CN203558865U - Ammonium chloride solution purification device - Google Patents
Ammonium chloride solution purification device Download PDFInfo
- Publication number
- CN203558865U CN203558865U CN201320765579.1U CN201320765579U CN203558865U CN 203558865 U CN203558865 U CN 203558865U CN 201320765579 U CN201320765579 U CN 201320765579U CN 203558865 U CN203558865 U CN 203558865U
- Authority
- CN
- China
- Prior art keywords
- ammonium chloride
- chloride solution
- pipe
- recovery liquid
- membrane element
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 title claims abstract description 78
- 235000019270 ammonium chloride Nutrition 0.000 title claims abstract description 38
- 238000000746 purification Methods 0.000 title abstract 4
- 239000007788 liquid Substances 0.000 claims abstract description 23
- 238000011084 recovery Methods 0.000 claims abstract description 18
- 239000012528 membrane Substances 0.000 claims description 24
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 3
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 238000005259 measurement Methods 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 238000001704 evaporation Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000002351 wastewater Substances 0.000 abstract description 3
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 abstract 2
- 229910052921 ammonium sulfate Inorganic materials 0.000 abstract 2
- 235000011130 ammonium sulphate Nutrition 0.000 abstract 2
- 230000003247 decreasing effect Effects 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- 241000196324 Embryophyta Species 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000013505 freshwater Substances 0.000 description 4
- 239000006200 vaporizer Substances 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 3
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 3
- 235000015320 potassium carbonate Nutrition 0.000 description 3
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The utility model discloses an ammonium chloride solution purification device. The ammonium chloride solution purification device is characterized by comprising a frame, a recovery liquid inlet pipe perpendicularly arranged on the frame and a tee pipe; a first end of the tee pipe is connected to one end of the recovery liquid inlet pipe, a second end is connected to the suction port of a high pressure pump, and a third end is connected to the inlet of a film component unit; the film component unit spans over two sides of the frame, and the outlet of the film component unit is connected to an ammonium chloride solution pipe and discharges concentrated ammonium chloride solution out of the device. By the aid of the ammonium sulfate solution purification device, eighty percent of water in ammonium chloride solution can be concentrated, so that power of an evaporator for evaporating ammonium sulfate is decreased greatly, the power is decreased by eighty percent through multiple tests, energy is saved, production cost is reduced, water in ammonium chloride waste water can be reused, and energy saving and emission reduction are achieved actually.
Description
Technical field
The utility model relates to chemical production equipment technical field, is specifically related to a kind of ammonium chloride solution purifying plant.
Background technology
By ammoniacal liquor and potassium chloride ions exchange process, producing salt of wormwood and ammonium chloride, is one of important method of producing salt of wormwood and ammonium chloride.This method, by separating the ammonium chloride solution of gained after salt of wormwood product, is concentrated to finite concentration through evaporator evaporation, then send crystallisation by cooling in crystallizer to separate out ammonium chloride, then through centrifugation, be drying to obtain finished product ammonium chloride.
It is too low that at present most domestic enterprise adopts the purity of shell and tube heat exchanger evaporation concentration ammonium chloride solution, makes the ammonium chloride solution that filters out, needs through a large amount of evaporations, expend a large amount of manpower and materials, inefficiency.
Utility model content
The technical problems to be solved in the utility model is to provide a kind of ammonium chloride solution purifying plant, and production efficiency is high, production cost is low, volume is little, quality product; Concentrated ammonium chloride solution concentration is out higher, only needs single vaporization moisture, can show that the ammonium chloride solution that concentration is higher is dense.
For achieving the above object, the technical solution of the utility model is as follows:
A kind of ammonium chloride solution purifying plant, comprising:
One support body,
The recovery liquid that one vertical rack is located on support body enters pipe,
One Y-tube, the first port of described Y-tube connects described recovery liquid and enters pipe one end, and the second port connects the inhalation port of high-pressure pump, the entrance of the 3rd port connecting membrane elements group,
Described membrane element group is across described support body both sides, and the outlet of described membrane element group connects monochlor(in)ate ammonium solution pipe, by outside concentrated ammonium chloride solution discharger out.
