CN203715704U - Combined 11t reduction-evaporation furnace suitable for producing titanium sponge - Google Patents

Combined 11t reduction-evaporation furnace suitable for producing titanium sponge Download PDF

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Publication number
CN203715704U
CN203715704U CN201420089238.1U CN201420089238U CN203715704U CN 203715704 U CN203715704 U CN 203715704U CN 201420089238 U CN201420089238 U CN 201420089238U CN 203715704 U CN203715704 U CN 203715704U
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China
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heater
titanium sponge
furnace
shaped reactor
applicable
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CN201420089238.1U
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Chinese (zh)
Inventor
梁曦彬
田忠元
丁星颖
吕涛
杨翰元
秦为涛
庞海龙
张素超
潘多鹏
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Jinchuan Group Co Ltd
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Jinchuan Group Co Ltd
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Abstract

The utility model discloses a combined 11t reduction-evaporation furnace suitable for producing titanium sponge. The reduction-evaporation furnace comprises a furnace body and a U-shaped reactor cylinder vertically arranged in the furnace body, wherein a flange of the U-shaped reactor cylinder is mounted on the top of the furnace body, the U-shaped reactor cylinder is internally provided with a magnesium chloride discharge pipe, a large reactor cover is arranged on the U-shaped reactor cylinder and is provided with a feed pipe, a reactor vacuumizing pipe, a heating pipe, an inner heater and an outer heater, the ratio of the length to the diameter of the U-shaped reactor cylinder is 2.48 and the ratio of the length to the diameter of the furnace body is 2.16. Since the aluminum silicate fiber precast blocks and calcium silicate insulation bricks are applied in the reduction-evaporation furnace disclosed by the utility model, the insulation effect of the furnace lining is good. Compared with the traditional furnace with insulation bricks as a lining, the reduction-evaporation furnace has the characteristics of small specific heat of furnace lining, less absorption of heat, fast heating, good insulation properties and the like. The production capacity per furnace reaches 11t and the power consumption is reduced to 4000kw.h/t.

