CN203479044U - Multilayer separating tower for distillation and condensation with high efficiency - Google Patents
Multilayer separating tower for distillation and condensation with high efficiency Download PDFInfo
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- CN203479044U CN203479044U CN201320333956.4U CN201320333956U CN203479044U CN 203479044 U CN203479044 U CN 203479044U CN 201320333956 U CN201320333956 U CN 201320333956U CN 203479044 U CN203479044 U CN 203479044U
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Abstract
The utility model relates to a multilayer separating tower for distillation and condensation with high efficiency. The multilayer separating tower comprises a first shell. A mixed gas inlet and a condensate water outlet are arranged on the first shell; the first shell is connected with a first condenser; the first condenser is connected with a first separating chamber; a first liquid collecting outlet is arranged on the first separating chamber; the first separating chamber is connected with a second condenser; the second condenser is in a connection with a second separating chamber; a second liquid collecting outlet is arranged on the second separating chamber; the second separating chamber is in a connection with a third condenser; the third condenser is connected with a second shell; and a non-condensable gas outlet is arranged on the second shell. The multilayer separating tower for distillation and condensation with high efficiency is advantageous in that the multilayer separating tower is simple structure with great condensing effect; a structure among all parts is compact; material as needed can be better condensed with high purity; and medium can be ensured to be condensed in different temperatures.
Description
Technical field
The utility model relates to a kind of multi-layer efficient distillation condensation separation tower.
Background technology
The effect of general condenser condenses is bad, the material that well condensation goes out to need, condensed material is impure, and three condensers that adopt are directly placed on support, need a lot of pipelines to connect, the separating technology of mist is more complicated also, can not well guarantee the condensation of medium under different temperatures.
Summary of the invention
The purpose of this utility model is in order to overcome above deficiency, provides simple in structure and cost is low, the simple multi-layer efficient of technique distillation condensation separation tower.
The purpose of this utility model is achieved through the following technical solutions: a kind of multi-layer efficient distillation condensation separation tower, comprise the first housing, described the first housing is provided with mist import and condensation-water drain, described the first housing is connected with the first condenser, described the first condenser is connected with the first separation chamber, described the first separation chamber is provided with the first liquid collecting outlet, described the first separation chamber is connected with the second condenser, described the second condenser is connected with the second separation chamber, described the second separation chamber is provided with the second liquid collecting outlet, described the second separation chamber is connected with the 3rd condenser, described the 3rd condenser is connected with the second housing, described the second housing is provided with on-condensible gas outlet.
On the first condenser, the second condenser and the 3rd condenser, be equipped with water inlet and delivery port.
Described the first housing is connected with reboiler, and described the first housing is provided with sensor.
The method of multi-layer efficient distillation condensation separation tower separating mixed gas: mist is entered by the mist import on the first housing, the first condenser adopts normal temperature circulating water, by the steam evaporation in mist, after evaporation, by condensation-water drain, discharged, uncooled mist enters the second condenser through the first condenser, the water cooling of 6-8 ℃ that the second condenser adopts, isolated dimethoxym ethane condensation is discharged by the first liquid collecting outlet in the first separation chamber, uncooled mist is through the 3rd condenser, the 3rd condenser adopts-31--28 ℃ of water quench, isolated methyl alcohol is separated through the second liquid collecting outlet in the second separation chamber, do not have the gas of condensation to discharge through the on-condensible gas outlet on the 4th housing.
The utlity model has following advantage: relatively simple for structure, compact conformation between each parts, condensation effective, well condensation goes out needed material, condensed material purity is high, well guarantees the condensation of medium under different temperatures, and technique is fairly simple, do not need pipeline, cost compare is low.
Accompanying drawing explanation:
Fig. 1 is structural representation of the present utility model;
Number in the figure: 1-the first housing, the import of 2-mist, 3-condensation-water drain, 4-the first condenser, 5-the second housing, the outlet of 6-dimethoxym ethane, 7-the second condenser, 8-the 3rd housing, the outlet of 9-methyl alcohol, 10-the 3rd condenser, 11-the 4th housing, the outlet of 12-on-condensible gas, 13-water inlet, 14-delivery port.
The specific embodiment:
In order to deepen understanding of the present utility model, below in conjunction with embodiment and accompanying drawing, the utility model is described in further detail, and this embodiment only, for explaining the utility model, does not form the restriction to the utility model protection domain.
As Fig. 1 shows a kind of combination condenser of the utility model, comprise the first housing 1, the first housing 1 is provided with mist import 2 and condensation-water drain 3, described the first housing 1 is connected with the first condenser 4, described the first condenser 4 is connected with the second housing 5, described the second housing 5 is provided with dimethoxym ethane outlet 6, described the second housing 5 is connected with the second condenser 7, described the second condenser 7 is connected with the 3rd housing 8, described the 3rd housing 8 is provided with methyl alcohol outlet 9, described the 3rd housing 8 is connected with the 3rd condenser 10, described the 3rd condenser 10 is connected with the 4th housing 11, described the 4th housing 11 is provided with on-condensible gas outlet 12.
On described the first condenser 4, the second condenser 7 and the 3rd condenser 10, be equipped with water inlet 13 and delivery port 14.Water inlet 13 inflow temperatures on the first condenser 4 are 32 ℃, delivery port 14 leaving water temperatures are asked 38 ℃, water inlet 13 inflow temperatures of the second condenser 7 are 7 ℃, delivery port 14 leaving water temperatures are asked 38 ℃, water inlet 13 inflow temperatures of the 3rd condenser 10 are-30 ℃, and delivery port 14 leaving water temperatures are asked-25 ℃.
