CN203469947U - Multifunctional high temperature and high pressure reaction kettle - Google Patents
Multifunctional high temperature and high pressure reaction kettle Download PDFInfo
- Publication number
- CN203469947U CN203469947U CN201320522805.3U CN201320522805U CN203469947U CN 203469947 U CN203469947 U CN 203469947U CN 201320522805 U CN201320522805 U CN 201320522805U CN 203469947 U CN203469947 U CN 203469947U
- Authority
- CN
- China
- Prior art keywords
- plug
- kettle
- reaction kettle
- high temperature
- still
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Abstract
The utility model discloses a multifunctional high temperature and high pressure reaction kettle. The multifunctional high temperature and high pressure reaction kettle comprises a kettle body (10), a capillary tube (12), a pressure tube screw (13), a first kettle plug (11) and a second kettle plug (6), wherein taper holes are formed in the first kettle plug (11) and/or the second kettle plug (6). The multifunctional high temperature and high pressure reaction kettle is simple in structure; when the multifunctional high temperature and high pressure reaction kettle is used, a corresponding optical window, an energy converter and a functional electrode are arranged in the taper holes, the in-situ observation comprising optics, spectroscopy, electricity, acoustics, electrochemistry and various physicochemical properties can be simultaneously realized on a sample in the reaction kettle at relatively high temperature and pressure, and the problems that in-situ observation means are limited by the structure defect of a conventional reaction kettle and operating temperature and pressure are not allowed to be too high can be solved.
Description
Technical field
The utility model relates to a kind of multidisciplinary research and industrial multifunctional high-temperature autoclave of being applicable to, and belongs to reactor field.
Background technology
High-temperature high-pressure reaction kettle can be the environment that people provide a kind of high temperature and high pressure, experimental simulation at earth interior Petrogenesis And Metallogenesis, the research and development of submarine hydrothermal solution Detection Techniques, and the field such as supercritical fluid extraction, supercritical water oxidation, petrochemical industry, coal-fired clean utilization, hydro-thermal material are synthetic, metal corrosion and protection and Pressure hydrometallurgy all has and relate to, it is the class device widely using in scientific experiment, engineering research and development and production practices.Along with the research and development of scientific research and engineering deepen continuously and expand, and industrial production is more and more high to the requirement of controlling, and often multiple in-situ observation system need to be installed on high-temperature high-pressure reaction kettle simultaneously.Yet, existing reactor is due to structural defect, can allow the in-situ observation means of installation very limited, after in-situ observation system is installed, operating temperature and pressure are also not high, conventionally cannot meet the demands, the multifunctional high pressure still that this just need to develop a kind of integrated multiple in-situ observation means simultaneously and can work under higher temperature and pressure.
Summary of the invention
The technical problems to be solved in the utility model: a kind of simultaneously integrated in-situ observation system of optics, spectroscopy, electricity, acoustics, electrochemistry and number of chemical sensor the multifunctional high-temperature autoclave that can work under higher temperature pressure of comprising is provided, causes the problem that the limited and operating temperature of the kind of in-situ observation means and pressure can not be too high to solve existing reactor because of fault of construction.
Technical solutions of the utility model:
A multifunctional high-temperature autoclave, comprises kettle, capillary, pressure pipe screw, the first still plug and the second still plug, it is characterized in that: at the first still plug and/or the second still, have taper hole beyond the Great Wall.
Above-mentioned the first still plug and/or the second still taper hole are beyond the Great Wall more than 1.
Aforesaid the second still plug is connected with kettle by sealing ring, hold-down ring and tightening nuts with the first still plug.
Aforesaid the second still plug and the first still are also provided with a nut beyond the Great Wall, between nut and tightening nuts, are provided with packing ring.
Aforementioned the first still plug and/or the second still have the aperture being communicated with capillary beyond the Great Wall.
The utility model beneficial effect:
Compared with the prior art, a kind of multifunctional high-temperature autoclave of the utility model, by having a plurality of taper holes beyond the Great Wall at autoclave still, corresponding optical window, transducer and functional electrode are installed during use in taper hole, can be under higher temperature, pressure to reactor in sample realize the in-situ observation that comprises optics, spectroscopy, electricity, acoustics, electrochemistry and multiple physicochemical properties etc. simultaneously.
accompanying drawing explanation:
Fig. 1 is vertical section structure schematic diagram of the present utility model.
the specific embodiment:
As Fig. 1, a kind of multifunctional high-temperature autoclave of the utility model, comprises kettle 10, capillary 12, pressure pipe screw 13, the first still plug 11 and the second still plug 6, has taper hole 7 and taper hole 8 on the second still plug 6; On the first still plug 11, have 1 taper hole 9; The first still plug 11 is connected with kettle 10 by sealing ring 5, hold-down ring 4 and tightening nuts 3 with the second still plug 6, so that still plug 11 and 6 can be tightly connected with kettle 10; On the first still plug still 11, be processed with an aperture, be communicated with capillary 12; On the second still plug 6, also process an aperture, be communicated with capillary 12.Outside the second still plug 6 and the first still plug 11, a nut 1 is also installed, tightening this nut can crush seal ring, makes sealing effectiveness better; Between nut 1 and tightening nuts 3, packing ring 2 is installed.
