CN203862213U - Horizontal type multistage compression reaction kettle - Google Patents
Horizontal type multistage compression reaction kettle Download PDFInfo
- Publication number
- CN203862213U CN203862213U CN201420283522.2U CN201420283522U CN203862213U CN 203862213 U CN203862213 U CN 203862213U CN 201420283522 U CN201420283522 U CN 201420283522U CN 203862213 U CN203862213 U CN 203862213U
- Authority
- CN
- China
- Prior art keywords
- kettle
- reaction still
- horizontal multi
- compressive reaction
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 36
- 230000006835 compression Effects 0.000 title abstract 4
- 238000007906 compression Methods 0.000 title abstract 4
- 230000007246 mechanism Effects 0.000 claims abstract description 11
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 239000012530 fluid Substances 0.000 claims description 8
- 238000005086 pumping Methods 0.000 claims description 8
- 239000011148 porous material Substances 0.000 claims description 5
- 230000007797 corrosion Effects 0.000 claims description 4
- 238000005260 corrosion Methods 0.000 claims description 4
- 230000000670 limiting effect Effects 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 10
- 238000000034 method Methods 0.000 abstract description 8
- 238000005516 engineering process Methods 0.000 abstract description 6
- 238000005265 energy consumption Methods 0.000 abstract description 5
- 238000003756 stirring Methods 0.000 abstract description 5
- 229910052751 metal Inorganic materials 0.000 abstract description 4
- 239000002184 metal Substances 0.000 abstract description 4
- 238000004090 dissolution Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 230000006872 improvement Effects 0.000 description 9
- 239000002585 base Substances 0.000 description 7
- 239000000203 mixture Substances 0.000 description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000004115 Sodium Silicate Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052911 sodium silicate Inorganic materials 0.000 description 2
- 239000003513 alkali Substances 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000009854 hydrometallurgy Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 238000012857 repacking Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Landscapes
- Mixers Of The Rotary Stirring Type (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model relates to a horizontal type multistage compression reaction kettle, which solves the problems that the conventional reaction kettle cannot be connected to enable the materials to be reacted and processed, the processing efficiency is low, the kettle is easily to cause pollution, and the energy consumption is high. The reaction kettle comprises a kettle body, wherein a plurality of baffle plates are arranged in the kettle body; heating devices are arranged between every two adjacent baffle plates; the baffle plates divide the space in the kettle body into a plurality of reaction chambers; the upper parts of every two adjacent reaction chambers are communicated; a plurality of stirring machines are arranged on the kettle body; the stirring machines comprise mounting base plates mounted on the kettle body, driving mechanisms arranged on the mounting base plates, stirring shafts and stirrers inserted into the reaction chambers and driven by the driving mechanisms; each stirring machine is in correspondence with each reaction chamber. According to the horizontal type multistage compression reaction kettle, a horizontal type compression multistate continuous operation method is adopted, so that materials are subjected to multistage continuous dissolution or reaction in one horizontal type reaction kettle, the solution mole number and the valuable metal components can meet the requirements of the technology, the production and processing technological processes are simplified, and the efficiency of the products is greatly improved.
Description
Technical field
The utility model relates to a kind of reactor, is specifically related to a kind of horizontal multi-stage compressive reaction still.
Background technology
Current domestic production sodium silicate solution waterglass, generally all adopt Batch Process, be about to the flower bulb alkali of high-temperature fusion shape cooling after, drop into again in normal-pressure reaction kettle and dissolve and be prepared into sodium silicate solution, step is comparatively loaded down with trivial details and conventionally need to change a plurality of reactors like this, and production efficiency is low, energy loss is serious; Also have in some hydrometallurgy extract technology processes, conventionally also take normal pressure equipment to leach and extract valuable metal composition in ore pulp, but its process exists easily, pollute, the shortcoming such as energy consumption is large, and efficiency is low.
Summary of the invention
For existing reactor in solution background technology can not connect, make material reaction processing, exist working (machining) efficiency low, easily pollute, the problem that energy consumption is large, the utility model provides a kind of horizontal multi-stage compressive reaction still.
The technical solution of the utility model is: a kind of horizontal multi-stage compressive reaction still, comprise kettle, in described kettle, be provided with a plurality of dividing plates, between described dividing plate, be provided with heater, described a plurality of dividing plates are divided into a plurality of reative cells by the space in kettle, the top of described adjacent reaction chamber is connected, described kettle is provided with a plurality of mixers, described mixer comprises the mounting base being arranged on kettle, be located at the driving mechanism on mounting base, insert in reative cell and the shaft and the agitator that by driving mechanism, are driven, each mixer is corresponding with a reative cell.