The first housing 1 is connected with reboiler 15, and described the first housing 1 is provided with sensor 16.Sensor 16 can be responded to the temperature of mist, if temperature is too low, can heat by reboiler 15.
The embodiment 1 of separating mixed gas: mist is entered by the mist import 2 on the first housing 1, the first condenser 4 adopts normal temperature circulating water, by the steam evaporation in mist, by condensation-water drain 3, discharged, uncooled mist enters the second condenser 7 through the first condenser 4, the second condenser 7 adopts is the water cooling of 7 ℃, isolated dimethoxym ethane condensation is discharged by the first liquid collecting outlet 6, uncooled mist is through the 3rd condenser 10, the 3rd condenser 10 adopts-30 ℃ of water quench, the second liquid collecting outlet 9 of isolated methyl alcohol process is separated, do not have the gas of condensation to discharge through the on-condensible gas outlet 12 on the second housing 11.Each stage condensation effective, well condensation go out needed material, and condensed material purity is high, and formaldehyde purity reaches 99.8%, and dimethoxym ethane purity reaches 99.7%, well guarantees the condensation of medium under different temperatures.
The embodiment 2 of separating mixed gas: mist is entered by the mist import 2 on the first housing 1, the first condenser 4 adopts normal temperature circulating water, by the steam evaporation in mist, by condensation-water drain 3, discharged, uncooled mist enters the second condenser 7 through the first condenser 4, the second condenser 7 adopts is the water cooling of 6.5 ℃, isolated dimethoxym ethane condensation is discharged by the first liquid collecting outlet 6, uncooled mist is through the 3rd condenser 10, the 3rd condenser 10 adopts-31 ℃ of water quench, the second liquid collecting outlet 9 of isolated methyl alcohol process is separated, do not have the gas of condensation to discharge through the on-condensible gas outlet 12 on the second housing 11.Each stage condensation effective, well condensation go out needed material, and condensed material purity is high, and formaldehyde purity reaches 99.4%, and dimethoxym ethane purity reaches 99.5%, well guarantees the condensation of medium under different temperatures.
The embodiment 3 of separating mixed gas: mist is entered by the mist import 2 on the first housing 1, the first condenser 4 adopts normal temperature circulating water, by the steam evaporation in mist, by condensation-water drain 3, discharged, uncooled mist enters the second condenser 7 through the first condenser 4, the second condenser 7 adopts is the water cooling of 7.5 ℃, isolated dimethoxym ethane condensation is discharged by the first liquid collecting outlet 6, uncooled mist is through the 3rd condenser 10, the 3rd condenser 10 adopts-30.5 ℃ of water quench, the second liquid collecting outlet 9 of isolated methyl alcohol process is separated, do not have the gas of condensation to discharge through the on-condensible gas outlet 12 on the second housing 11.Each stage condensation effective, well condensation go out needed material, and condensed material purity is high, and formaldehyde purity reaches 99.6%, and dimethoxym ethane purity reaches 99.7%, well guarantees the condensation of medium under different temperatures.
The boiling point of methyl alcohol is-21 ℃, and described dimethoxym ethane boiling point is 42.3 ℃.
Claims (3)
1. a multi-layer efficient distills condensation separation tower, comprise the first housing (1), it is characterized in that: described the first housing (1) is provided with mist import (2) and condensation-water drain (3), described the first housing (1) is connected with the first condenser (4), described the first condenser (4) is connected with the first separation chamber (5), described the first separation chamber (5) is provided with the first liquid collecting outlet (6), described the first separation chamber (5) is connected with the second condenser (7), described the second condenser (7) is connected with the second separation chamber (8), described the second separation chamber (8) is provided with the second liquid collecting outlet (9), described the second separation chamber (8) is connected with the 3rd condenser (10), described the 3rd condenser (10) is connected with the second housing (11), described the second housing (11) is provided with on-condensible gas outlet (12).
2. multi-layer efficient distills condensation separation tower according to claim 1, it is characterized in that: on described the first condenser (4), the second condenser (7) and the 3rd condenser (10), be equipped with water inlet (13) and delivery port (14).
3. multi-layer efficient distills condensation separation tower according to claim 1, it is characterized in that: described the first housing (1) is connected with reboiler (15), and described the first housing (1) is provided with sensor (16).
Priority Applications (1)
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CN201320333956.4U CN203479044U (en) | 2013-06-09 | 2013-06-09 | Multilayer separating tower for distillation and condensation with high efficiency |
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CN201320333956.4U CN203479044U (en) | 2013-06-09 | 2013-06-09 | Multilayer separating tower for distillation and condensation with high efficiency |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103335534A (en) * | 2013-06-09 | 2013-10-02 | 南通久信石墨科技开发有限公司 | Multi-layer efficient distilling condensation separating tower and mixed gas separating method thereof |
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2013
- 2013-06-09 CN CN201320333956.4U patent/CN203479044U/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103335534A (en) * | 2013-06-09 | 2013-10-02 | 南通久信石墨科技开发有限公司 | Multi-layer efficient distilling condensation separating tower and mixed gas separating method thereof |
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Granted publication date: 20140312 |