CN203448113U - Energy-saving efficient self-cleaning polymerization device - Google Patents
Energy-saving efficient self-cleaning polymerization device Download PDFInfo
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- CN203448113U CN203448113U CN201320524974.0U CN201320524974U CN203448113U CN 203448113 U CN203448113 U CN 203448113U CN 201320524974 U CN201320524974 U CN 201320524974U CN 203448113 U CN203448113 U CN 203448113U
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Abstract
The utility model relates to an energy-saving efficient self-cleaning polymerization device which is composed of a tubular reactor and a self-cleaning strengthened heat transfer device, wherein the self-cleaning strengthened heat transfer device mainly comprises rotors, a middle support frame, a backwater-side hanging member, a limiting member and lifting hook hanging members; the middle support frame is used for supporting each section of rotor string to enhance the rigidity of a rotary shaft and the self-centering effect of the rotors and prolong the service life of the whole device. A positioning hinge pin of each lifting hook hanging member is matched with a positioning hole of the adjacent lifting hook hanging member, the lifting hook hanging members at the end parts of multiple tubes form a whole connection structure for sure, and the axial tensile strength of the single lifting hook hanging member is improved. A lifting hook, a hollow shaft and a positioning recess of each lifting hook hanging member are positioned in the tube so as to reduce the fluid impact as well as the fluid resistance. The device provided by the utility model enhances sufficient mixing of the reaction materials and quickly releases the heat of a polymerization reaction; moreover, the device also has a self-cleaning effect, solves the problem of kettle sticking, improves the product quality and production efficiency and avoids the shortcomings of the traditional production mode.
Description
Technical field
The present invention relates to a kind of process units of polymerization technique, be specifically related to a kind of energy-conservation, efficient, automatically cleaning polyplant.
Background technology
Adopt the product of polymerisation processing and manufacturing to have a lot, the production of PVC of take is example, and the production of PVC mainly contains two kinds of preparation technologies, the one, carbide; The 2nd, ethylene process, primary raw material is oil.On international market, the production of PVC mainly be take ethylene process as main, and domestic rich coal, the endowment of resources oil-poor, weak breath of being subject to limits, and mainly take carbide as main, and carbide accounts for the more than 70% of China PVC aggregated capacity.According to practical experience, in calcium carbide (CaC2) legal system, get in the production of PVC, there will be sticky still problem in various degree.Sticky still is that polymer forms dirt at polymeric kettle inwall, can cause heat transfer coefficient to decline, thereby affect reaction, carries out, and reduces output; Stripping, dry run discharging difficulty; Wall dirt is sneaked into and in finished product, is reduced the series of problems such as polyvinyl chloride resin quality.This not only affects autocontrol performance, reduction production capacity and the utilization rate of equipment and installations of polymeric kettle, affect product quality, cleaning polymeric kettle has also increased labour cost, and cause the harm problem of vinyl chloride (VCM) to clear still personnel, having larger potential safety hazard, is a problem of the urgent solution of people all the time.
In early days, people mainly adopt small-sized polymerization kettle to produce polyvinyl chloride resin, for keeping the normal heat transfer of polymeric kettle and stirring, run well, and adopt the clear method of 1 still 1, so time-consuming taking a lot of work.Afterwards, the external method of spraying the clear still of wall that adopts, was used giant, with the water under high pressure of 30MPa, from manhole, sprayed, and to remove sticky wall thing in still, reduced artificial clear still number of times.At present, adopt anti-fouling agent to solve problem, by reduce or eliminate sticky still problem to still wall spraying anti-fouling agent more.But also there is following problem in it:
1. the viscosity fastness of anti-stick coating is low, easily sneaks in product, reduces the purity of product, and affects the effect of antitack agent.
2. anti oxidation time is not enough, can make antitack agent lose efficacy in advance, causes product quality to decline.
3. colour cast problem, polymerization process floating coat thing can be abraded to be fallen in still, and dark anti-fouling agent can pollute resin (as " American Red ”,“ Britain is blue "), and therefore pollutes resin and make the partially red or partially blue color and luster that affects goods of resin.