As a kind of improvement of the present utility model, the height of described dividing plate is 2/3 to 5/6 of kettle height.
As further improvement of the utility model, the bottom of described dividing plate is provided with intercommunicating pore.
As further improvement of the utility model, described heater adopts vertical U-shaped heating tube or circle serpentine heating pipe.
As further improvement of the utility model, in described kettle, be provided with wearproof net.
As further improvement of the utility model, described mounting base is provided with gap slot, on described shaft, is provided with and puts shaft device, and the described shaft device of putting is located in gap slot.
As further improvement of the utility model, described shaft device and the shaft Joint put, described gap slot is provided with putting the stopper of shaft device axial limiting.
As further improvement of the utility model, described agitator adopts disk turbine agitator.
As further improvement of the utility model, described disk turbine agitator is provided with blade, and the root of described blade is provided with anti-gas corrosion pressure relief vent.
As further improvement of the utility model, also comprise fluid pressure pumping plant, described mixer is provided with mechanical seal, and described fluid pressure pumping plant is connected with mechanical seal.
The beneficial effects of the utility model are, adopt the multistage continued operation method of horizontal pressure, can be by multistage continuous-dissolution or reaction in a horizontal reacting still, reach solution molal quantity and valuable metal composition that technique needs, simplified the step of production and processing technology operation, greatly improve the efficiency of product, also avoided the shortcoming that pollution is large, energy consumption is large existing in production process simultaneously.The utility model also has simple in structure, easy accessibility, the advantage such as floor space is little.
Accompanying drawing explanation
Accompanying drawing 1 is the structural representation of the utility model embodiment.
Accompanying drawing 2 for mixer 5 in accompanying drawing 1 be located in kettle 1 structural representation.
Accompanying drawing 3 is the structural representation of disc turbine formula blade 541.
Accompanying drawing 4 is the top view of accompanying drawing 3.
Accompanying drawing 5 is the structural representation of open turbine formula blade 542.
Accompanying drawing 6 is the top view of accompanying drawing 5.
Accompanying drawing 7 is the structural representation of screw blade 543.
Accompanying drawing 8 is the top view of accompanying drawing 7.
Accompanying drawing 9 is the structure amplification view at I place in accompanying drawing 2.
In figure, 1, kettle; 11, reative cell; 12, wearproof net; 2, fluid pressure pumping plant; 3, dividing plate; 31, intercommunicating pore; 4, heater; 5, mixer; 51, mounting base; 511, gap slot; 512, stopper; 52, driving mechanism; 53, shaft; 531, put shaft device; 54, agitator; 541, disk turbine agitator; 5411, blade; 5412, anti-gas corrosion pressure relief vent; 542, open turbine stirrer; 543, spiral agitator; 55, mechanical seal; 56, reductor; 57, shaft coupling.
The specific embodiment
Below in conjunction with accompanying drawing, the utility model embodiment is described further:
By Fig. 1 in conjunction with Fig. 2, 3, 4, 5, 6, 7, 8, shown in 9, a kind of horizontal multi-stage compressive reaction still, comprise kettle 1 and fluid pressure pumping plant 2, in described kettle 1, be provided with a plurality of dividing plates 3, 3 described, dividing plate is provided with heater 4, specifically, described heater 4 adopts vertical U-shaped heating tube or circle serpentine heating pipe, the setting of heater can be so that the processing effect of product be good, be beneficial to the dispersed with stirring that improves agitator, mix, dissolve, reaction efficiency, in particular, pressure in kettle is higher than normal pressure, more can improve the reaction efficiency of product.Described a plurality of dividing plates 3 are divided into a plurality of reative cells 11 by the space in kettle 1, the top of described adjacent reaction chamber 11 is connected, described kettle 1 is provided with a plurality of mixers 5, described mixer 5 comprises the mounting base 51 that is arranged on kettle 1, be located at driving mechanism 52 on mounting base 51, insert in reative cell 11 and the shaft 53 and the agitator 54 that by driving mechanism 52, are driven, specifically, described driving mechanism 52 is connected with shaft 53 by reductor 56, shaft coupling 57, and described driving mechanism 52 is drive motors.Each mixer 5 is corresponding with a reative cell 11.The utility model is to adopt the multistage continued operation method of horizontal pressure, can be by multistage continuous-dissolution or reaction in a horizontal reacting still, reach solution molal quantity and valuable metal composition that technique needs, simplified the step of production and processing technology operation, greatly improve the efficiency of product, also avoided the shortcoming that pollution is large, energy consumption is large existing in production process simultaneously.The utility model also has simple in structure, easy accessibility, the advantage such as floor space is little.
