CN203842576U - Enamel reaction kettle suitable for producing vitamin E - Google Patents
Enamel reaction kettle suitable for producing vitamin E Download PDFInfo
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- CN203842576U CN203842576U CN201420155745.0U CN201420155745U CN203842576U CN 203842576 U CN203842576 U CN 203842576U CN 201420155745 U CN201420155745 U CN 201420155745U CN 203842576 U CN203842576 U CN 203842576U
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- China
- Prior art keywords
- kettle
- reaction kettle
- enamel reaction
- producing vitamin
- enamel
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Abstract
The utility model provides an enamel reaction kettle suitable for producing vitamin E. The enamel reaction kettle comprises a kettle body, a reaction kettle cavity, a stirring shaft, a motor, a stirrer and a discharging hole, wherein the reaction kettle cavity is arranged in the kettle body; the motor drives the stirring shaft to rotate; the stirrer is arranged at the tail end of the stirring shaft; the discharging hole is formed at the bottom part of the kettle body; the kettle body is also internally provided with a vacuum device which is positioned at the upper part of the reaction kettle cavity; the vacuum device is separated from the reaction kettle cavity by a partitioning plate and comprises a cylinder, a piston, an exhausting hole and a gas inlet hole; the piston is positioned in the cylinder and can move in a reciprocating manner; the exhausting hole is positioned at the outer wall of the kettle body; the gas inlet hole penetrates through the partitioning plate; and the top part of the kettle body is provided with a transmission mechanism for driving the piston to move in a reciprocating manner. The enamel reaction kettle provided by the utility model has the advantages that before use, air in the reaction kettle can be exhausted, so that substances to be reacted is prevented from being polluted; and the enamel reaction kettle is suitable for producing the vitamin E.
Description
Technical field
The invention belongs to reactor technical field, relate in particular to a kind of enamel reaction still that is suitable for producing vitamin E.
Background technology
Enamel reaction still is will be containing the glass of high silicon dioxide, and lining is at the inner surface of steel vessel, and through high temperature sintering and securely adherence becomes composite product on metal surface.So it has the stability of glass and the two-fold advantage of metal strength, be a kind of good corrosion resistant apparatus, be widely used in the fields such as chemical industry, medicine, agricultural chemicals and fuel.But some material in still, impurity easily and in air reacts, and a lot of reaction needed are carried out under the environment of low pressure, and although existing enamel reaction still sealing is better, but before reaction, in still, still can retain a certain amount of air, ensuing reaction is affected.
Summary of the invention
For addressing the above problem, technical scheme of the present utility model is, a kind of enamel reaction still that is suitable for producing vitamin E is provided, and comprises kettle, be located at the reactor chamber in described kettle, shaft, drives the motor of described shaft rotation, is installed on the agitator of described shaft tail end, be located at the discharging opening of described autoclave body bottom, in described kettle, be also provided with vacuum plant, described vacuum plant is positioned at the top in described reactor chamber, and described vacuum plant separates by dividing plate and described reactor chamber; Described vacuum plant comprises cylinder, is positioned at the reciprocating piston of cylinder interior, is positioned at the steam vent of described kettle outer wall, runs through the air admission hole of described dividing plate; Described kettle top is provided with the transmission mechanism that drives described reciprocating motion of the pistons.
Described transmission mechanism comprises gear drive and toggle, described gear drive comprises driving wheel, driven pulley and follower, described driven pulley is coaxially connected with follower, and described follower is connected with the crank of described toggle, thereby drives described piston movement.
Further, described driving wheel is driven by described motor.
Preferably, described shaft is provided with shaft seal through the position of described dividing plate.
Preferably, the lower surface of described dividing plate is coated with one deck enamel.
Preferably, on the inwall in described reactor chamber, temperature sensor is installed, for observing reaction temperature.
Beneficial effect: before use, the air of reactor inside can be extracted out, prevent from polluting question response material, be applicable to producing vitamin E, and vacuum plant and shaft are used same motor to drive, economize on resources, the fricative heat of piston movement can also be accelerated extent of reaction simultaneously, simple in structure.