4. operating difficulties while using, needs hand spray, and cannot guarantee uniformity and the integrality of spraying.
In order to change above-mentioned deficiency, the present invention proposes a kind of efficient energy-saving automatically cleaning polyplant.
Summary of the invention
The object of the invention is to design a kind of efficient energy-saving automatically cleaning polyplant, abandoned and usingd the method for conventional polymeric still as polymerizing reactor, adopt shell and tube reactor as reaction unit, and in tubulation, add rotator type cleaning and heat-transfer enhancing device, the abundant mixing of strengthening reaction mass, and the heat of polymerisation is discharged fast, cooling tube side polymer material, can also play automatic cleaning action, solve sticky still problem, improve quality and the production efficiency of product, thus all drawbacks of having avoided traditional mode of production mode to bring.
The present invention is that the technical scheme that addresses the above problem employing is: a kind of efficient energy-saving automatically cleaning polyplant, consists of shell and tube reactor and a kind of rotator type cleaning and heat-transfer enhancing device, shell and tube reactor is comprised of end socket, tubulation, cylindrical shell, deflection plate and tube sheet, and adopts conventional project organization and assembly relation, cleaning and heat-transfer enhancing device mainly comprises rotor, intermediate support beam, backwater end suspension member, locating part and suspension hook suspension member, the end facing water of tubulation is provided with suspension hook suspension member, the backwater end of tubulation is provided with backwater end suspension member, rotating shaft two ends are fixedly supported on suspension member by locating part, rotating shaft is by the axis hole of rotor, the hollow shaft axis hole of intermediate support beam and the axis hole of locating part, in tubulation, place a plurality of rotors, rotor is arranged in groups and is enclosed within rotating shaft, intermediate support beam is between every group of last rotor and locating part, Rotor terminal coordinates with intermediate support beam front end, locating part front end coordinates with intermediate support beam end, the blade external diameter of intermediate support beam is less than tubulation internal diameter but is greater than rotor diameter, be used for supporting every section of rotor string, strengthen the rigidity of rotating shaft and rotor from centering effect, thereby the service life of the even whole device of Extending Rotor.The stopper slot of suspension hook suspension member coordinates with tubulation end, thereby plays the fixedly effect of suspension member for limiting moving radially of suspension member, plays the effect that axially fastens cleaning and heat-transfer enhancing device simultaneously; The alignment pin of suspension hook suspension member matches with the locating hole of adjacent suspension hook suspension member, the suspension hook suspension member that guarantees many tubulation ends presents Integral connection structure, strengthen the axial tensile strength of single suspension hook suspension member, further limit in addition moving radially and circumferentially rotating of suspension hook suspension member.The positioning concave stations of suspension hook suspension member matches with the end of locating part, and the axial limiting of being convenient to locating part is fixed, and reduces the contact-making surface between locating part and fluid, reduces fluid resistance; The suspension hook of suspension hook suspension member, hollow shaft and positioning concave stations are positioned at tubulation, can reduce the impact to tubulation porch fluid, thereby greatly reduce fluid resistance.
Reaction mass enters tube side through tube side entrance, and the product of polymerisation enters next step operation through tube side outlet; The fluid thrust of reaction mass can be rotated by rotor driven, and rotatablely moving of rotor can be accelerated the even mixing of each reaction mass, makes polymerisation more thorough, improves the reaction efficiency of polymerisation; And the augmentation of heat transfer effect through cleaning and heat-transfer enhancing device, before polymerisation, can absorb fast the hot fluid heat of shell side entrance inflow to reaction temperature, the cold fluid that after reaction, shell side inlet streams enters absorbs the heat of polymerisation fast, the cold fluid absorbing after heat flows out through shell side outlet, is convenient to proceeding of reaction.Due to the automatic cleaning action of cleaning and heat-transfer enhancing device, fluid is no longer sticked on tube wall, but along with the screw of fluid constantly moves ahead, thereby solved the sticky still problem of traditional handicraft, improved the quality of product.