Description

A kind of 11t that is applicable to titanium sponge production combines also-steam stove
Technical field
The utility model belongs to titanium sponge and produces also-steam stove technical field, is specifically related to a kind of 11t that is applicable to titanium sponge production and combines also-steam stove.
Background technology
In sponge titanium smelting process, in the situation that early stage, raw material and equipment met the demands, going back steaming process production and determined quality product, power consumption, is crucial in sponge titanium smelting technique and important link.
The energy utilization rate that China's titanium industry is produced is greatly improved in recent years, but still has gap with advanced international standard.Analyze as an example of reduction distillation produce titanium sponge by combination method example, China's ton titanium power consumption is down to 6000 kWh/t~8000 kWh/t by 11000 kWh/t at present, is less than 3000 kWh/t and go back steaming process ton titanium power consumption in the integrated process technique of Japan.
At present, owing to abroad titanium metallurgical technology being enforced a tight blockade, force China's titanium sponge to produce away the road of independent research, cause domestic titanium sponge industry production state of the art gap compared with advanced foreign technology larger, be mainly manifested in the aspect such as the optimization of production technique and equipment and the automatization of production process.Domestic current titanium sponge enterprise is external imported technology at the Technology origin of the developing direction of the critical processes such as chlorination, refining, electrolysis.There is not introduction precedent and go back steaming process advanced foreign technology production line, block tight.And domestic titanium sponge industry is for strengthening enterprise competitiveness, all go back successively skill upgrading and the retrofit work of steam stove at present, single stove production capacity tonnage is to maximization future development.
The large-scale inverse u shape of domestic current employing also-steam stove technology be mainly titanium sponge industry Zunyi Titanium Factory of leading enterprise and the Luoyang Shuangrui Wanji Titanium Co., Ltd. faster of growing up in the industry.Zunyi Titanium Factory and Luoyang Shuangrui Wanji Titanium Co., Ltd. are accumulated and are put into practice by knowhow, under the promotion of lifting self market competitiveness, success in succession researched and developed 12t, 10t large-scale energy-saving type inverse u shape also-steam stove technology, and original system is carried out to technological transformation and lifting, put into production, improve single stove production capacity and annual capacity, reduced unit consumption of product and production cost.
Combine also-steam stove production capacity of the 12t of largest domestic belongs to the first in the world, but due to equipment, Process configuration imperfection, and the titanium hard core of core that sticks together is obvious, and density is higher, and hardness is larger, broken difficulty.And combine also-steam stove production capacity of two auspicious 10t is combined also-steam stove list stove production capacity with respect to 12t and has been lacked nearly 2t.Meanwhile, domestic existing 4t, 5t, 6t, 8t, 12t stove thermal insulation layer all adopt common heat preservation clay brick, alumina silicate fiber felt, quartz sand.Lagging material adopts clayey insulating brick and common magnesia brick, due to clay brick and magnesia brick heavier, under hot environment, use for a long time, the phenomenon that there will be stove brick to stay, and the specific heat coefficient of this refractory materials is relatively large, this combine also-heat-up rate of steam stove, heat retaining property are poor, and power consumption is higher.Although, two auspicious 10t combine also-steam stove and have adopted aluminum silicate fiber piece as lagging material, but it is not clear and definite to the requirement of aluminum silicate fiber piece, the selection of aluminum silicate fiber piece is extremely important, and density is too small, and quality kicks the beam, surface does not have solidification treatment, if adopted, easily cause inner lining material in use to occur subsiding, this at home titanium sponge industry promote in limited the biggest factor.
The length-to-diameter ratio difference of combining also-steam stove corresponding to the type of furnace of different tonnages.The steam stove length-to-diameter ratio of going back of 5t, 6t, 8t, 10t, 12t is respectively 2.07,2.08,2.51,2.43,2.52.Thereby the length-to-diameter ratio of corresponding reactor size is also different.The length-to-diameter ratio of 10t stove is 1.94.At present, row's magnesium chloride climb wall pipe problem of Cracking, affect the discharge of magnesium chloride, belong to the common problem existing in titanium sponge industry, be badly in need of being resolved.In addition, at present traditional resistance wire structure go back steam stove, separate unit stove electrical heating element consumption is large, manufacturing cost is high, group number is many, manufacture uneconomical, and due to support resistance wire to put a brick quantity more, invisible weight and the caloric receptivity that increases furnace lining material, has increased furnace lining and has stayed possibility and the power consumption that phenomenon occurs.Meanwhile, traditional furnace type structure can not effectively be avoided the come off phenomenon of overlap resistance silk of carbon steel reactor iron scale cheaply, easily causes going back steam stove electrical heating element ground connection, cannot make to go back steam stove and reach technological control temperature and be forced to and end to produce.Secondly, the inlet and outlet that tradition is gone back steam stove adopts natural ventilation system, can not effectively take away the amount of heat producing due to thermopositive reaction in reactor, causes Sponge Titanium compact structure, and hard core is larger.