For above-mentioned and relevant object, one or more embodiment comprise below by the feature that describes in detail and particularly point out in the claims.Explanation below and accompanying drawing describe some illustrative aspects in detail, and its indication is only some modes in the utilizable variety of way of principle of each embodiment.Other benefit and novel features consider the detailed description along with below by reference to the accompanying drawings and become obviously, and the disclosed embodiments are to comprise being equal to of all these aspects and they.
accompanying drawing explanation
Below in conjunction with accompanying drawing, the utility model is further described.
Fig. 1 is the structural representation of the utility model enamel reaction still;
Fig. 2 is the utility model drive mechanism schematic diagram;
Fig. 3 is the utility model toggle structural representation.
The specific embodiment
As shown in Figures 1 to 3, for the utility model is suitable for producing the enamel reaction still of vitamin E, comprise kettle, in described kettle 1, leave a cavity, as reactor chamber 7; Shaft 2; Drive the motor 3 of described shaft 2 rotations; Be installed on the agitator 4 of described shaft 2 tail ends, described agitator 4 can be selected U-shaped, or inverted T-shaped, can be according to reaction needed selected shape; Be located at the discharging opening 5 of described kettle 1 bottom.In described kettle 1, be also provided with vacuum plant, the outer wall of described vacuum plant and described kettle 1 share, and described vacuum plant is positioned at the top in described reactor chamber 7, and described vacuum plant separates by dividing plate 6 and described reactor chamber 7; Described vacuum plant encloses formation cylinder by shared outer wall and described dividing plate 6, is positioned at the reciprocating piston 8 of cylinder interior, and piston 8 can be selected steel alloy or polytetrafluoroethylene (PTFE).Be positioned at the steam vent 9 of described kettle 1 outer wall, the air admission hole 10 that runs through described dividing plate 6, when described piston 8 is when taking exercises, air compressing in described cylinder, density increases, cause pressure to increase, steam vent 9 is opened, carry out exhaust, when described piston 8 moves right, accordingly, gas pressure intensity diminishes, INO, extract the gas in described reactor chamber out, kettle 1 top is provided with and drives the reciprocating transmission mechanism 11 of described piston 8, therefore before reaction, can carry out steps of exhausting, in the process of reaction, also can bleed, and in reciprocating motion of the pistons process, because friction can produce heat, also can accelerate reaction rate.
In some optional embodiments, described transmission mechanism 11 comprises gear drive and toggle, described gear drive comprises driving wheel 12, driven pulley 13 and follower 14, described driving wheel 12 and described driven pulley 13 engagements, drive described driven pulley 13 motions, again because described driven pulley 13 is coaxially connected with follower 14, thereby drive described follower 14 motions, the surface of described follower 14 can be provided with a projection, projection is provided with axle construction, described follower 14 is connected with the crank of described toggle by axle construction, the motion of crank drivening rod, thereby drive described piston 8 motions that are connected with described connecting rod.
In some optional embodiments, described driving wheel 12 is driven by described motor 3, and described vacuum plant and described shaft 2 are used same motor to drive, and economize on resources.
In some optional embodiments, described shaft 2 is provided with shaft seal through the position of described dividing plate 6, increases sealing.
In some optional embodiments, the lower surface of described dividing plate 6 is coated with one deck enamel, prevents that reactant from corroding described dividing plate 6.
In some optional embodiments, on the inwall in described reactor chamber 7, temperature sensor 15 is installed, for observing reaction temperature, regulate extent of reaction.
Those skilled in the art it is also understood that various illustrative box, module, circuit and the algorithm steps in conjunction with embodiment herein, described all can be embodied as electronic hardware, computer software or its combination.For the interchangeability between hardware and software is clearly described, above various illustrative parts, frame, module, circuit and step have all been carried out usually describing around its function.As for this function, be embodied as hardware or be embodied as software, depend on specific application and the design constraint that whole system is applied.Those skilled in the art can realize described function in flexible mode for each application-specific, still, thisly realize decision-making and should not be construed as and deviate from protection domain of the present disclosure.