In a preferred embodiment of the present utility model, described recovery liquid enters on pipe check valve is set, and the trend of liquid is reclaimed in described check valve restriction.
In a preferred embodiment of the present utility model, described recovery liquid enters the under meter that in the pipeline of pipe, a measurement is also set and reclaims the flow velocity of liquid; And coordinate a butterfly valve, control recovery liquid and enter pipe break-make.
In a preferred embodiment of the present utility model, described membrane element group comprises three membrane elements of parallel arrangement, and described membrane element is packaged in a pressurized vessel, and described pressurized vessel adopts special steel to make.
In a preferred embodiment of the present utility model, described membrane element comprises some film silks, the outer net with water-permeable that the outside bag of described film silk is established.
By technique scheme, the beneficial effects of the utility model are:
The utility model can by concentrated 80 percent fresh water in ammonium chloride solution out, thereby the vaporizer power for evaporating ammonium chloride is greatly reduced, the ammonia chloride crystal colourity concentrated by membrane separation technique is vivid, improved ammonium chloride quality, more main is the power that greatly reduces vaporizer, and through repeatedly test, power has reduced 80 percent, thereby accomplished saves energy, reduced productive expense.Make the fresh water in the waste water of containing ammonium chloride obtain reuse.Really accomplish energy-saving and emission-reduction.
Accompanying drawing explanation
In order to be illustrated more clearly in the utility model embodiment or technical scheme of the prior art, to the accompanying drawing of required use in embodiment or description of the Prior Art be briefly described below, apparently, accompanying drawing in the following describes is only embodiment more of the present utility model, for those of ordinary skills, do not paying under the prerequisite of creative work, can also obtain according to these accompanying drawings other accompanying drawing.
Fig. 1 is front view of the present utility model.
Fig. 2 is rear view of the present utility model.
Fig. 3 is left view of the present utility model.
Fig. 4 is the sectional view of membrane element of the present utility model.
Embodiment
For technique means, creation characteristic that the utility model is realized, reach object and effect is easy to understand, below in conjunction with concrete diagram, further set forth the utility model.
With reference to Fig. 1, shown in Fig. 2 and Fig. 3, a kind of ammonium chloride solution purifying plant, comprising:
One support body 100,
The recovery liquid that one vertical rack is located on support body 100 enters pipe 200,
One Y-tube 300, the first port 301 of described Y-tube 300 connects described recovery liquid and enters pipe 200 one end, and the second port 302 connects the entrance 501 of inhalation port 401, the three port 303 connecting membrane elements groups 500 of high-pressure pump 400,
Described membrane element group 500 is across described support body 100 both sides, and the outlet 502 of described membrane element group 500 connects monochlor(in)ate ammonium solution pipe 600, by outside concentrated ammonium chloride solution discharger out; One gate valve 601 and the motorized valve 602 arranged side by side with gate valve are wherein set on ammonium chloride solution pipe 600.
Described recovery liquid enters on pipe 200 check valve 201 is set, and the trend of liquid is reclaimed in described check valve 201 restrictions; Described recovery liquid enters the under meter 202 that the flow velocity of a measurement recovery liquid is also set in the pipeline of managing 200; And coordinate a butterfly valve 203, control recovery liquid and enter pipe 200 break-makes.
Described membrane element group 500 comprises three membrane elements 700 of parallel arrangement, and described membrane element 700 is packaged in a pressurized vessel 701, and described pressurized vessel 701 adopts special steel to make.
With reference to Fig. 4, described membrane element 700 comprises some film silks 702, the outer net with water-permeable 703 that the outside bag of described film silk 702 is established, and described film silk 702 two ends are fixed on pressurized vessel 701 by an end plate 704.
