convenient to the jade Non-Destructive Testing instance model promoted.
In order to achieve the above object, the utility model is by the following technical solutions: a kind of jade Non-Destructive Testing instance model, comprise jade mould plate, described jade mould plate is provided with smooth flat district, bucket type thinning area, matrix thinning area, matrix Jin Moqu, matrix carbon film district, tubular thinning area, thoroughly spend variation zone, Guang San prism district, raw material leaves over district, cuts and leave over district, color vector district, special light efficiency district and marked area.
Further, described marked area comprises hardness marked area, composition mark district, lattice marked area, title mark district.
Further, described jade mould plate side is provided with operation skid-proof regions, and described operation skid-proof regions is used for preventing that landing from damaging.
Further, described color vector district is positioned on the jade mould plate side relative with operation skid-proof regions.
Further, described raw material is left over district and is cut and leaves over district and be positioned on jade mould plate side.
Further, described lattice marked area is positioned on jade mould plate side.
Further, it is respectively rectangle projection that described smooth flat district and hardness indicate district, described bucket type thinning area is terrace with edge connected in star, described matrix thinning area is elliposoidal groove, described matrix Jin Moqu and matrix carbon film district are respectively hemispherical groove, described matrix carbon film district groove is darker than matrix Jin Mo district groove, described tubular thinning area is cylindrical grooves, described degree variation zone is oblong-shaped ramps, described Guang San prism district is terrace with edge shape through hole, described composition mark district, lattice marked area, title mark district is respectively rectangular recess, described color vector district is cylindrical grooves, described special light efficiency district is hemispherical projections.
Further, described jade mould plate is rectangular parallelepiped.
Further, described jade mould plate is long is 45mm, and wide is 20mm, and height is 3mm.
The relative prior art of the utility model has following beneficial effect:
1, the utility model making is to be a kind of new product and the new technology of Identification of Jades and teaching research design specially, meet Chinese exclusive jade and learned the demand that the quick nondestructive science and technology of present stage research and development is identified teaching and research, fill up domestic and international jade and detected with identifying teaching and research field and cannot not cut apart sample, not change under the prerequisite of test sample form, obtained fast the blank of 15 national standard data of all regulations and conclusion.
2, the utility model is for helping researcher's rapid systemization to grasp detected jade character in research work, in teaching process, to student, carry out quick on-the-spot teaching demonstration, the Improvement and perfection of the model of the special national standard piece for jade, promote the aspects such as jade mineralogical study and development, there is important practical value.
3, the utility model is significant with assessment jade value to Rapid identification, for the social supervision check in jade market and the law enforcement of cracking down on counterfeit goods etc. provide technical basis.
4, the utility model is due to the function of the sample of the various proterties of set, meet the demand of existing various high-tech detecting instruments, make jade standard substance sample reach the requirement of Non-Destructive Testing and evaluation, with national word standards, can produce in batches by enough existing exact instrument, cost is low, China's jade is detected and stepped into modernization stage and industrialization process.
5, the utility model is because whole process has been used harmless optical detecting instrument, greatly reduced testing process, many links merge, greatly reduced detection time along with jadeware collection climax period is large to Identification of Jades demand, standardization, have the huge market demand, the culture of Chinese jade and industry are just being moved towards to internationalize to have important practical significance.
6, the utility model can detect jade sample and rises to after national standard of physical; can protect better the reputation of China's jade, strengthen its competitive power in market at home and abroad, also can prevent trade barrier; promote technological cooperation, thereby form optimum order and obtain optimal economic social benefit.
7, the utility model stimulates China's checkout equipment production domesticization and industrialization process; break away from China's precision detecting instrument by the situation of minority developed country monopolization abroad; national high-technology industry development to China has great impetus; for standard, good effect is played in its commercial activity meeting; for promoting the unique jade culture of China; advance Chinese jade cultural industry to form and large-scale development, allow Chinese jade culture go to the world and there is very important engine effect.
8, the utility model technique is simple, and disposable making never consumes, avoid the destructive waste of repeatedly sampling, greatly reduced cost, automated production in manufacturing process, shorten making flow process, guaranteed standardization, greatly reduced the sample making time, it is example that the thin slice that original simple utilization of only take is limited to is made a link, original technique, makes by hand substantially, utilizes machine about one day, utilize after the utility model method for making, all processes only need 30-40 minute.
9, the utility model is with respect to current existing other similar amateur products, can produce in batches, preserve transportation safety, easy to use, be convenient to promote.
Accompanying drawing explanation
Fig. 1 is the structural representation of the utility model under first visual angle;
Fig. 2 is the structural representation of the utility model under second visual angle;
Fig. 3 is front view of the present utility model.
Reference numeral implication is as follows: 1, smooth flat district; 2, hardness marked area; 3, bucket type thinning area; 4, matrix thinning area; 5, matrix Jin Moqu; 6, matrix carbon film district; 7, tubular thinning area; 8, thoroughly spend variation zone; 9, Guang San prism district; 10, composition mark district; 11, lattice marked area; 12, raw material is left over district; 13, title mark district; 14, cut and leave over district; 15, color vector district; 16, special light efficiency district; 17, operation skid-proof regions; 18, jade mould plate.