The height of described dividing plate 3 is 2/3 to 5/6 of kettle 1 height.Specifically, intercommunicating pore 31 can be offered according to solid concentration in the bottom of described dividing plate 3.Such structure makes product processing to control the purity of dissolving gradient or reaction extract according to the adjustment of solid concentration flow.Certainly, in actual production process, can adjust according to the characteristic of institute's converted products the quantity of the height of dividing plate or the distance of adjacent separator or bottom intercommunicating pore.
In described kettle 1, be provided with wearproof net 12.Specifically, described wearproof net 12 is located on the inwall of kettle 1 bottom (referring to accompanying drawing 2).In particular, described wearproof net is fixedly connected with by welding, screw or pin with inner wall of kettle.Arranging of wearproof net effectively reduced the wearing and tearing of solid particle to still bottom, and wearproof net is only arranged on the bottom of tank body, not only simple in structure but also production cost is lower.
Described mounting base 51 is provided with gap slot 511, on described shaft 53, is provided with and puts shaft device 531, and the described shaft device 531 of putting is located in gap slot 511.Described shaft device 531 and shaft 53 Joints put, described gap slot 511 is provided with putting the stopper 512 of shaft device 531 axial limitings.Such structure, when servicing machine seals, avoids shaft to drop, and makes product maintenance convenient.
Described agitator 54 can adopt disk turbine agitator 541, open turbine stirrer 542 or adopt spiral agitator 543 to realize.Certainly in actual production, can select different agitators according to different media, the agitator that can certainly select the utility model not mention, the agitator that the utility model is mentioned certainly also can separately or combine in reactor.Certainly, different mixers can adopt different agitators, and in particular, the indoor mixer of differential responses also can be different.The utility model is provided with blade 5411 on described disk turbine agitator 541, the root of described blade 5411 (root of blade refers near shaft place) is provided with anti-gas corrosion pressure relief vent 5412, such structure avoids blade because centrifugal force liquid is discharged from rear formation vacuum, to be corroded in the course of the work, thereby has guaranteed the service life of product
Described mixer 5 is provided with mechanical seal 55, and described fluid pressure pumping plant 2 is connected with mechanical seal 55.Specifically, in mechanical seal place or fluid pressure pumping plant place, different sensor or the switches such as flow, temperature, pressure, liquid level can be set as required, every data of monitoring system pressure and operation, thus reliability and the security in product processing guaranteed.
Every technical staff's notice: although the utility model describes according to the above-mentioned specific embodiment; but invention thought of the present utility model is not limited in this utility model; the repacking of any utilization inventive concept, all will include in this patent scope of patent protection.
Claims (10)
1. a horizontal multi-stage compressive reaction still, comprise kettle (1), it is characterized in that: in described kettle (1), be provided with a plurality of dividing plates (3), between described dividing plate (3), be provided with heater (4), described a plurality of dividing plates (3) are divided into a plurality of reative cells (11) by the space in kettle (1), the top of described adjacent reaction chamber (11) is connected, described kettle (1) is provided with a plurality of mixers (5), described mixer (5) comprises the mounting base (51) being arranged on kettle (1), be located at the driving mechanism (52) on mounting base (51), insert in reative cell (11) and the shaft (53) and the agitator (54) that by driving mechanism (52), are driven, each mixer (5) is corresponding with a reative cell (11).
2. horizontal multi-stage compressive reaction still according to claim 1, the height that it is characterized in that described dividing plate (3) is 2/3 to 5/6 of kettle (1) height.
3. horizontal multi-stage compressive reaction still according to claim 1 and 2, is characterized in that the bottom of described dividing plate (3) is provided with intercommunicating pore (31).
4. horizontal multi-stage compressive reaction still according to claim 1, is characterized in that described heater (4) adopts vertical U-shaped heating tube or circle serpentine heating pipe.
