CN203625031U - Combined steam-type graphite hydrogen chloride synthesis furnace - Google Patents
Combined steam-type graphite hydrogen chloride synthesis furnace Download PDFInfo
- Publication number
- CN203625031U CN203625031U CN201320738045.XU CN201320738045U CN203625031U CN 203625031 U CN203625031 U CN 203625031U CN 201320738045 U CN201320738045 U CN 201320738045U CN 203625031 U CN203625031 U CN 203625031U
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- Prior art keywords
- furnace tube
- graphite
- furnace
- chassis
- assembly
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- Expired - Lifetime
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 55
- 229910002804 graphite Inorganic materials 0.000 title claims abstract description 55
- 239000010439 graphite Substances 0.000 title claims abstract description 55
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 230000015572 biosynthetic process Effects 0.000 title claims abstract description 31
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 31
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 title abstract description 10
- 229910000041 hydrogen chloride Inorganic materials 0.000 title abstract description 9
- 238000001816 cooling Methods 0.000 claims abstract description 57
- 239000011229 interlayer Substances 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 78
- 239000002253 acid Substances 0.000 claims description 11
- 239000001257 hydrogen Substances 0.000 claims description 11
- 229910052739 hydrogen Inorganic materials 0.000 claims description 11
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 7
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 6
- 229910052801 chlorine Inorganic materials 0.000 claims description 6
- 239000000460 chlorine Substances 0.000 claims description 6
- 239000010865 sewage Substances 0.000 claims description 6
- 238000003466 welding Methods 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 5
- 230000001413 cellular effect Effects 0.000 claims description 4
- 238000011067 equilibration Methods 0.000 claims description 3
- 230000005855 radiation Effects 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 238000013022 venting Methods 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 3
- 238000005660 chlorination reaction Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 230000002194 synthesizing effect Effects 0.000 description 2
- 239000000110 cooling liquid Substances 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
Abstract
The utility model provides a combined steam-type graphite hydrogen chloride synthesis furnace, comprising a synthesis furnace I, a cooling box II and a graphite cooler III, wherein a lamp holder component, a synthesis section component and a synthesis furnace end socket component are arranged on the synthesis furnace I; the combined steam-type graphite hydrogen chloride synthesis furnace comprises an inner furnace tube I, an outer furnace tube II and an upper end socket; the outer furnace tube I, the outer furnace tube II and the upper end socket are arranged outside the inner furnace tube; a clearance interlayer is formed among the inner furnace tube, the outer furnace tube I and the outer furnace tube II; a cooling box section component is arranged on the cooling box II and comprises a hydrochloric acid (HCL) pipeline cooling box arranged outside and an HCL outlet pipeline arranged inside; and a cooler top component and a honeycomb graphite heat exchange cooling section are arranged on the graphite cooler III. By adopting the combined steam-type graphite hydrogen chloride synthesis furnace disclosed by the utility model, the heat transfer efficiency is effectively improved and the heat energy is burnt to obtain full energy conversion.
Description
Technical field
The utility model relates to a kind of graphite equipment synthetic furnace, relates in particular to a kind of combined steam formula graphite synthesis furnace for hydrochloride.
Background technology
The production of technical hydrochloric acid mainly adopts chlorine and the synthesizing chlorinated hydrogen of combustion of hydrogen, again by synthetic higher than 1500 ℃ of high temperature in synthetic furnace, in this process, need to synthesize by igniting, then cooling, hydrogen chloride gas after cooling absorbs and generates synthetic hydrochloric acid with diluted acid water again, comprise: first synthetic, rear cooling, finally absorb basic three process.
Conventional production adopts respectively at least three or multiple devices to complete respectively above-mentioned basic three process, its equipment, and human input is many, and production cost is higher, and production efficiency is low, wastage of material is more serious.
At present comparatively advanced flow process is: by above-mentioned synthetic, cooling, absorb basic three process and be synthesized in two equipment and complete, adopt two hydrochloric acid synthetic furnaces of minimal equipment.Synthesizing of general hydrochloric acid.In the process of burning generation hydrogenchloride, produce larger heat, and these heats are not utilized preferably, to cause the waste of the energy.
At present, more advanced technology, is to adopt on the basis of hydrochloric acid synthetic furnace, the combustion heat of hydrogenchloride is passed to circulating hot water, to increase the heat content of circulating hot water, realizing the recycling of heat, generates byproduct steam or hot water, to make full use of the energy.