The utility model can by concentrated 80 percent fresh water in ammonium chloride solution out, thereby the vaporizer power for evaporating ammonium chloride is greatly reduced, the ammonia chloride crystal colourity concentrated by membrane separation technique is vivid, improved ammonium chloride quality, more main is the power that greatly reduces vaporizer, and through repeatedly test, power has reduced 80 percent, thereby accomplished saves energy, reduced productive expense.Make the fresh water in the waste water of containing ammonium chloride obtain reuse.Really accomplish energy-saving and emission-reduction.
More than show and described ultimate principle of the present utility model and principal character and advantage of the present utility model.The technician of the industry should understand; the utility model is not restricted to the described embodiments; that in above-described embodiment and specification sheets, describes just illustrates principle of the present utility model; do not departing under the prerequisite of the utility model spirit and scope; the utility model also has various changes and modifications, and these changes and improvements all fall within the scope of claimed the utility model.The claimed scope of the utility model is defined by appending claims and equivalent thereof.
Claims (5)
1. an ammonium chloride solution purifying plant, is characterized in that, comprising:
One support body,
The recovery liquid that one vertical rack is located on support body enters pipe,
One Y-tube, the first port of described Y-tube connects described recovery liquid and enters pipe one end, and the second port connects the inhalation port of high-pressure pump, the entrance of the 3rd port connecting membrane elements group,
Described membrane element group is across described support body both sides, and the outlet of described membrane element group connects monochlor(in)ate ammonium solution pipe, by outside concentrated ammonium chloride solution discharger out.
2. a kind of ammonium chloride solution purifying plant according to claim 1, is characterized in that: described recovery liquid enters on pipe check valve is set, and the trend of liquid is reclaimed in described check valve restriction.
3. a kind of ammonium chloride solution purifying plant according to claim 1, is characterized in that: described recovery liquid enters the under meter that in the pipeline of pipe, a measurement is also set and reclaims the flow velocity of liquid; And coordinate a butterfly valve, control recovery liquid and enter pipe break-make.
4. a kind of ammonium chloride solution purifying plant according to claim 1, is characterized in that: described membrane element group comprises three membrane elements of parallel arrangement, and described membrane element is packaged in a pressurized vessel, and described pressurized vessel adopts special steel to make.
5. a kind of ammonium chloride solution purifying plant according to claim 4, is characterized in that: described membrane element comprises some film silks, the outer net with water-permeable that the outside bag of described film silk is established.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320765579.1U CN203558865U (en) | 2013-11-26 | 2013-11-26 | Ammonium chloride solution purification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320765579.1U CN203558865U (en) | 2013-11-26 | 2013-11-26 | Ammonium chloride solution purification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203558865U true CN203558865U (en) | 2014-04-23 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320765579.1U Expired - Lifetime CN203558865U (en) | 2013-11-26 | 2013-11-26 | Ammonium chloride solution purification device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203558865U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111661853A (en) * | 2020-01-03 | 2020-09-15 | 宁夏云泰科技有限公司 | Production process of industrial ammonium chloride |
-
2013
- 2013-11-26 CN CN201320765579.1U patent/CN203558865U/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111661853A (en) * | 2020-01-03 | 2020-09-15 | 宁夏云泰科技有限公司 | Production process of industrial ammonium chloride |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: ANHUI CLEAN ENVIRONMENT BIOLOGICAL TECHNOLOGY CO., Free format text: FORMER OWNER: XI N DEQI WATER PROCESSING CO., LTD. Effective date: 20150107 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 710061 XI'AN, SHAANXI PROVINCE TO: 230088 HEFEI, ANHUI PROVINCE |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20150107 Address after: 230088 Anhui city of Hefei province high tech Zone Huayi Science Park building E Room 401 Patentee after: ANHUI CLEAN ENVIRONMENTAL BIOTECHNOLOGY CO.,LTD. Address before: 710061, No. 16, No. 11002, Ziwei building, electronic road, Xi'an hi tech Zone, Shaanxi, China Patentee before: XI'AN DEQI WATER TREATMENT Co.,Ltd. |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20140423 |