CN203529927U - Anhydrous hydrogen fluoride production equipment - Google Patents

Anhydrous hydrogen fluoride production equipment Download PDF

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Publication number
CN203529927U
CN203529927U CN201320677983.3U CN201320677983U CN203529927U CN 203529927 U CN203529927 U CN 203529927U CN 201320677983 U CN201320677983 U CN 201320677983U CN 203529927 U CN203529927 U CN 203529927U
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CN
China
Prior art keywords
water
reboiler
communicated
water tank
outlet
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN201320677983.3U
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Chinese (zh)
Inventor
张宏保
刘海成
李家朋
任洪志
张鲁鲁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Luoyang Fluorine And Potassium Technology Co ltd
Luoyang Potassium Fluoride Technology Co ltd
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Luoyang Fluofide & Potassium Technology Co Ltd
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Priority to CN201320677983.3U priority Critical patent/CN203529927U/en
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Publication of CN203529927U publication Critical patent/CN203529927U/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/129Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Abstract

The utility model provides anhydrous hydrogen fluoride production equipment which comprises a rectification column, a degassing tower, a hot blast stove and a thermal circulation device, wherein the thermal circulation device comprises a hot water storage tank, a residual heat exchanger, a rectification reboiler in butt joint with the rectification column and a degasification reboiler in butt joint with the degassing tower; the residual heat exchanger comprises a water tank and a gas heating pipe used for heating water; the air inlet of the gas heating pipe is communicated with the waste gas discharge outlet of the hot blast stove; the water outlet of the hot water storage tank is communicated with the heating water inlet of the rectification reboiler and the heating water inlet of the degasification reboiler through a water inlet pipe; the heating water outlet of the rectification reboiler and the heating water outlet of the degasification reboiler are respectively communicated with the water inlet of the water tank through a water return pipe; the water outlet of the water tank is communicated with the hot water storage tank through a water outlet pipe. The production equipment has the advantages of scientific design, reduced energy consumption and pollution, improved gas utilization rate.