The byproduct steam of prior art or the hydrochloric acid synthetic furnace of hot water, the inside and outside wall of its synthetic furnace stove cylinder is light wall shape conventionally, or more shallow enhancement of heat transfer groove, wall internal drilling etc., its heat transfer surface area is relatively little, thereby has limited the effect of conducting heat.
In addition, in order to improve heat-transfer effect, between inside and outside stove cylinder, interlayer arranges spiral deflector and division plate, for flow direction and the raising flow velocity of Directed cooling liquid or heating fluid.The traverse baffle of the byproduct steam of prior art or the hydrochloric acid synthetic furnace of hot water is a kind of single tabular or ring made from metal, plastics or graphite.Because metal, plastics and graphite are rigid material, and between traverse baffle and outer furnace tube, leave space, therefore, water coolant or heating fluid just easily leak from space, cause the obstruction of passage or the inequality of conducting heat, and have affected heat-transfer effect.
Utility model content
It is a kind of rational in infrastructure that the purpose of this utility model is to provide, and effectively improves a kind of combined steam formula graphite synthesis furnace for hydrochloride of heat transfer efficiency.
To achieve these goals, a kind of combined steam formula graphite synthesis furnace for hydrochloride that the utility model provides, synthetic furnace I, cooling tank II and graphite cooler III;
Synthetic furnace I is provided with bulb socket assembly, synthesis stage assembly, synthetic furnace closing end component; Comprise interior stove cylinder and be located at outer furnace tube I, outer furnace tube II, the upper cover outside interior stove cylinder, the gap interlayer forming between interior stove cylinder and outer furnace tube I, outer furnace tube II, interlayer carries out heat conduction, heat radiation, cooling for water;
Cooling tank II is provided with cooling tank section assembly, comprises the HCL tube-cooled case of outer setting, the HCL outlet conduit that inside is provided with, and HCL outlet conduit is provided with pressure tap and temperature-measuring port, and channel bend arranges pipeline movable joint with HCL outlet conduit and is connected;
Graphite cooler III is provided with water cooler top assembly and honeycomb graphite heat exchange cooling section; Water cooler top assembly external structure is provided with casing water tank, and there is the water cooler upper cover plate being connected with channel bend inside; The structure of honeycomb graphite heat exchange cooling section is: external structure is provided with the cooler cylinder being connected with casing water tank, is provided with hanging support on cooler cylinder, and bottom is provided with heat transfer block lower cover; Internal structure is disposed with the water cooler upper cover being connected with water cooler upper cover plate from top to bottom, water cooler heat transfer block I, water cooler heat transfer block II.
Reasonable, bulb socket assembly comprises: bulb socket, manhole differential, manhole connecting pipe, lamp holder, chassis I, chassis II, differential.Be provided with the hydrogen inlet on bulb socket, in the II of chassis, be provided with acid discharge mouth, sewage draining exit.
Reasonable, synthesis stage assembly comprises: described interior stove cylinder is provided with and connects pad and be connected with chassis I, described lighting-up tuyere, the mouth of showing on trial, venting, HCL export by solid welding joint in accordance with regulations angle be arranged on interior furnace tube outer wall.Between described outer furnace tube I and outer furnace tube II, being provided with gasket seal connects.The inwall of the inwall of described outer furnace tube I and outer furnace tube II is provided with interlayer.Described hot water injects by the water-in and the balancing pipeline lower interface that are arranged on outside outer furnace tube I.
Reasonable, synthetic furnace closing end component comprises: upper cover and liquidometer mouth, population, pressure tap, temperature-measuring port, hot water outlet or vapor outlet port and the equilibration tube water outlet on its outer wall be set.Described balancing pipeline carries out the thermal exchange in furnace sandwich.
Reasonablely be, cooling tank section assembly is outside to be connected with outer furnace tube II and cylindrical shell tank outer wall by HCL tube-cooled case, the inner solid welding joint of HCL outlet conduit and interior stove cylinder top that passes through is connected, and is connected in honeycomb graphite heat exchange block with described honeycomb graphite heat exchange cooling section top water cooler upper cover plate.
Reasonable, water cooler top assembly and inner HCL outlet conduit and water cooler upper cover plate are provided with cavity, cooling for injected water.
Reasonable, inner honeycomb graphite cooling and absorbing heat exchanging segment assembly, is characterized in that, comprising: described molectron is provided with from bottom to up pad and connects water cooler heat transfer block I, II.Described heat transfer block I, II are provided with nest bee-hole in length and breadth.Described nest bee-hole is for cooling HCL and cooling heat conduction.
