CN203683091U - Loading and unloading storing system of fuming sulphuric acid - Google Patents

Loading and unloading storing system of fuming sulphuric acid Download PDF

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Publication number
CN203683091U
CN203683091U CN201320764372.2U CN201320764372U CN203683091U CN 203683091 U CN203683091 U CN 203683091U CN 201320764372 U CN201320764372 U CN 201320764372U CN 203683091 U CN203683091 U CN 203683091U
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CN
China
Prior art keywords
oleum
liquid seal
storage tank
pipe
acid
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201320764372.2U
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Chinese (zh)
Inventor
郭彦召
李燕平
李幼民
连保香
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ANYANG SHUANGHUAN AUXILIARIES Co Ltd
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ANYANG SHUANGHUAN AUXILIARIES Co Ltd
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Priority to CN201320764372.2U priority Critical patent/CN203683091U/en
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Publication of CN203683091U publication Critical patent/CN203683091U/en
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Abstract

The utility model discloses a loading and loading system of fuming sulphuric acid. The loading and unloading system comprises a fuming sulphuric acid storing tank, an absorbing liquid storing tank, a liquid seal tank, an acid discharging pipe, an exhaust pipe, an emptying pipeline and valves. The loading and unloading system is characterized in that one end of the acid discharging pipe is connected to the fuming sulphuric acid storing tank, the other end of the acid discharging pipe is connected to the valve of an acid discharging hole, one end of the exhaust pipe is connected to the fuming sulphuric acid storing tank, the other end of the exhaust pipe is connected with the valve of the emptying pipeline, the exhaust pipe is connected with the top end of the liquid seal tank, two ends of the liquid discharging pipe are respectively connected to the valve at the bottom of the liquid seal tank and an overflow pipe, one end of the overflow pipe is connected to an overflow hole in the side wall of the liquid seal tank, and the other end of the overflow pipe is connected to the absorbing liquid storing tank. According to the whole set of system, sulfur trioxide can not overflow when the fuming sulphuric acid is loaded or unloaded, thus the utilization rate of the fuming sulphuric acid is increased, and the environment protection is facilitated.