Description

Anhydrous hydrogen fluoride production unit
Technical field
The utility model relates to a kind of anhydrous hydrogen fluoride production unit, specifically, has related to a kind of anhydrous hydrogen fluoride production unit with energy-saving and emission-reduction and exhaust gas utilization.
Background technology
In the production unit of existing anhydrous hydrogen fluoride, in rectifying tower and degassing tower, steam coils is installed, has a circular fluid bed to carry out steam supply for this steam coils, thereby realize the heat supply to rectifying tower and degassing tower.Yet in actual production, the energy consumption of circular fluid bed is very large, increase enterprise's production cost, and circular fluid bed self also wants discharging waste gas, be unfavorable for energy-saving and emission-reduction.And in the production process of anhydrous hydrogen fluoride, in hotblast stove expellant gas, containing very high heat, this part gas directly enters atmosphere, has not only wasted energy, and environment is caused to disadvantageous effect.。
In order to solve the problem of above existence, people are seeking a kind of desirable technical solution always.
Summary of the invention
The purpose of this utility model is for the deficiencies in the prior art, thereby provides a kind of design science, reduction energy consumption, minimizing to pollute, improve the anhydrous hydrogen fluoride production unit of exhaust gas utilization rate.
To achieve these goals, the technical scheme that the utility model adopts is: a kind of anhydrous hydrogen fluoride production unit, comprise rectifying tower, degassing tower, hotblast stove, thermocirculator, described thermocirculator comprises hot water tank, afterheat heat exchanger, the rectifying reboiler docking with described rectifying tower and the degassed reboiler docking with described degassing tower; Described afterheat heat exchanger comprises water tank and for the gas heating pipe to water heating, the inlet mouth of described gas heating pipe is communicated with the Waste gas outlet of described hotblast stove; The water outlet of described hot water tank is communicated with the heating water-in of described rectifying reboiler and the heating water-in of described degassed reboiler by inlet channel, the hot water outlet that adds that adds hot water outlet and described degassed reboiler of described rectifying reboiler is communicated with the water-in of described water tank by water return pipeline respectively, and the water outlet of described water tank is communicated with described hot water tank by outlet conduit; Described inlet channel is provided with water pump.
Based on above-mentioned, the winding of described gas heating pipe is on described water tank.
Based on above-mentioned, described hot water tank is provided with moisturizing pipeline.
Based on above-mentioned, be communicated with the bottom of described rectifying tower and the bottom of described rectifying reboiler and be communicated with the bottom of described degassing tower and the pipeline of the bottom of described degassed reboiler on be all connected with blow-off line, described in each, on blow-off line, be equipped with wash water valve.
The utility model utilizes the heat of Exhaust Gas in described hotblast stove, by waste gas, water heated and utilize the mode of recirculated water to carry out heat supply to described rectifying tower and described degassing tower, replaced circular fluid bed heat supply of the prior art, avoided circular fluid bed energy consumption, eliminated the exhaust emission of circular fluid bed, effectively utilized the heat of waste gas in hotblast stove.This anhydrous hydrogen fluoride production unit has advantages of design science, reduces energy consumption, reduces and pollute, improve exhaust gas utilization rate.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model.
In figure: 1. rectifying tower; 2. degassing tower; 3. rectifying reboiler; 4. degassed reboiler; 5. hot water tank; 6. afterheat heat exchanger; 7. water pump; 8. moisturizing pipeline; 9. inlet channel; 10. water return pipeline; 11. outlet conduits.
Embodiment
Below by embodiment, the technical solution of the utility model is described in further detail.
embodiment 1
As shown in Figure 1, a kind of anhydrous hydrogen fluoride production unit, comprise rectifying tower 1, degassing tower 2, hotblast stove, thermocirculator, described thermocirculator comprises hot water tank 5, afterheat heat exchanger 6, the rectifying reboiler 3 docking with described rectifying tower 1 and the degassed reboiler 4 docking with described degassing tower 2; Described afterheat heat exchanger 6 comprises water tank and for the gas heating pipe to water heating, the inlet mouth of described gas heating pipe is communicated with the Waste gas outlet of described hotblast stove; The water outlet of described hot water tank 5 is communicated with the heating water-in of described rectifying reboiler 3 and the heating water-in of described degassed reboiler 4 by inlet channel 9, the hot water outlet that adds that adds hot water outlet and described degassed reboiler 4 of described rectifying reboiler 3 is communicated with the water-in of described water tank by water return pipeline 10 respectively, and the water outlet of described water tank is communicated with described hot water tank 5 by outlet conduit 11; Described inlet channel 9 is provided with water pump 7.Described water pump 7 designs are on described inlet channel 9, because water tank rest on the ground conventionally, and the heating water-in of described rectifying reboiler 3 and the heating water-in of described degassed reboiler 4 are generally higher, thus need to water be stamped with described water pump 7, and provide power for water cycle.And described water return pipeline 10 and described outlet conduit 11 are to dirty or advection, do not need to install water pump.
Described rectifying reboiler 3 is identical with the internal structure of described degassed reboiler 4, but vary in size, 30 square metres of rectifying reboiler 3 heat interchanging areas, 20 square metres of degassed reboiler 4 heat interchanging areas, this is mainly according to described rectifying tower 1 and the required thermal design of described degassing tower 2 internal recycle.
In production process, waste gas in described hotblast stove is arranged into described gas heating pipe, after described gas heating pipe is heated, water in described water tank is heated, hot water is transported in described hot water tank 5 by described outlet conduit 11, described water pump 7 pumps into described rectifying reboiler 3 and described degassed reboiler 4 by the hot water in described hot water tank 5 by described inlet channel 9, thereby making described rectifying reboiler 3 is described rectifying tower 1 heat supply, making described degassed reboiler 4 is described degassing tower 2 heat supplies, then the water through heat exchange is back to described water tank by described water return pipeline 10 from described rectifying reboiler 3 and described degassed reboiler 4, again recycle.The utility model utilizes the heat of Exhaust Gas in described hotblast stove, by waste gas, water heated and utilize the mode of recirculated water to carry out heat supply to described rectifying tower 1 and described degassing tower 2, replaced circular fluid bed heat supply of the prior art, avoided circular fluid bed energy consumption, eliminated the exhaust emission of circular fluid bed, effectively utilized the heat of waste gas in hotblast stove.
embodiment 2
Embodiment 2 is with the difference of embodiment 1: the winding of described gas heating pipe is on described water tank, design has increased the heat interchanging area of described gas heating pipe and described water tank to greatest extent like this, thereby heat can be passed to water tank fast and effectively after described gas heating pipe is heated by waste gas, water is heated, utilize the mode of this gas-liquid heat exchange to carry out efficient utilization to the waste-gas heat of described hotblast stove discharge.
embodiment 3
Embodiment 3 is with the difference of embodiment 2: described hot water tank 5 is provided with moisturizing pipeline ,when being run off in circulating transfer process, supplements in time in water.
embodiment 4
Embodiment 4 is with the difference of embodiment 3: be communicated with the bottom of described rectifying tower 1 and the bottom of described rectifying reboiler 3 and be communicated with the bottom of described degassing tower 2 and the pipeline of the bottom of described degassed reboiler 4 on be all connected with blow-off line, described in each, on blow-off line, be equipped with wash water valve.The blowdown terminal of each blow-off line is communicated with and shares a sewage draining exit, and blow-off line and wash water valve conveniently collect waste water, and unified discharge, is convenient to sewage to process.
Finally should be noted that: above embodiment is only in order to illustrate that the technical solution of the utility model is not intended to limit; Although the utility model is had been described in detail with reference to preferred embodiment, those of ordinary skill in the field are to be understood that: still can modify or part technical characterictic is equal to replacement embodiment of the present utility model; And not departing from the spirit of technical solutions of the utility model, it all should be encompassed in the middle of the technical scheme scope that the utility model asks for protection.