Reasonable, outer furnace tube I assembly below is provided with differential and chassis I and is arranged on the upper side of chassis II.In described stove, chassis I is arranged on inner barrel below.Described manhole plate is arranged on manhole differential downside by bolt.Described manhole differential is bolted at chassis II downside.Described chassis II is provided with acid discharge mouth and the sewage draining exit of mouth down.Described manhole connecting pipe setting is by chassis I, chassis II and manhole differential inner chamber.Described bulb socket is arranged in the inner chamber of manhole connecting pipe and manhole differential.In described bulb socket, lamp holder is set, bulb socket is outer is provided with hydrogen inlet, chlorine inlet by angle.
Reasonable, between interior stove cylinder bottom and chassis I, be provided with pad, described interior stove cylinder top is provided with synthetic upper cover plate.Described outer furnace tube I bottom is provided with o type circle and connects by spring rod assembly.Described upper cover is connected with outer furnace tube II by bolt assembly.Described water cooler lower cover is provided with long draw assembly and is connected with cooler cylinder.
Reasonable, balancing pipeline is connected to the hot water inlet and the upper cover outer wall top that below outer furnace tube I outer wall, are provided with and is provided with on hot water outlet.
An innovative point as this utility model is, is provided with the spiral deflector that adopts stainless steel to make in stove inner/outer tube interlayer body, and described hot water is helicoidal flow by spiral stream guidance plate structure.
Another innovative point as this utility model is, the manufacture of described interior stove cylinder material employing impermeable graphite, and heat transfer block adopts the cellular through hole of vertical and horizontal direction, and outer furnace tube adopts stainless material to make.
A kind of combined integral graphite synthesis furnace for hydrochloride that the utility model provides, hydrogen and chlorine enter from inlet mouth, by lighting near bulb socket lighting-up tuyere, the synthetic hydrogen chloride gas that generates in synthesis stage; High-temp chlorination hydrogen enters cooling tank section assembly, by the water cooling in interlayer, enter honeycomb graphite cooling and absorbing heat exchanging segment assembly, after a part is cooling, flow in heat transfer block lower cover chamber by the cellular through hole of vertical direction in honeycomb graphite, export and condensation acid outlet outflow by HCL, tail gas is discharged from tail gas outlet.
A kind of combined integral graphite synthesis furnace for hydrochloride that the utility model provides, rational in infrastructure, effectively improve heat transfer efficiency.
Accompanying drawing explanation
The structural representation of a kind of combined steam formula of Fig. 1 the utility model graphite synthesis furnace for hydrochloride.
Embodiment
Below in conjunction with accompanying drawing 1 and specific embodiment, the utility model is described in further detail to explanation.
As shown in Figure 1, a kind of combined steam formula graphite synthesis furnace for hydrochloride of the present utility model, comprises: synthetic furnace I, cooling tank II and graphite cooler III from bottom to top successively.
Synthetic furnace I is provided with bulb socket assembly A, synthesis stage assembly B, synthetic furnace closing end component C; Comprise interior stove cylinder and be located at outer furnace tube I, outer furnace tube II, the upper cover 20 outside interior stove cylinder, the gap interlayer forming between interior stove cylinder and outer furnace tube I, outer furnace tube II, interlayer carries out heat conduction, heat radiation, cooling for water;
Cooling tank II is provided with cooling tank section assembly D; comprise the HCL tube-cooled case 39 of outer setting; the HCL outlet conduit 22 that inside is provided with, HCL outlet conduit 22 is provided with pressure tap 23 and temperature-measuring port 24, and channel bend 26 arranges pipeline movable joint 25 with HCL outlet conduit 22 and is connected;
Graphite cooler III is provided with water cooler top assembly E and honeycomb graphite heat exchange cooling section F; Water cooler top assembly E external structure is provided with casing water tank 27, and there is the water cooler upper cover plate 28 being connected with channel bend 26 inside; The structure of honeycomb graphite heat exchange cooling section F is: external structure is provided with the cooler cylinder 30 being connected with casing water tank 27, is provided with hanging support 31 on cooler cylinder 30, and bottom is provided with heat transfer block lower cover 35; Internal structure is disposed with the water cooler upper cover 29 being connected with water cooler upper cover plate 28 from top to bottom, water cooler heat transfer block I 33, water cooler heat transfer block II 34.