Description

A kind of handling stocking system of oleum
Technical field
The utility model relates to a kind of handling and field of storage of sulfuric acid, and specifically, the utility model relates to a kind of handling stocking system of oleum.
Background technology
Oleum is the sulfuric acid that concentration is very high, and when practical application, oleum usually relates to accumulating problem, and oleum highly volatile goes out sulphur trioxide, and sulphur trioxide is the material that human body is all harmful to, harm staff health.In open system, have overflowing of a large amount of sulphur trioxides, the one, reduce the service efficiency of raw material oleum, cause waste, the 2nd, overflow gas contamination environment, increase treating tail gas cost.
Summary of the invention
Technical problem to be solved in the utility model is to provide a kind of handling stocking system of oleum simple in structure.
In order to solve the problems of the technologies described above, the technical scheme that the utility model adopts is: a kind of handling stocking system of oleum, comprise oleum storage tank, absorption liquid storage tank, liquid seal can, unload acid tube, vapor pipe, exhausting pipeline and valve, described one end of unloading acid tube is connected on oleum storage tank, the other end is connected on the valve that unloads acid mouth, one end of described vapor pipe is connected on oleum hold-up vessel, and the other end is connected on the valve of exhausting pipeline; Described vapor pipe is connected with the top of described liquid seal can, the two ends of liquid discharge pipe are connected on the valve bottom described liquid seal can and on upflow tube, one end of described upflow tube is connected on the overflow port of liquid seal can sidewall, the other end is connected on absorption liquid storage tank, on vapor pipe on described liquid seal can and oleum storage tank, vapor pipe links together, in described liquid seal can, be provided with blow-down pipe, blow-down pipe is vertically located at liquid seal can middle part.
Described liquid seal can sidewall is provided with acid-filling mouth.
Described liquid seal can, for two-layer up and down, connects by blow-down pipe between levels.
Described overflow port is located between blow-down pipe and liquid seal can bottom.
The bottom of described absorption liquid storage tank is also provided with acid solution drain tube, and acid solution drain tube is provided with valve.
Described oleum storage tank is provided with pressure monitoring device, level monitoring device and device for detecting temperature, and described absorption liquid storage tank is provided with level monitoring device and device for detecting temperature.
Adopt the beneficial effect of above technical scheme to be: sulfuric acid loading and unloading system of the present utility model, in the situation that not affecting normal handling, liquid seal can fully absorbs the sulphur trioxide overflowing and has greatly reduced overflowing of sulphur trioxide in system, and what make oleum draws off environment safer more environmental protection.The utilization ratio that has improved oleum raw material, the sulphur trioxide overflowing is recycled after being converted into acid solution.On oleum storage tank and absorption liquid storage tank, be all provided with monitoring device can Real-Time Monitoring the every terms of information of storage pot liquid, facilitate staff's real-time monitored to improve the security of whole system.
Accompanying drawing explanation
Mark in the each accompanying drawing of this specification sheets expressed content and figure is made to brief description below:
Fig. 1 is structural representation of the present utility model;
Mark in above-mentioned figure is: 1, oleum storage tank; 2, absorption liquid storage tank; 3, liquid seal can; 4, charge pump; 5, absorption liquid drain tube; 6, unload acid mouthful; 7, exhausting pipeline; 8, vapor pipe; 9, blow-down pipe; 10, upflow tube; 11, liquid discharge pipe; 12, spout; 13, pressure monitoring device; 14, level monitoring device; 15, device for detecting temperature; 16, overflow port; 17, unload acid tube; 18, valve.
Embodiment
Contrast accompanying drawing below, by the description to embodiment, embodiment of the present utility model is described in further detail as effect and the principle of work etc. of the mutual alignment between the shape of related each member, structure, each several part and annexation, each several part: the loading and unloading system of this oleum comprises oleum storage tank 1, sulfuric acid storage tank 2, liquid seal can 3, unloads acid tube 17 and vapor pipe 8.As shown in Figure 1, oleum is stored in oleum storage tank 1, in the time that unloading oleum, needs dock with dress oleum tank car bottom discharge flange unloading acid mouth 6, exhausting pipeline 7 docks with tank car top emptying valve, open valve 18 simultaneously, unload the valve of acid mouthfuls 6 and exhausting pipeline 7, sulfur trioxide gas in oleum storage tank 1 passes into tank car by vapor pipe 8, and oleum passes into tank car by unloading acid tube 17.After unloading acid, close the valve unloading on acid mouthfuls 6 and exhausting pipeline 7, then disconnect and unloading being connected of acid mouthfuls 6 and exhausting pipeline 7 and tank car.Whole unload in sour process can be adjusted and unload sour speed and unload acid amount by being arranged on pressure monitoring device 13, level monitoring device 14 and device for detecting temperature 15 on oleum storage tank 1 in safety range.Exhausting pipeline 7 is provided with valve, valve opening be connected with tank car and allow unnecessary gas enter tank car while unloading acid.Valve closes when normal storage state on exhausting pipeline 7, the sulphur trioxide in oleum storage tank 1 enters liquid seal can 3 by vapor pipe 8 and is absorbed.The whole system in sour process of unloading, in air-tight state, does not have sulfur trioxide gas and overflows.On oleum storage tank 1, being also provided with charge pump 4 sends into oleum between reacting vehicle.
Normal storage state, valve 18 is opened, and oleum storage tank 1 is connected with liquid seal can 3, and oleum storage tank 1 is whole airtight.Described liquid seal can 3 is divided into two-layer up and down, between levels, connects by blow-down pipe 9, has certain pressure in oleum storage tank 1, and the size of pressure is determined by the degree of depth that in liquid seal can 3, blow-down pipe 9 inserts in absorption liquid.If may cause absorption liquid suck-back in liquid seal can 3 when the pressure in oleum storage tank 1 is lower simultaneously, because so a small amount of absorption liquid that liquid seal can 3 is upper and lower double-layer structure suck-back can only be back in the upper strata cavity of liquid seal can by blow-down pipe 9, because the liquid that exists of cavity 3 can not enter oleum storage tank 1 by suck-back.A small amount of sulphur trioxide is absorbed by the absorption liquid in liquid seal can 3, and whole system does not have sulphur trioxide and overflows.Due to the material properties of oleum itself, the situation that in oleum storage tank 1, pressure is too large or too little there will not be substantially.
When liquid seal can 3 changes liquid operation, valve-off 18, open the valve on liquid discharge pipe 11, absorption liquid in liquid seal can 3 is put into sulfuric acid storage tank 2, close the valve on liquid discharge pipe 11 after discharging absorption liquid, open spout 12, inject absorption liquid, control by overflow port 16 height that absorbs liquid level, absorption liquid unnecessary after reservoir quantity exceedes overflow port 16 can flow in absorption liquid storage tank 2 by upflow tube 10, and described liquid discharge pipe 11 is connected on described upflow tube 10.After fluid injection, close spout 12, open valve 18.Absorption liquid is stored in absorption liquid storage tank 2, emits by absorption liquid drain tube 5 when exceeding after certain liquid measure, carries out follow-up recycling or environmental protection treatment.
By reference to the accompanying drawings the present invention is exemplarily described above; obviously the utility model specific implementation is not subject to the restrictions described above; as long as adopted the improvement of the various unsubstantialities that method of the present utility model design and technical scheme carry out; or without improving, design of the present utility model and technical scheme are directly applied to other occasion, all within protection domain of the present utility model.