Embodiment
Below in conjunction with accompanying drawing, the utility model is described in further detail:
As Figure 1-3, a kind of jade Non-Destructive Testing instance model, comprises jade mould plate 18, and jade mould plate 18 is rectangular parallelepiped, and jade mould plate 18 is long is 45mm, and wide is 20mm, and height is 3mm, and jade mould plate 18 is provided with smooth flat district 1, bucket type thinning area 3, matrix thinning area 4, matrix Jin Mo district 5, matrix carbon film district 6, tubular thinning area 7, thoroughly spend variation zone 8, Guang San prism district 9, raw material is left over district 12, cut and leave over district 14, color vector district 15, special light efficiency district 16, hardness marked area 2, composition mark district 10, lattice marked area 11, title mark district 13, jade mould plate 18 sides are provided with operation skid-proof regions 17, and operation skid-proof regions 17 is damaged for preventing landing, and color vector district 15 is positioned on jade mould plate 18 sides relative with operation skid-proof regions 17, lattice marked area 11, raw material is left over district 12 and is cut and leaves over district 14 and be positioned on jade mould plate 18 sides, smooth flat district 1 and hardness marked area 2 are respectively rectangle projection, bucket type thinning area 3 is terrace with edge connected in star, matrix thinning area 4 is elliposoidal groove, and matrix Jin Mo district 5 and matrix carbon film district 6 are respectively hemispherical groove, and matrix carbon film district 6 grooves are darker than matrix Jin Mo district 5 grooves, tubular thinning area 7 is cylindrical grooves, degree variation zone 8 is oblong-shaped ramps thoroughly, and Guang San prism district 9 is terrace with edge shape through hole, composition mark district 10, lattice marked area 11, title mark district 13 is respectively rectangular recess, and color vector district 15 is cylindrical grooves, and special light efficiency district 16 is hemispherical projections.
Smooth flat district 1 is for refractometer test refractive index and birefraction and utilize infrared spectrometer and Raman spectrometer test composition, structure and absorption spectrum; Bucket type thinning area 3 for Raman spectrometer at thinner region analysis ingredient, structure and absorption spectrum, utilize jewelry microscope and transmission electron microscope observation crystal property, cleavage and utilize dichroscope test pleochroism; Matrix thinning area 4 for Raman spectrometer at thinner regional analysis composition, structure and absorption spectrum, utilize jewelry microscope and transmission electron microscope observation crystal property, cleavage, form complementary with bucket type thinning area 3; Matrix Jin Mo district 5 is for scanning electron microscope test photosensitiveness feature and observation crystal microstructure, cleavage and utilize electron probe microanalyzer test composition; Matrix carbon film district 6 is for scanning electron microscope test photosensitiveness feature and observation crystal microstructure, cleavage and utilize electron probe microanalyzer test composition, forms complementary with matrix Jin Mo district 5; Crystal, for high-power microscope test photosensitiveness feature, is observed micro-in tubular thinning area 7, comprises structure crystal proterties, growth line, port, rift and utilizes dichroscope test pleochroism; Inspection is amplified for magnifier and jewelry microscope in degree variation zone 8 thoroughly, observes crystal structure characteristic and photosensitiveness feature; Guang San prism district 9 observes and records iridescence for amplifying camera instrument, dispersion phenomenon, test dispersion values and special photosensitiveness; Raw material is left over district 12 for amplifying and picture pick-up device observed and recorded, observes crystal face striped, twin crystal line, colour band, growth pit, etch-figure, molten mound, twin crystal line, studies its external characteristic; Cut leave over district 14 for amplify observe with picture pick-up device and breach, polishing line, micro-breach, cavity, the burning trace of study sample, clash into trace, must shape girdle, extra facet, crest line is sharp-pointed or round and smooth phenomenon, initial analysis judges relative density, hardness, cleavage, the rift surface of jade; Color vector district 15, for sample being observed to gloss and being carried out color vector mark, utilizes the color vector table that existing industry is current, to the color of sample carry out quantitative analysis and and the qualitative mark of digitizing; Asterism, chatoyancy, halo effect, gold sand effect are observed for magnifier or gemolite by special light efficiency district 16; Hardness marked area 2 for hardness pen at compressive surface domain test with indicate hardness; Composition mark district 10 detects laggard rower note for electron probe microanalyzer, infrared spectrometric analyzer, Raman spectrometer, Xray fluorescence spectrometer to sample composition, for calibration instrument with again select survey detecting instrument in process of the test, has suggesting effect; Lattice marked area 11 is carried out icon indication for microscope, scanning electron microscope, transmission electron microscope, nuclear magnetic resonance to recording the crystal orientation lattice of crystal; Title mark district 13 is for carrying out standardization name according to national standard to jade sample.
Possessing under the prerequisite of above all functions, whole instance model is exactly a sample solid that applicable laser volume measuring instrument is measured, can test density and quality.
The detection from a jade sample obtain described all 15 item number certificate and the indexs of GB, specifically application and solutions is as shown in Table 2:
Table two:
By table two, can be drawn, instance model of the present utility model can meet the testing requirement of jade sample, even if some detection methods have some limitations, the distinct methods of another kind of instrument also can make up preferably.
