CN203811588U - Thin-layer chromatography sample applying device - Google Patents

Thin-layer chromatography sample applying device Download PDF

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Publication number
CN203811588U
CN203811588U CN201420152462.0U CN201420152462U CN203811588U CN 203811588 U CN203811588 U CN 203811588U CN 201420152462 U CN201420152462 U CN 201420152462U CN 203811588 U CN203811588 U CN 203811588U
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China
Prior art keywords
needle
thin
point sample
sample applying
sample
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Expired - Fee Related
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CN201420152462.0U
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Chinese (zh)
Inventor
杜海坤
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Individual
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Individual
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Expired - Fee Related legal-status Critical Current

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Abstract

The utility model relates to a thin-layer chromatography sample applying device which is characterized by comprising a sample applying needle and a sample applying bracket, wherein the sample applying needle comprises a needle tube and a needle head, and a baffle is arranged on the needle head; the sample applying bracket comprises a flat plate, a bracket frame and four bracket legs, wherein a sample applying hole which is used for allowing the needle head to pass through is formed in the flat plate, the diameter of the sample applying hole is less than that of the baffle, the flat plate is connected with the bracket frame through a clamping groove, scales are formed in one side of the bracket frame, and the bracket legs with adjustable heights can extend and retract up and down; the distance between the baffle and the flat tip of the sample applying needle is equal to that between a plane in which the sample applying hole is formed and a thin-layer plate. The thin-layer chromatography sample applying device has the advantages of simplicity and convenience in operation and no need of control over sample applying strength and is suitable for beginners to perform sample application.

Description

A kind of thin-layer chromatography spot sample device
Technical field
The utility model relates to a kind of thin-layer chromatography spot sample device, belongs to technical field of chromatographic analysis.
Background technology
Thin-layered chromatography is a kind of important experimental technique of chemistry, field of medicaments, while using thin-layered chromatography to carry out qualitative or quantitative test, general tack spotting needle or the microsyringe of adopting carries out point sample, when point sample, syringe needle need contact with thin layer plate, but in point sample process, the dynamics of point sample is not easy to hold, dynamics is excessive, easily the coating thing on thin layer plate is punctured, cause the inhomogeneous of point sample, affect the effect of thin-layer developing; Dynamics is too small, and the Contact Thin laminate that syringe needle can not be good causes sample point sample amount very few; Meanwhile, for beginner, in point sample process, hand is easily shaken, and the more difficult dynamics to point sample is controlled, and has had a strong impact on the quality of point sample.
Utility model patent " a kind of sampling needle for thin-layer chromatography ", number of patent application 201320276138.5, a kind of sampling needle for thin-layer chromatography is disclosed, adopt the frame mode that connects moving casing and fixed sleeving by spring, making syringe needle to more easy-regulating of the pressure of thin layer plate, although this sampling needle for thin-layer chromatography has solved the uppity problem of point sample dynamics to a certain extent, but still is manual force, for beginner, be still difficult for operating.
Utility model patent " sample dripping bracket of microsyringe ", number of patent application 201120146715.X, discloses a kind of sample dripping bracket of microsyringe, adopts this support point sample convenient, material is easy to get, but this sample dripping bracket of microsyringe still comes with some shortcomings, after injector is inserted, also need manually to adjust the height of injector syringe needle and place, three leg bottoms plane, more time-consuming, in addition, plug has blocked the part scale of injector, is not suitable for carrying out sxemiquantitative or quantitative thin-layer chromatographic analysis.
Summary of the invention
The purpose of this utility model is to overcome the shortcoming existing in prior art, provides a kind of easy and simple to handle, and without controlling point sample dynamics, applicable beginner carries out the thin-layer chromatography spot sample device of point sample operation.
For achieving the above object, the utility model adopts following scheme:
A kind of thin-layer chromatography spot sample device, comprises spotting needle and point sample support, and described spotting needle comprises needle tubing and syringe needle, and syringe needle is provided with baffle plate; Described point sample support comprises flat board, stand frame and 4 rack legs, and described flat board is provided with the point sample hole that can pass for syringe needle, and the diameter in point sample hole is less than the diameter of baffle plate, and flat board is connected by draw-in groove with stand frame, and a side of stand frame is provided with scale; Described rack leg can stretch up and down, highly adjustable; Described baffle plate equates with the distance of place, point sample hole plane separation thin layer plate apart from the distance of spotting needle tack needle point.
Described flat board is made up of transparent plastic.
The quantity in described point sample hole is at least 1.
When use, by a side of stand frame near thin layer plate, because the thickness of thin layer plate may there are differences, before point sample, the length of rack leg is finely tuned, baffle plate is equated, by the scale on stand frame one side frame apart from the distance of spotting needle tack needle point with the distance of place, point sample hole plane separation thin layer plate, can determine easily the distance between point sample position and adjacent two point of samples, complete after a point sample, by the dull and stereotyped mobile point sample of pull hole, carry out next point sample.
The beneficial effects of the utility model are:
(1) the utility model is simple to operate, because baffle plate equates with the distance of place, point sample hole plane separation thin layer plate apart from the distance of spotting needle tack needle point, therefore without the dynamics of controlling point sample, there will not be the bad phenomenon that causes point sample failure of holding because of point sample dynamics, be particularly suitable for beginner and use;
(2) stand frame is provided with scale, and the distance between convenient position and adjacent two point of samples of determining point sample is carried out point sample by the dull and stereotyped mobile point sample of pull hole, each point of sample point-blank, without pencil setting-out on thin layer plate again.
Brief description of the drawings
Fig. 1 is the utility model structural representation.
Description of reference numerals:
1-needle tubing; 2-syringe needle; 3-baffle plate; 4-point sample hole; 5-flat board; 6-stand frame; 7-rack leg.
Embodiment
Below in conjunction with accompanying drawing, embodiment of the present utility model is described, the utility model discloses a kind of thin-layer chromatography spot sample device, comprise spotting needle and point sample support, described spotting needle comprises needle tubing 1 and syringe needle 2, syringe needle 1 is provided with baffle plate 3; Described point sample support comprises 6 and 4 rack legs 7 of flat board 5, stand frame that are made up of transparent plastic, described dull and stereotyped 5 are provided with the point sample hole 4 that can pass for syringe needle 2, the diameter in point sample hole 4 is less than the diameter of baffle plate 3, and dull and stereotyped 5 are connected by draw-in groove with stand frame 6, and a side of stand frame 6 is provided with scale; Described rack leg 7 can stretch up and down, highly adjustable; Described baffle plate 3 equates with the distance of point sample hole 4 place plane separation thin layer plates apart from the distance of spotting needle tack needle point.
Method of operating: when use, by a side of stand frame 6 near thin layer plate, because the thickness of thin layer plate may there are differences, before point sample, the length of rack leg 7 is finely tuned, baffle plate 3 is equated with the distance of point sample hole 4 place plane separation thin layer plates apart from the distance of spotting needle tack needle point, by the scale on stand frame 6 one side frames, can determine easily the distance between point sample position and adjacent two point of samples, complete after a point sample, by the dull and stereotyped mobile point sample of pull hole, carry out next point sample.
By reference to the accompanying drawings embodiment of the present utility model is described although above-mentioned; but the not restriction to the utility model protection domain; one of ordinary skill in the art should be understood that; on the basis of the technical solution of the utility model, those skilled in the art do not need to pay various amendments that creative work can make or distortion still in protection domain of the present utility model.