Utility model content
The purpose of this utility model is the technical problem existing in prior art in order to solve, and provides a kind of 11t that is applicable to titanium sponge production to combine also-steam stove.
In order to achieve the above object, the utility model is by the following technical solutions: be a kind ofly applicable to the 11t that titanium sponge produces and combine also-steam stove, comprise body of heater and be vertically arranged on the U-shaped reactor shell in body of heater, the flange of described U-shaped reactor shell is arranged on body of heater top, the row's of being provided with magnesium chloride pipe in described U-shaped reactor shell, described U-shaped reactor shell is provided with the large lid of reactor, described reactor covers greatly and is provided with filling tube, reactor vacuum-pumping tube, heating tube, internal heater and external heat device, the length-to-diameter of described U-shaped reactor shell is 2.48, the length-to-diameter of described body of heater is 2.16, on described inboard wall of furnace body, be bonded with alumina silicate fiber felt, be close to alumina silicate fiber felt and build calcium silicate thermal insulation brick from top to bottom by laying bricks or stones, be close to calcium silicate thermal insulation brick and build aluminum silicate fiber prefabricated section from top to bottom by laying bricks or stones, on described aluminum silicate fiber prefabricated section, be provided with resistive band from top to bottom, described bottom of furnace body is followed successively by alumina silicate fiber felt and high-alumina lightening insulating brick from bottom to top, described high-alumina lightening insulating brick is connected with the aluminum silicate fiber prefabricated section on inboard wall of furnace body, described furnace body outer wall is provided with takes out body of heater valve tube, air intake band and air-out band, described air-out band is positioned at the below of air intake band, on described air intake band and air-out band, be respectively equipped with blast pipe and air outlet tube, described blast pipe is connected with blower fan, the position of the inner corresponding air intake band of described body of heater and air-out band is provided with air port.
As further improvement of the utility model, described row's magnesium chloride pipe is homogeneous tube structure.
As further improvement of the utility model, Tao Ding by hollow on described aluminum silicate fiber prefabricated section is fixed with 7 groups of resistive bands from top to bottom through the fixed orifices of the anti-oxidation iron sheet corundum the brim of a hat, described resistive band and the welding of external terminal stud, be provided with nickel network rod in the Tao Ding of described hollow.
As further improvement of the utility model, described blast pipe is to be respectively equipped with air inlet adjustment valve on two and each blast pipe.
As further improvement of the utility model, described air outlet tube is one.
As further improvement of the utility model, described inboard wall of furnace body is provided with 2 layers of aligning post, and every layer of aligning post is 8 and is distributed on inboard wall of furnace body one week.
As further improvement of the utility model, on the flange of described body of heater top and U-shaped reactor shell, be respectively equipped with mutual corresponding sealing groove, in described sealing groove, be provided with sealing-ring.
As further improvement of the utility model, described U-shaped reactor shell and the large lid of reactor be bolted and U-shaped reactor shell and the large lid of reactor between be provided with vacuum rubber gasket.
As further improvement of the utility model, on described furnace body outer wall different positions, be respectively equipped with 7 thermopairs.
As further improvement of the utility model, described U-shaped reactor shell inner bottom part is provided with sieve plate.
The relative prior art of the utility model has following beneficial effect:
1, the utility model adopts aluminum silicate fiber prefabricated section and calcium silicate thermal insulation brick to make furnace lining high insulating effect, compare the stove of traditional employing insulating brick as liner, it has that furnace lining specific heat is little, heat absorption less, the feature such as quick heating, good heat insulating, furnace bottom heat insulation brick adopts high-alumina lightening insulating brick, and under hot environment, the soft intensity of ultimate compression strength and lotus improves.Compare common aluminum silicate fiber piece, aluminum silicate fiber prefabricated section density is large, intensity is high, adopt this composite structure, both reduced scattering and disappearing of furnace temperature heat, ensure again the intensity of body of heater, guaranteed that terminal stud, thermopair, air port are not sunk by furnace lining material and shorten the accuracy of combining also-steam stove life-span and thermometric.The utility model list stove production capacity has reached 11t, and power consumption is reduced to 4000kw.h/t.In addition, the utility model adopts blower fan forced ventilation, according to conversion zone reaction liquid fluctuating, the two wind inlet channels in top, lower air-out air channel are set, to the heat radiation of reaction zone in reactor, compare traditional effect of natural ventilation very good, not only make more than reducing material speed reaches 500kg/h, to have shortened reduction cycle, and solved large type of furnace titanium sponge and easily produce the problem of hard core.