Bulb socket assembly A comprises: bulb socket 1, manhole differential 2, manhole connecting pipe 3, lamp holder 4, chassis I 5, chassis II 6, differential 7; Be provided with hydrogen inlet a1, a2 on bulb socket, in chassis II 6, be provided with acid discharge mouth c, sewage draining exit d.Synthesis stage assembly B comprises: interior stove cylinder 13 is provided with and connects pad 9 and be connected with chassis I 5, lighting-up tuyere e, show on trial a mouthful k1, k2, venting j, f, HCL export i by solid welding joint A5 in accordance with regulations angle be arranged on interior stove cylinder 13 outer walls.Between outer furnace tube I 14 and outer furnace tube II 18, being provided with pad 15 is tightly connected.The inwall of the inwall of outer furnace tube I 14 and outer furnace tube II 18 is provided with interlayer; Hot water injects by the water-in L and the balancing pipeline lower interface that are arranged on outside outer furnace tube I 14.Synthetic furnace closing end component C comprises: upper cover 20 and liquidometer mouth m1, m2, population T, pressure tap R, temperature-measuring port s, hot water outlet or vapor outlet port h and the equilibration tube water outlet on its outer wall is set; The thermal exchange that balancing pipeline 21 carries out in furnace sandwich.Cooling tank section assembly D is outside to be connected with outer furnace tube II 18 and cylindrical shell water tank 27 outer walls by HCL tube-cooled case 39, inside is connected by HCL outlet conduit 22 and the solid welding joint A5 in interior stove cylinder 13 tops, is connected in honeycomb graphite heat exchange block I, II with honeycomb graphite heat exchange cooling section F top water cooler upper cover plate 28.Water cooler top assembly E and inner HCL outlet conduit 22 and water cooler upper cover plate 28 are provided with cavity, cooling for injected water.Inner honeycomb graphite cooling and absorbing heat exchanging segment assembly F, is characterized in that, comprising: molectron is provided with from bottom to up pad 32 and connects water cooler heat transfer block I, II; Heat transfer block I, II are provided with nest bee-hole in length and breadth; Nest bee-hole is for cooling HCL and cooling heat conduction.
Outer furnace tube I assembly 14 belows are provided with differential 7 and chassis I 5 and are arranged on the upper side of chassis II 6; In stove, chassis I 5 is arranged on inner barrel 13 belows; Manhole plate A8 is arranged on manhole differential 2 downsides by bolt A9.Manhole differential 2 is connected to chassis II 6 downsides by bolt A7; Chassis II 6 is provided with acid discharge mouth c and the sewage draining exit d of mouth down; Manhole connecting pipe 3 arranges by chassis I 5, chassis II 6 and manhole differential 2 inner chambers; Bulb socket is arranged in the inner chamber of manhole connecting pipe 3 and manhole differential 2.Lamp holder is set in bulb socket, and bulb socket is outer is provided with hydrogen inlet a1-2, chlorine inlet b by angle.
Between interior stove cylinder 13 bottoms and chassis I 5, be provided with pad 9, interior stove cylinder 13 tops are provided with synthetic upper cover plate A6; Outer furnace tube I 14 bottoms are provided with o type circle 8 and connect by spring rod assembly 10; Upper cover 20 is connected with outer furnace tube II 18 by bolt assembly; Water cooler lower cover 37 is provided with long draw assembly 36 and is connected with cooler cylinder 30.
Balancing pipeline 21 is connected to the hot water inlet and the upper cover 20 outer walls tops that below outer furnace tube I outer wall, are provided with and is provided with on hot water outlet; In stove inner/outer tube interlayer body, be provided with the spiral deflector A4 that adopts stainless steel to make, hot water is helicoidal flow by spiral deflector A4 structure.
Interior stove cylinder material adopts impermeable graphite manufacture, and heat transfer block adopts the cellular through hole of vertical and horizontal direction, and outer furnace tube adopts stainless material to make.