Each parts all adopt nickel-base alloy processing and fabricating above, so that reactor corrosion resistance is good, can be applicable to the corrosive fluids medium under normal temperature ~ 650 ℃ and normal pressure ~ 100 MPa condition.
During use, corresponding optical window, transducer and functional electrode are installed in taper hole, can be under higher temperature, pressure to reactor in sample realize the in-situ observation that comprises optics, spectroscopy, electricity, acoustics, electrochemistry and multiple physicochemical properties etc. simultaneously.Such as, in the interior assembling mineral electrodes of taper hole 7, at the interior assembling chemical sensor electrode of taper hole 8, at the interior assembled heat galvanic couple of taper hole 9, now the utility model multifunctional high-temperature autoclave can carry out the electro-chemical test of HTHP hydrothermal system, the functional studies such as in site measurement of the physicochemical properties of reactor still inner fluid simultaneously.
Claims (5)
1. a multifunctional high-temperature autoclave, comprise kettle (10), capillary (12), pressure pipe screw (13), the first still plug (11) and the second still plug (6), it is characterized in that: on the first still plug (11) and/or the second still plug (6), have taper hole.
2. a kind of multifunctional high-temperature autoclave according to claim 1, is characterized in that: the first described still plug (11) and/or the taper hole on the second still plug (6) are more than 1.
3. a kind of multifunctional high-temperature autoclave according to claim 1, is characterized in that: the second described still plug (6) is connected with kettle (10) by sealing ring (5), hold-down ring (4) and tightening nuts (3) with the first still plug (11).
4. a kind of multifunctional high-temperature autoclave according to claim 1, it is characterized in that: the second described still plug (6) and the first still plug (11) are outer is also provided with a nut (1), between nut (1) and tightening nuts (3), is provided with packing ring (2).
5. a kind of multifunctional high-temperature autoclave according to claim 1, is characterized in that: on the first described still plug (11) and/or the second still plug (6), have the aperture being communicated with capillary (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320522805.3U CN203469947U (en) | 2013-08-26 | 2013-08-26 | Multifunctional high temperature and high pressure reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320522805.3U CN203469947U (en) | 2013-08-26 | 2013-08-26 | Multifunctional high temperature and high pressure reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203469947U true CN203469947U (en) | 2014-03-12 |
Family
ID=50218365
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320522805.3U Expired - Fee Related CN203469947U (en) | 2013-08-26 | 2013-08-26 | Multifunctional high temperature and high pressure reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203469947U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103406070A (en) * | 2013-08-26 | 2013-11-27 | 中国科学院地球化学研究所 | Multifunctional high-temperature and high-pressure reaction kettle |
-
2013
- 2013-08-26 CN CN201320522805.3U patent/CN203469947U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103406070A (en) * | 2013-08-26 | 2013-11-27 | 中国科学院地球化学研究所 | Multifunctional high-temperature and high-pressure reaction kettle |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103406070A (en) | Multifunctional high-temperature and high-pressure reaction kettle | |
| CN102445478B (en) | Working electrode for realizing electrochemical test of high-temperature high-pressure water system | |
| CN104614310B (en) | A kind of high temperature pressure corrosion electro-chemical measuring apparatus and measuring method | |
| CN202111297U (en) | Thermocouple connector used on high-reliability occasions | |
| CN203705392U (en) | Electrochemical experiment device for high-temperature leaching of mineral | |
| CN203469947U (en) | Multifunctional high temperature and high pressure reaction kettle | |
| CN202153205U (en) | Corrosion test facility under oil pipe joint real object circulating stress | |
| CN203705152U (en) | A metal corrugated pipe high temperature high pressure fatigue life test apparatus | |
| CN103644423B (en) | A kind of online hanger device of pipeline | |
| CN105699201B (en) | High pressure shell pass type pressure testing device for floating head type heat exchanger | |
| CN203395485U (en) | Liquid pipeline with pressure relieving and constant hydraulic pressure displaying functions | |
| CN204611219U (en) | A kind of broken pipe seal arrangement | |
| CN204294716U (en) | The expanding compound tube end sizing of hydraulic pressure of dual-metal clad steel pipe and sealing device | |
| CN201988213U (en) | Ethanol recovering device | |
| CN201852739U (en) | Pipeline pressure fluctuation experiment device | |
| CN205483964U (en) | Duct flow formula developments galvanic corrosion test fixture device | |
| CN204128906U (en) | A kind of PE pipe external pressure test device | |
| CN203629758U (en) | Tool specialized for leakage test of corrugated tube | |
| CN203571317U (en) | Pup-joint type pipeline on-line coupon combined device | |
| CN203009822U (en) | Plugging structure of sealed cavity | |
| CN205719393U (en) | High pressure is shatter-proof pressure transducer | |
| CN207366336U (en) | A kind of corrosion device for test button fatigue mechanics performance test | |
| CN203849113U (en) | Simple low-pressure single tube pressure test tool | |
| CN202209499U (en) | Pipe stopper | |
| CN201322700Y (en) | Gas-oil separating device online-monitored by power transformer |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140312 Termination date: 20170826 |