2, the U-shaped reactor shell row of the utility model magnesium chloride pipe adopts homogeneous tube structure, has solved traditional row's magnesium chloride pipe weld seam problem easy to crack.
3, the utility model adopts the anti-oxidation iron sheet corundum the brim of a hat and the Tao Ding of special construction, effectively resistive band and the brim of a hat are combined, play the problem that prevents iron scale overlap joint reactor, reduce the fault of also-steam stove, can realize working continuously of also-steam stove, after realizing forehearth and finishing, without blowing out cooling maintenance, directly reactor can be entered to hot stove and produce, improve the utilization ratio of waste heat.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model;
Fig. 2 is the structural representation of the utility model terminal stud;
Fig. 3 is the local enlarged diagram of A portion in Fig. 1.
Reference numeral implication is as follows: 1, U-shaped reactor shell; 2, the large lid of reactor; 3, reactor vacuum-pumping tube; 4, filling tube; 5, heating tube; 6, internal heater; 7, external heat device; 8, sealing-ring; 9, vacuum rubber gasket; 10, body of heater; 11, aligning post; 12, blower fan; 13, blast pipe; 14, air inlet adjustment valve; 17, air intake band; 18, air-out band; 19, air outlet tube; 20, take out body of heater valve tube; 21, alumina silicate fiber felt; 22, calcium silicate thermal insulation brick; 23, aluminum silicate fiber prefabricated section; 24, resistive band; 25, Tao Ding; 26, the anti-oxidation iron sheet corundum the brim of a hat; 27, nickel network rod; 28, terminal stud; 29, thermopair; 30, row's magnesium chloride pipe; 31, sieve plate; 32, high-alumina lightening insulating brick.
Embodiment
Below in conjunction with accompanying drawing, the utility model is described in further detail:
As Figure 1-3, a kind of 11t that is applicable to titanium sponge production combines also-steam stove, comprise body of heater 10 and be vertically arranged on the U-shaped reactor shell 1 in body of heater 10, the flange of U-shaped reactor shell 1 is arranged on body of heater 10 tops, on the flange of body of heater 10 tops and U-shaped reactor shell 1, be respectively equipped with mutual corresponding sealing groove, in sealing groove, be provided with sealing-ring 8, in U-shaped reactor shell 1, be provided with the row's magnesium chloride pipe 30 into homogeneous tube structure, U-shaped reactor shell 1 inner bottom part is provided with sieve plate 31, U-shaped reactor shell 1 is provided with the large lid 2 of reactor, the large lid 2 of U-shaped reactor shell 1 and reactor be bolted and U-shaped reactor shell 1 and the large lid 2 of reactor between be provided with vacuum rubber gasket 9, the large lid 2 of reactor is provided with filling tube 4, reactor vacuum-pumping tube 3, heating tube 5, internal heater 6 and external heat device 7, the length-to-diameter of U-shaped reactor shell 1 is 2.48, the length-to-diameter of body of heater 10 is 2.16.
On body of heater 10 inwalls, be bonded with alumina silicate fiber felt 21, be close to alumina silicate fiber felt 21 and build calcium silicate thermal insulation brick 22 from top to bottom by laying bricks or stones, be close to calcium silicate thermal insulation brick 22 and build aluminum silicate fiber prefabricated section 23 from top to bottom by laying bricks or stones, Tao Ding 25 by hollow on aluminum silicate fiber prefabricated section 23 is fixed with 7 groups of resistive bands 24 from top to bottom through the fixed orifices of the anti-oxidation iron sheet corundum the brim of a hat 26, resistive band 24 welds with external terminal stud 28, in the Tao Ding 25 of hollow, be provided with the nickel network rod 27 of 3-4mm, if Tao Ding 25 ruptures in producing, can guarantee that Tao Ding 25 still can support resistive band 24, reduce electrical accident, fixed resistor band 24 in this way, reliability is high, simultaneously again to playing of resistive band 24 phenomenon of anti-oxidation iron sheet overlap joint.Body of heater 10 bottoms are followed successively by alumina silicate fiber felt 21 and high-alumina lightening insulating brick 32 from bottom to top, high-alumina lightening insulating brick 32 is connected with the aluminum silicate fiber prefabricated section 23 on body of heater 10 inwalls, body of heater 10 inwalls are provided with 2 layers of aligning post 11, every layer of aligning post 11 is 8 and is distributed on body of heater 10 inwall one week, hang in the location of burner hearth for U-shaped reactor shell 1, avoid breaking furnace lining and electrical heating element.
On body of heater 10 outer wall different positionss, be respectively equipped with 7 thermopairs 29.Body of heater 10 outer walls are provided with takes out body of heater valve tube 20, air intake band 17 and air-out band 18, air-out band 18 is positioned at the below of air intake band 17, on air intake band 17 and air-out band 18, be respectively equipped with blast pipe 13 and air outlet tube 19, blast pipe 13 is connected with blower fan 12, blast pipe 13 is to be respectively equipped with air inlet adjustment valve 14 on two and each blast pipe 13, air outlet tube 19 is one, the inner corresponding air intake band 17 of body of heater 10 is provided with the air port identical with burner hearth with the position of air-out band 18, these air ports are distributed on burner hearth inside, the homogeneity of principal security air intake and the homogeneity of air-out, in reduction process according to the liquid level of U-shaped reactor shell 1 interior reaction mass, open air inlet adjustment valve 14 corresponding on blast pipe 13, cold wind is blasted air intake band 17 by blower fan 12, by the air port between air intake band 17 and burner hearth, cold wind is shunted, evenly entering burner hearth dispels the heat to reactor reaction region, guarantee that the heat in reactor obtains sufficient heat exchange, be beneficial to the carrying out of reaction and the improvement of titanium sponge structure.