5. horizontal multi-stage compressive reaction still according to claim 1, is characterized in that being provided with wearproof net (12) in described kettle (1).
6. horizontal multi-stage compressive reaction still according to claim 1, it is characterized in that described mounting base (51) is provided with gap slot (511), on described shaft (53), be provided with and put shaft device (531), the described shaft device (531) of putting is located in gap slot (511).
7. horizontal multi-stage compressive reaction still according to claim 6, is characterized in that described shaft device (531) and shaft (53) Joint put, and described gap slot (511) is provided with putting the stopper (512) of shaft device (531) axial limiting.
8. horizontal multi-stage compressive reaction still according to claim 1, is characterized in that described agitator (54) adopts disk turbine agitator (541).
9. horizontal multi-stage compressive reaction still according to claim 8, is characterized in that described disk turbine agitator (541) is provided with blade (5411), and the root of described blade (5411) is provided with anti-gas corrosion pressure relief vent (5412).
10. horizontal multi-stage compressive reaction still according to claim 1, characterized by further comprising fluid pressure pumping plant (2), and described mixer (5) is provided with mechanical seal (55), and described fluid pressure pumping plant (2) is connected with mechanical seal (55).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201420283522.2U CN203862213U (en) | 2014-05-30 | 2014-05-30 | Horizontal type multistage compression reaction kettle |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201420283522.2U CN203862213U (en) | 2014-05-30 | 2014-05-30 | Horizontal type multistage compression reaction kettle |
Publications (1)
Publication Number | Publication Date |
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CN203862213U true CN203862213U (en) | 2014-10-08 |
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CN201420283522.2U Expired - Lifetime CN203862213U (en) | 2014-05-30 | 2014-05-30 | Horizontal type multistage compression reaction kettle |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104826572A (en) * | 2015-04-23 | 2015-08-12 | 宜兴市聚金信化工有限公司 | Neutralization reaction device for rubber antioxidant production |
CN105664820A (en) * | 2016-01-14 | 2016-06-15 | 湘潭大学 | Horizontal reactor |
CN105734280A (en) * | 2016-05-18 | 2016-07-06 | 招金矿业股份有限公司金翅岭金矿 | Square leaching tank |
WO2017181761A1 (en) * | 2016-04-18 | 2017-10-26 | 山东万圣博科技股份有限公司 | Apparatus and method for continuous melting of phenylenediamine |
CN110170292A (en) * | 2019-06-24 | 2019-08-27 | 上海华谊(集团)公司 | Hydroformylation process, reaction unit and the reaction system using the device |
CN112494988A (en) * | 2020-12-11 | 2021-03-16 | 浙江工业大学 | Horizontal liquid-liquid extraction device and use method thereof |
-
2014
- 2014-05-30 CN CN201420283522.2U patent/CN203862213U/en not_active Expired - Lifetime
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104826572A (en) * | 2015-04-23 | 2015-08-12 | 宜兴市聚金信化工有限公司 | Neutralization reaction device for rubber antioxidant production |
CN105664820A (en) * | 2016-01-14 | 2016-06-15 | 湘潭大学 | Horizontal reactor |
CN105664820B (en) * | 2016-01-14 | 2018-05-25 | 湘潭大学 | Horizontal reactor |
WO2017181761A1 (en) * | 2016-04-18 | 2017-10-26 | 山东万圣博科技股份有限公司 | Apparatus and method for continuous melting of phenylenediamine |
CN105734280A (en) * | 2016-05-18 | 2016-07-06 | 招金矿业股份有限公司金翅岭金矿 | Square leaching tank |
CN105734280B (en) * | 2016-05-18 | 2018-08-24 | 招金矿业股份有限公司金翅岭金矿 | A kind of rectangular leaching tanks |
CN110170292A (en) * | 2019-06-24 | 2019-08-27 | 上海华谊(集团)公司 | Hydroformylation process, reaction unit and the reaction system using the device |
CN112494988A (en) * | 2020-12-11 | 2021-03-16 | 浙江工业大学 | Horizontal liquid-liquid extraction device and use method thereof |
CN112494988B (en) * | 2020-12-11 | 2023-12-19 | 浙江工业大学 | Horizontal liquid-liquid extraction device and application method thereof |
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Legal Events
Date | Code | Title | Description |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CX01 | Expiry of patent term | ||
CX01 | Expiry of patent term |
Granted publication date: 20141008 |