Claims (4)

1. an anhydrous hydrogen fluoride production unit, comprise rectifying tower, degassing tower and hotblast stove, it is characterized in that: it also comprises thermocirculator, described thermocirculator comprises hot water tank, afterheat heat exchanger, the rectifying reboiler docking with described rectifying tower and the degassed reboiler docking with described degassing tower; Described afterheat heat exchanger comprises water tank and for the gas heating pipe to water heating, the inlet mouth of described gas heating pipe is communicated with the Waste gas outlet of described hotblast stove; The water outlet of described hot water tank is communicated with the heating water-in of described rectifying reboiler and the heating water-in of described degassed reboiler by inlet channel, the hot water outlet that adds that adds hot water outlet and described degassed reboiler of described rectifying reboiler is communicated with the water-in of described water tank by water return pipeline respectively, and the water outlet of described water tank is communicated with described hot water tank by outlet conduit; Described inlet channel is provided with water pump.
2. anhydrous hydrogen fluoride production unit according to claim 1, is characterized in that: the winding of described gas heating pipe is on described water tank.
3. anhydrous hydrogen fluoride production unit according to claim 1 and 2, is characterized in that: described hot water tank is provided with moisturizing pipeline.
4. anhydrous hydrogen fluoride production unit according to claim 3, it is characterized in that: be communicated with the bottom of described rectifying tower and the bottom of described rectifying reboiler and be communicated with the bottom of described degassing tower and the pipeline of the bottom of described degassed reboiler on be all connected with blow-off line, described in each, on blow-off line, be equipped with wash water valve.
CN201320677983.3U 2013-10-31 2013-10-31 Anhydrous hydrogen fluoride production equipment Expired - Lifetime CN203529927U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201320677983.3U CN203529927U (en) 2013-10-31 2013-10-31 Anhydrous hydrogen fluoride production equipment

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Application Number Priority Date Filing Date Title
CN201320677983.3U CN203529927U (en) 2013-10-31 2013-10-31 Anhydrous hydrogen fluoride production equipment

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CN203529927U true CN203529927U (en) 2014-04-09

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107388276A (en) * 2016-05-14 2017-11-24 江西理文化工有限公司 A kind of waste heat recovery and Application way
CN108946668A (en) * 2018-10-17 2018-12-07 杨松 A kind of anhydrous hydrogen fluoride preparation section

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107388276A (en) * 2016-05-14 2017-11-24 江西理文化工有限公司 A kind of waste heat recovery and Application way
CN108946668A (en) * 2018-10-17 2018-12-07 杨松 A kind of anhydrous hydrogen fluoride preparation section

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: LUOYANG FLUORIDE + POTASSIUM TECHNOLOGY CO., LTD.

Free format text: FORMER NAME: LUOYANG FLUORIDE + POTASSIUM TECHNOLOGY LTD.

Owner name: LUOYANG FLUORIDE + POTASSIUM TECHNOLOGY COMPANY

Free format text: FORMER NAME: LUOYANG FLUORIDE + POTASSIUM TECHNOLOGY CO., LTD.

CP01 Change in the name or title of a patent holder

Address after: 471400, Luoyang, Songxian, Henan province Township Po Industrial Agglomeration Area Luoyang fluorine potassium Technology Co., Ltd.

Patentee after: LUOYANG POTASSIUM FLUORIDE TECHNOLOGY CO.,LTD.

Address before: 471400, Luoyang, Songxian, Henan province Township Po Industrial Agglomeration Area Luoyang fluorine potassium Technology Co., Ltd.

Patentee before: Luoyang Fluorine and Potassium Technology Co.,Ltd.

Address after: 471400, Luoyang, Songxian, Henan province Township Po Industrial Agglomeration Area Luoyang fluorine potassium Technology Co., Ltd.

Patentee after: Luoyang Fluorine and Potassium Technology Co.,Ltd.

Address before: 471400, Luoyang, Songxian, Henan province Township Po Industrial Agglomeration Area Luoyang fluorine potassium Technology Co., Ltd.

Patentee before: Luoyang Fluoride & Potassium Technology Co.,Ltd.

CX01 Expiry of patent term

Granted publication date: 20140409

CX01 Expiry of patent term