Claims (6)
1. an enamel reaction still that is suitable for producing vitamin E, comprise kettle (1), be located at the reactor chamber (7) in described kettle (1), shaft (2), drive the motor (3) of described shaft (2) rotation, be installed on the agitator (4) of described shaft (2) tail end, be located at the discharging opening (5) of described kettle (1) bottom, it is characterized in that, described kettle is also provided with vacuum plant in (1), described vacuum plant is positioned at the top in described reactor chamber (7), and described vacuum plant separates by dividing plate (6) and described reactor chamber (7); Described vacuum plant comprises cylinder, is positioned at the reciprocating piston of cylinder interior (8), is positioned at the steam vent (9) of described kettle (1) outer wall, runs through the air admission hole (10) of described dividing plate (6); Described kettle (1) top is provided with and drives the reciprocating transmission mechanism of described piston (8) (11).
2. a kind of enamel reaction still that is suitable for producing vitamin E according to claim 1, it is characterized in that, described transmission mechanism (11) comprises gear drive and toggle, described gear drive comprises driving wheel (12), driven pulley (13) and follower (14), described driven pulley (13) is coaxially connected with follower (14), described follower (14) is connected with the crank of described toggle, thereby drives described piston (8) motion.
3. a kind of enamel reaction still that is suitable for producing vitamin E according to claim 2, is characterized in that, described driving wheel (12) is driven by described motor (3).
4. a kind of enamel reaction still that is suitable for producing vitamin E according to claim 1, is characterized in that, described shaft (2) is provided with shaft seal through the position of described dividing plate (6).
5. a kind of enamel reaction still that is suitable for producing vitamin E according to claim 1, is characterized in that, the lower surface of described dividing plate (6) is coated with one deck enamel.
6. according to described a kind of enamel reaction still that is suitable for producing vitamin E of claim 1 to 5 any one, it is characterized in that, temperature sensor (15) is installed, for observing reaction temperature on the inwall in described reactor chamber (7).
Priority Applications (1)
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CN201420155745.0U CN203842576U (en) | 2014-04-01 | 2014-04-01 | Enamel reaction kettle suitable for producing vitamin E |
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CN201420155745.0U CN203842576U (en) | 2014-04-01 | 2014-04-01 | Enamel reaction kettle suitable for producing vitamin E |
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CN203842576U true CN203842576U (en) | 2014-09-24 |
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CN201420155745.0U Expired - Fee Related CN203842576U (en) | 2014-04-01 | 2014-04-01 | Enamel reaction kettle suitable for producing vitamin E |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104511268A (en) * | 2014-11-27 | 2015-04-15 | 宁波远欧精细化工有限公司 | Reaction kettle |
CN106633504A (en) * | 2016-11-25 | 2017-05-10 | 重庆澳菱工贸有限公司 | Preparation method and device of polyvinyl chloride plastic dipping fluid |
CN106732250A (en) * | 2016-11-25 | 2017-05-31 | 重庆澳菱工贸有限公司 | Leaching modeling liquid prepares kettle |
-
2014
- 2014-04-01 CN CN201420155745.0U patent/CN203842576U/en not_active Expired - Fee Related
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104511268A (en) * | 2014-11-27 | 2015-04-15 | 宁波远欧精细化工有限公司 | Reaction kettle |
CN104511268B (en) * | 2014-11-27 | 2016-10-05 | 宁波远欧精细化工有限公司 | A kind of reactor |
CN106633504A (en) * | 2016-11-25 | 2017-05-10 | 重庆澳菱工贸有限公司 | Preparation method and device of polyvinyl chloride plastic dipping fluid |
CN106732250A (en) * | 2016-11-25 | 2017-05-31 | 重庆澳菱工贸有限公司 | Leaching modeling liquid prepares kettle |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: Enamel reaction kettle suitable for producing vitamin E Effective date of registration: 20170815 Granted publication date: 20140924 Pledgee: Bank of China, Limited by Share Ltd, Shuyang branch Pledgor: Jiangsu Xi Xin VITAMIN company limited Registration number: 2017320000027 |
|
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140924 Termination date: 20200401 |