Claims (3)

1. a thin-layer chromatography spot sample device, is characterized in that, comprises spotting needle and point sample support, and described spotting needle comprises needle tubing and syringe needle, and syringe needle is provided with baffle plate; Described point sample support comprises flat board, stand frame and 4 rack legs, and described flat board is provided with the point sample hole that can pass for syringe needle, and the diameter in point sample hole is less than the diameter of baffle plate, and flat board is connected by draw-in groove with stand frame, and a side of stand frame is provided with scale; Described rack leg can stretch up and down, highly adjustable; Described baffle plate equates with the distance of place, point sample hole plane separation thin layer plate apart from the distance of spotting needle tack needle point.
2. a kind of thin-layer chromatography spot sample device as claimed in claim 1, is characterized in that, described flat board is made up of transparent plastic.
3. a kind of thin-layer chromatography spot sample device as claimed in claim 1, is characterized in that, the quantity in described point sample hole is at least 1.
CN201420152462.0U 2014-04-01 2014-04-01 Thin-layer chromatography sample applying device Expired - Fee Related CN203811588U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420152462.0U CN203811588U (en) 2014-04-01 2014-04-01 Thin-layer chromatography sample applying device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420152462.0U CN203811588U (en) 2014-04-01 2014-04-01 Thin-layer chromatography sample applying device

Publications (1)

Publication Number Publication Date
CN203811588U true CN203811588U (en) 2014-09-03

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CN201420152462.0U Expired - Fee Related CN203811588U (en) 2014-04-01 2014-04-01 Thin-layer chromatography sample applying device

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104965047A (en) * 2014-10-13 2015-10-07 中国药科大学 Novel planar chromatography sample application instrument and step repeated sample application method
CN105424864A (en) * 2015-12-30 2016-03-23 宁波美成生物科技有限公司 Trace sample injecting device
CN105954458A (en) * 2016-07-25 2016-09-21 哈尔滨理工大学 Thin-layer chromatography sample application needle with supporting feet
CN110082473A (en) * 2019-05-16 2019-08-02 广州市鹭江远科技有限公司 A kind of spot sample device for aflatoxins detection based on thin layer chromatography
CN114544853A (en) * 2022-02-23 2022-05-27 山西农业大学 Multifunctional sample application device for planar chromatography

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104965047A (en) * 2014-10-13 2015-10-07 中国药科大学 Novel planar chromatography sample application instrument and step repeated sample application method
CN105424864A (en) * 2015-12-30 2016-03-23 宁波美成生物科技有限公司 Trace sample injecting device
CN105424864B (en) * 2015-12-30 2017-06-20 宁波美成生物科技有限公司 Two-dimensional deviT
CN105954458A (en) * 2016-07-25 2016-09-21 哈尔滨理工大学 Thin-layer chromatography sample application needle with supporting feet
CN110082473A (en) * 2019-05-16 2019-08-02 广州市鹭江远科技有限公司 A kind of spot sample device for aflatoxins detection based on thin layer chromatography
CN114544853A (en) * 2022-02-23 2022-05-27 山西农业大学 Multifunctional sample application device for planar chromatography

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140903

Termination date: 20150401

EXPY Termination of patent right or utility model