The utility model set traditional mineralogy, the sample routine sampling technology that petrological study is used, the comprehensive common observation thin slice of ore, the micro-mating plate of ore, electronic lens lamination patch, the special light efficiency experiment of jewel ball, transparent dispersive prism, jade inclined-plane thin slice, the advantage of the multi mineral samples such as crystal specimen of ore, according to the requirement of up-to-date natural jade national standard (GB/T-16553-2010), from Identification of Jades, learn teaching and universal practical development demand, systematically designed and do not damaged, cut apart and sample block models is treated in consumption, or do not change under the prerequisite of the existing physical aspect of sample piece and chemical composition, on a monoblock sample, the unlimited special-purpose jade sample moulding that repeats to record and reduce the every detection index of sample to be checked.The utility model has met the demand that Chinese exclusive jade is learned present stage research and development, take " instrumental analysis is as main, and it is auxiliary that macroscopic view is appreciated ", filled up domestic and international blank, also to be made into national jade standard substance sample, directly perceived, practical, convenient contrast detects and research learning, synchronize with national word standard and carry out issue, with respect to current existing other similar amateur products, cost is low, and technique is simple, can produce in batches, preserve transportation safety, easy to use, be convenient to promote.Current on the occasion of jadeware collection climax period to the large standardization of Identification of Jades demand, authenticate technology among the people is tending towards universalness, has the huge market demand, Chinese jade culture and industry are just being moved towards to internationalize and are being had important practical significance.
Claims (5)
1. a jade Non-Destructive Testing instance model, is characterized in that: comprise jade mould plate (18), described jade mould plate (18) is provided with smooth flat district (1), bucket type thinning area (3), matrix thinning area (4), matrix Jin Moqu (5), matrix carbon film district (6), tubular thinning area (7), thoroughly spend variation zone (8), Guang San prism district (9), raw material is left over district (12), cut and leave over district (14), color vector district (15), special light efficiency district (16) and marked area, described marked area comprises hardness marked area (2), composition mark district (10), lattice marked area (11), title mark district (13), described smooth flat district (1) and hardness marked area (2) are respectively rectangle projection, described bucket type thinning area (3) is terrace with edge connected in star, described matrix thinning area (4) is elliposoidal groove, described matrix Jin Moqu (5) and matrix carbon film district (6) are respectively hemispherical groove, described matrix carbon film district (6) groove is darker than matrix Jin Moqu (5) groove, described tubular thinning area (7) is cylindrical grooves, described degree variation zone (8) is oblong-shaped ramps, described Guang San prism district (9) is terrace with edge shape through hole, described composition mark district (10), lattice marked area (11), title mark district (13) is respectively rectangular recess, and described color vector district (15) is cylindrical grooves, and described special light efficiency district (16) is hemispherical projections, described lattice marked area (11), raw material is left over district (12), cut and leave over district (14) and color vector district (15) are positioned on jade mould plate (18) side.
2. a kind of jade Non-Destructive Testing instance model according to claim 1, is characterized in that: described jade mould plate (18) side is provided with operation skid-proof regions (17), and described operation skid-proof regions (17) is damaged for preventing landing.
3. a kind of jade Non-Destructive Testing instance model according to claim 2, is characterized in that: described color vector district (15) is positioned on jade mould plate (18) side relative with operation skid-proof regions (17).
4. a kind of jade Non-Destructive Testing instance model according to claim 1, is characterized in that: described jade mould plate (18) is rectangular parallelepiped.
5. a kind of jade Non-Destructive Testing instance model according to claim 1, is characterized in that: described jade mould plate (18) is long is 45mm, and wide is 20mm, and height is 3mm.
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| CN201420280815.5U CN203894090U (en) | 2014-05-29 | 2014-05-29 | Jade nondestructive testing sample model |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110458804A (en) * | 2019-07-05 | 2019-11-15 | 自然资源部珠宝玉石首饰管理中心(国家珠宝玉石质量监督检验中心) | A kind of hotan jade is sub to expect identification systems and method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110458804A (en) * | 2019-07-05 | 2019-11-15 | 自然资源部珠宝玉石首饰管理中心(国家珠宝玉石质量监督检验中心) | A kind of hotan jade is sub to expect identification systems and method |
| CN110458804B (en) * | 2019-07-05 | 2023-03-10 | 国家珠宝玉石首饰检验集团有限公司 | Xinjiang Hetian jade material identification system and method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: GANSU CULTURAL ART APPRAISAL AND EVALUATION LLC Free format text: FORMER OWNER: WEN XINXU Effective date: 20150707 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20150707 Address after: 3009, good luck carnival, Tianshui North Road, Chengguan District, Gansu, Lanzhou 730010, China Patentee after: Gansu Province cultural art appraisal appraisal Co., Ltd. Address before: 730030, Jincheng Road, Chengguan District, Gansu, Lanzhou Province, Jincheng jewelry, 40 west of the third floor, No. 3, Longxi Patentee before: Wen Xinxu |