Principle of work:
Hydrogen and chlorine enter from raw material inlet mouth a1-2 and b respectively, light the synthetic hydrogen chloride gas that generates in synthesis stage B by bulb socket assembly (A) and lighting-up tuyere e burning; Upper cover (20) the interlayer inner chamber water-cooled heat exchange that high-temp chlorination hydrogen first passes through in synthetic furnace closing end component C enters cooling tank section assembly (D) and water cooler top assembly E, after secondary heat exchange is cooling, enter heat exchange and honeycomb graphite cooling down absorption segment E, in heat exchange and honeycomb graphite cooling down absorption segment E, a part, by the cooling rear further cooling of honeycomb graphitic cooling block, cools and isolates partially liq from gas-liquid; Flow into the 35 acid mouth a outputs of heat transfer block lower cover from honeycomb graphite upright opening, another part HCL gas continues under the effect of the interlayer water coolant of honeycomb graphite cooling down absorption segment E, and absorption liquid acid concentration is enhanced; The absorption liquid that has been enhanced concentration continues to flow downward, and enters gas-liquid separation section, and flows out from the 35 condensation acid outlets of heat transfer block lower cover, and all the other not treatable HCL tail gas are discharged from tail gas outlet.
In sum, a kind of combined steam formula graphite synthesis furnace for hydrochloride of the present utility model, effectively improves heat transfer efficiency, and combustion heat energy has been obtained to sufficient energy transformation, saves equipment cost.
Claims (4)
1. a combined steam formula graphite synthesis furnace for hydrochloride, is characterized in that, comprising: synthetic furnace I, cooling tank II and graphite cooler III;
Described synthetic furnace I is provided with bulb socket assembly (A), synthesis stage assembly (B), synthetic furnace closing end component (C); Comprise interior stove cylinder and be located at outer furnace tube I, outer furnace tube II, the upper cover (20) outside interior stove cylinder, the gap interlayer forming between described interior stove cylinder and described outer furnace tube I, outer furnace tube II, described interlayer carries out heat conduction, heat radiation, cooling for water;
Described cooling tank II is provided with cooling tank section assembly (D); comprise the HCL tube-cooled case (39) of outer setting; the HCL outlet conduit (22) that inside is provided with; described HCL outlet conduit (22) is provided with pressure tap (23) and temperature-measuring port (24), and channel bend (26) arranges pipeline movable joint (25) with HCL outlet conduit (22) and is connected;
Described graphite cooler III is provided with water cooler top assembly (E) and honeycomb graphite heat exchange cooling section (F); Described water cooler top assembly (E) external structure is provided with casing water tank (27), and there is the water cooler upper cover plate (28) being connected with channel bend (26) inside; The structure of described honeycomb graphite heat exchange cooling section (F) is: external structure is provided with the cooler cylinder (30) being connected with casing water tank (27), on described cooler cylinder (30), be provided with hanging support (31), described bottom is provided with heat transfer block lower cover (35); Internal structure is disposed with the water cooler upper cover (29) being connected with water cooler upper cover plate (28) from top to bottom, water cooler heat transfer block I (33), water cooler heat transfer block II (34).
2. a kind of combined steam formula graphite synthesis furnace for hydrochloride according to claim 1, it is characterized in that, described bulb socket assembly (A) comprising: bulb socket (1), manhole differential (2), manhole connecting pipe (3), lamp holder (4), chassis I (5), chassis II (6), differential (7); The described hydrogen inlet (a1, a2) being provided with on bulb socket, is provided with acid discharge mouth (c), sewage draining exit (d) in described chassis II (6);
Described synthesis stage assembly (B) comprising: described interior stove cylinder (13) is provided with and connects pad (9) and be connected with chassis I (5), described lighting-up tuyere (e), show on trial mouthful (k1, k2), a venting (j, f), HCL export (i) by consolidate welding joint (A5) in accordance with regulations angle be arranged on interior stove cylinder (13) outer wall; Between described outer furnace tube I (14) and outer furnace tube II (18), being provided with pad (15) is tightly connected.The inwall of the inwall of described outer furnace tube I (14) and outer furnace tube II (18) is provided with interlayer; Described hot water injects by being arranged on the outer water-in (L) of outer furnace tube I (14) and balancing pipeline lower interface;
Described synthetic furnace closing end component (C) comprising: upper cover (20) and liquidometer mouth (m1, m2), population (T), pressure tap (R), temperature-measuring port (s), hot water outlet or vapor outlet port (h) and the equilibration tube water outlet on its outer wall is set; Described balancing pipeline (21) carries out the thermal exchange in furnace sandwich;
Described cooling tank section assembly (D) is outside to be connected with outer furnace tube II (18) and cylindrical shell water tank (27) outer wall by HCL tube-cooled case (39), the inner solid welding joint (A5) of HCL outlet conduit (22) and interior stove cylinder (13) top that passes through is connected, and is connected in honeycomb graphite heat exchange block (I, II) with described honeycomb graphite heat exchange cooling section (F) top water cooler upper cover plate (28);
Described water cooler top assembly (E) and inner HCL outlet conduit (22) and water cooler upper cover plate (28) are provided with cavity, cooling for injected water;
Described inner honeycomb graphite cooling and absorbing heat exchanging segment assembly (F), is characterized in that, comprising: described molectron is provided with from bottom to up pad (32) and connects water cooler heat transfer block I, II; Described heat transfer block I, II are provided with nest bee-hole in length and breadth; Described nest bee-hole is for cooling HCL and cooling heat conduction.