Claims (8)

1. the handling stocking system of an oleum, comprise oleum storage tank, absorption liquid storage tank, liquid seal can, unload acid tube, vapor pipe, exhausting pipeline and valve, it is characterized in that: described in unload acid tube one end be connected on oleum storage tank, the other end is connected on the valve that unloads acid mouth, one end of described vapor pipe is connected on oleum hold-up vessel, and the other end is connected on the valve of exhausting pipeline; Described vapor pipe is connected with the top of described liquid seal can, and the two ends of liquid discharge pipe are connected on the valve bottom described liquid seal can and on upflow tube, and one end of described upflow tube is connected on the overflow port of liquid seal can sidewall, and the other end is connected on absorption liquid storage tank.
2. the handling stocking system of oleum according to claim 1, is characterized in that: on the vapor pipe on described liquid seal can and oleum storage tank, vapor pipe links together.
3. the handling stocking system of oleum according to claim 1, is characterized in that: in described liquid seal can, be provided with blow-down pipe, blow-down pipe is vertically located at liquid seal can middle part.
4. the handling stocking system of oleum according to claim 3, is characterized in that: described liquid seal can, for two-layer up and down, connects by blow-down pipe between levels.
5. the handling stocking system of oleum according to claim 2, is characterized in that: described liquid seal can sidewall is provided with acid-filling mouth.
6. the handling stocking system of oleum according to claim 2, is characterized in that: described overflow port is located between blow-down pipe and liquid seal can bottom.
7. the handling stocking system of oleum according to claim 1, is characterized in that: the bottom of described absorption liquid storage tank is also provided with acid solution drain tube, acid solution drain tube is provided with valve.
8. the handling stocking system of oleum according to claim 1, it is characterized in that: described oleum storage tank is provided with pressure monitoring device, level monitoring device and device for detecting temperature, described absorption liquid storage tank is provided with level monitoring device and device for detecting temperature.
CN201320764372.2U 2013-11-28 2013-11-28 Loading and unloading storing system of fuming sulphuric acid Expired - Fee Related CN203683091U (en)

Priority Applications (1)

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CN201320764372.2U CN203683091U (en) 2013-11-28 2013-11-28 Loading and unloading storing system of fuming sulphuric acid

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Application Number Priority Date Filing Date Title
CN201320764372.2U CN203683091U (en) 2013-11-28 2013-11-28 Loading and unloading storing system of fuming sulphuric acid

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105460877A (en) * 2014-08-31 2016-04-06 天津渤大硫酸工业有限公司 Totally-sealed fuming sulfuric acid storing and filling system
CN116101981A (en) * 2023-02-20 2023-05-12 新疆紫金有色金属有限公司 Method for producing and manufacturing food-grade sulfuric acid and concentrated sulfuric acid impurity removing device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105460877A (en) * 2014-08-31 2016-04-06 天津渤大硫酸工业有限公司 Totally-sealed fuming sulfuric acid storing and filling system
CN116101981A (en) * 2023-02-20 2023-05-12 新疆紫金有色金属有限公司 Method for producing and manufacturing food-grade sulfuric acid and concentrated sulfuric acid impurity removing device

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140702

Termination date: 20211128

CF01 Termination of patent right due to non-payment of annual fee