Claims (10)

1. a 11t who is applicable to titanium sponge production combines also-steam stove, comprise body of heater (10) and be vertically arranged on the U-shaped reactor shell (1) in body of heater (10), the flange of described U-shaped reactor shell (1) is arranged on body of heater (10) top, the row's of being provided with magnesium chloride pipe (30) in described U-shaped reactor shell (1), described U-shaped reactor shell (1) is provided with the large lid of reactor (2), the large lid of described reactor (2) is provided with filling tube (4), reactor vacuum-pumping tube (3), heating tube (5), internal heater (6) and external heat device (7), it is characterized in that: the length-to-diameter of described U-shaped reactor shell (1) is 2.48, the length-to-diameter of described body of heater (10) is 2.16, on described body of heater (10) inwall, be bonded with alumina silicate fiber felt (21), be close to alumina silicate fiber felt (21) and build calcium silicate thermal insulation brick (22) from top to bottom by laying bricks or stones, be close to calcium silicate thermal insulation brick (22) and build aluminum silicate fiber prefabricated section (23) from top to bottom by laying bricks or stones, on described aluminum silicate fiber prefabricated section (23), be provided with resistive band (24) from top to bottom, described body of heater (10) bottom is followed successively by alumina silicate fiber felt (21) and high-alumina lightening insulating brick (32) from bottom to top, described high-alumina lightening insulating brick (32) is connected with the aluminum silicate fiber prefabricated section (23) on body of heater (10) inwall, described body of heater (10) outer wall is provided with takes out body of heater valve tube (20), air intake band (17) and air-out band (18), described air-out band (18) is positioned at the below of air intake band (17), on described air intake band (17) and air-out band (18), be respectively equipped with blast pipe (13) and air outlet tube (19), described blast pipe (13) is connected with blower fan (12), the position of the inner corresponding air intake band of described body of heater (10) (17) and air-out band (18) is provided with air port.
2. a kind of 11t that is applicable to titanium sponge production according to claim 1 combines also-steam stove, it is characterized in that: described row's magnesium chloride pipe (30) is homogeneous tube structure.
3. a kind of 11t that is applicable to titanium sponge production according to claim 1 combines also-steam stove, it is characterized in that: the upper Tao Ding (25) by hollow of described aluminum silicate fiber prefabricated section (23) is fixed with 7 groups of resistive bands (24) from top to bottom through the fixed orifices of the anti-oxidation iron sheet corundum the brim of a hat (26), described resistive band (24) and external terminal stud (28) welding, be provided with nickel network rod (27) in the Tao Ding (25) of described hollow.
4. a kind of combine also-steam stove of 11t that titanium sponge is produced that is applicable to according to claim 1, is characterized in that: described blast pipe (13) is to be respectively equipped with air inlet adjustment valve (14) on two and each blast pipe (13).
5. a kind of 11t that is applicable to titanium sponge production according to claim 1 combines also-steam stove, it is characterized in that: described air outlet tube (19) is one.
6. a kind of 11t that is applicable to titanium sponge production according to claim 1 combines also-steam stove, it is characterized in that: described body of heater (10) inwall is provided with 2 layers of aligning post (11), and every layer of aligning post (11) is 8 and is distributed on body of heater (10) inwall one week.
7. a kind of 11t that is applicable to titanium sponge production according to claim 1 combines also-steam stove, it is characterized in that: on the flange of described body of heater (10) top and U-shaped reactor shell (1), be respectively equipped with mutual corresponding sealing groove, in described sealing groove, be provided with sealing-ring (8).
8. a kind of combine also-steam stove of 11t that titanium sponge is produced that is applicable to according to claim 1, is characterized in that: described U-shaped reactor shell (1) and the large lid of reactor (2) be bolted and U-shaped reactor shell (1) and the large lid of reactor (2) between be provided with vacuum rubber gasket (9).
9. a kind of 11t that is applicable to titanium sponge production according to claim 1 combines also-steam stove, it is characterized in that: on described body of heater (10) outer wall different positions, be respectively equipped with 7 thermopairs (29).
10. a kind of 11t that is applicable to titanium sponge production according to claim 1 combines also-steam stove, it is characterized in that: described U-shaped reactor shell (1) inner bottom part is provided with sieve plate (31).
CN201420089238.1U 2014-02-28 2014-02-28 Combined 11t reduction-evaporation furnace suitable for producing titanium sponge Expired - Lifetime CN203715704U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103820655A (en) * 2014-02-28 2014-05-28 金川集团股份有限公司 11t combined reduction-distilling furnace for titanium sponge production
CN104357659A (en) * 2014-12-09 2015-02-18 遵义钛业股份有限公司 Vacuum ladle for adding magnesium for reduction in production of titanium sponge and discharging magnesium chloride by distillation

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103820655A (en) * 2014-02-28 2014-05-28 金川集团股份有限公司 11t combined reduction-distilling furnace for titanium sponge production
CN104357659A (en) * 2014-12-09 2015-02-18 遵义钛业股份有限公司 Vacuum ladle for adding magnesium for reduction in production of titanium sponge and discharging magnesium chloride by distillation

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