3. a kind of combined steam formula graphite synthesis furnace for hydrochloride according to claim 1, is characterized in that, described outer furnace tube I assembly (14) below is provided with differential (7) and chassis I (5) and is arranged on the upper side of chassis II (6); In described stove, chassis I (5) is arranged on inner barrel (13) below; Described manhole plate (A8) is arranged on manhole differential (2) downside by bolt (A9).Described manhole differential (2) is connected to chassis II (6) downside by bolt (A7); Described chassis II (6) is provided with acid discharge mouth (c) and the sewage draining exit (d) of mouth down; Described manhole connecting pipe (3) arranges by chassis I (5), chassis II (6) and manhole differential (2) inner chamber; Described bulb socket is arranged in the inner chamber of manhole connecting pipe (3) and manhole differential (2).In described bulb socket, lamp holder is set, bulb socket is outer is provided with hydrogen inlet (a1-2), chlorine inlet (b) by angle.
4. a kind of combined steam formula graphite synthesis furnace for hydrochloride according to claim 1, is characterized in that, between described interior stove cylinder (13) bottom and chassis I (5), is provided with pad (9), and described interior stove cylinder (13) top is provided with synthetic upper cover plate (A6); Described outer furnace tube I (14) bottom is provided with o type circle (8) and connects by spring rod assembly (10); Described upper cover (20) is connected with outer furnace tube II (18) by bolt assembly; Described water cooler lower cover (37) is provided with long draw assembly (36) and is connected with cooler cylinder (30).
5.a kind of combined steam formula graphite synthesis furnace for hydrochloride according to claim 1, is characterized in that, described balancing pipeline (21) is connected to the hot water inlet and upper cover (20) the outer wall top that below outer furnace tube I outer wall, are provided with and is provided with on hot water outlet;
In described stove inner/outer tube interlayer body, be provided with the spiral deflector (A4) that adopts stainless steel to make, described hot water is helicoidal flow by spiral deflector (A4) structure.
6.according to a kind of combined steam formula graphite synthesis furnace for hydrochloride described in claim 1 and 5, it is characterized in that, described interior stove cylinder material adopts impermeable graphite manufacture, and heat transfer block adopts the cellular through hole of vertical and horizontal direction, and outer furnace tube adopts stainless material to make.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320738045.XU CN203625031U (en) | 2013-11-21 | 2013-11-21 | Combined steam-type graphite hydrogen chloride synthesis furnace |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320738045.XU CN203625031U (en) | 2013-11-21 | 2013-11-21 | Combined steam-type graphite hydrogen chloride synthesis furnace |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203625031U true CN203625031U (en) | 2014-06-04 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320738045.XU Expired - Lifetime CN203625031U (en) | 2013-11-21 | 2013-11-21 | Combined steam-type graphite hydrogen chloride synthesis furnace |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203625031U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108821237A (en) * | 2018-09-25 | 2018-11-16 | 李晓垚 | A kind of food grade hydrochloric acid synthetic furnace |
| CN111457749A (en) * | 2020-06-06 | 2020-07-28 | 南通星球石墨股份有限公司 | Synthetic furnace chassis heat transfer system |
-
2013
- 2013-11-21 CN CN201320738045.XU patent/CN203625031U/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108821237A (en) * | 2018-09-25 | 2018-11-16 | 李晓垚 | A kind of food grade hydrochloric acid synthetic furnace |
| CN111457749A (en) * | 2020-06-06 | 2020-07-28 | 南通星球石墨股份有限公司 | Synthetic furnace chassis heat transfer system |
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Address after: 226500 Jiangsu province Nantong City Jiuhua town Rugao City Huaxing Road No. 8 Patentee after: Nantong star graphite Co.,Ltd. Address before: 226500 Jiangsu province Nantong City Jiuhua Jiuhua town of Rugao City neighborhood Patentee before: NANTONG STAR GRAPHITE EQUIPMENT Co.,Ltd. |
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Granted publication date: 20140604 |