A kind of efficient energy-saving automatically cleaning of the present invention polyplant, rotor is the forms such as helical-blade rotor, fluting helical-blade rotor or the crossed combined rotor of blade rotation direction.
A kind of efficient energy-saving automatically cleaning of the present invention polyplant, the blade number that intermediate support beam distributes along hollow shaft circumferencial direction be two, three or more.
A kind of efficient energy-saving automatically cleaning of the present invention polyplant, backwater end suspension member is the forms such as suspension hook suspension member, twisted strip type suspension member, open-type hanging part or low flow-resistance quick-mounting hanger.
A kind of efficient energy-saving automatically cleaning of the present invention polyplant, suspension hook suspension member along the equally distributed suspension hook number of hollow shaft circumferencial direction be two, three or more.
A kind of efficient energy-saving automatically cleaning of the present invention polyplant, the alignment pin of suspension hook suspension member and locating hole cross section are circle, ellipse or polygon.
A kind of efficient energy-saving automatically cleaning of the present invention polyplant, the rotor whole string that can join end to end is threaded onto in rotating shaft, and rotating shaft can be the pole of rigidity, can be also flexible tightrope; Also can be divided into identical or different some groups of rotor quantity by locating part, rotor is evenly rotated.
A kind of efficient energy-saving automatically cleaning of the present invention polyplant, rotor, intermediate support beam, backwater end suspension member, locating part and suspension hook suspension member are by macromolecular material, polymer-based composite, metal or ceramic material.
Beneficial effect of the present invention is: 1, the operation power of rotor comes from the fluid thrust of liquid reactants, does not need additionally to add power set; 2, the fluid thrust of reaction mass can be rotated by rotor driven, and rotatablely moving of rotor can be accelerated the even mixing of each reaction mass, makes polymerisation more thorough, improves the reaction efficiency of polymerisation; 3, the augmentation of heat transfer effect of process cleaning and heat-transfer enhancing device, before polymerisation, can absorb fast shell side heat to reaction temperature, after reaction, the heat of polymerisation is discharged fast, the shell side cooling fluid of flowing through, further absorb the heat of tube side polymerisation, be convenient to proceeding of reaction; 4, due to the automatic cleaning action of cleaning and heat-transfer enhancing device, make fluid no longer stick on tube wall, but along with the screw of fluid constantly moves ahead, with regard to having avoided, because of the heat transfer coefficient that sticky still produces, decline like this, thereby solved the sticky still problem of traditional handicraft, avoided the use of anti-fouling agent, saved production cost, and improved the quality of products to a certain extent.
Accompanying drawing explanation
Fig. 1 is the assembling schematic diagram of a kind of efficient energy-saving automatically cleaning of the present invention polyplant;
Fig. 2 is the cleaning and heat-transfer enhancing device assembling schematic diagram of a kind of efficient energy-saving automatically cleaning of the present invention polyplant;
Fig. 3 is the rotor schematic three dimensional views of a kind of efficient energy-saving automatically cleaning of the present invention polyplant;
Fig. 4 is the intermediate support beam schematic three dimensional views of a kind of efficient energy-saving automatically cleaning of the present invention polyplant;
Fig. 5 is the backwater end suspension member schematic three dimensional views of a kind of efficient energy-saving automatically cleaning of the present invention polyplant;
Fig. 6 is the suspension hook suspension member schematic three dimensional views of a kind of efficient energy-saving automatically cleaning of the present invention polyplant.
In figure, 1-tube side entrance, 2-end socket, the outlet of 3-shell side, 4-tubulation, 5-cylindrical shell, 6-rotor, 7-intermediate support beam, 7-1-blade, 7-2-hollow shaft, 8-backwater end suspension member, 9-locating part, the outlet of 10-tube side, 11-shell side entrance, 12-suspension hook suspension member, 12-1-alignment pin, 12-2-stopper slot, 12-3-suspension hook, 12-4-hollow shaft, 12-5-positioning concave stations, 12-6-locating hole, 13-deflection plate, 14-rotating shaft, 15-tube sheet.
The specific embodiment
As shown in Figure 1, a kind of implementation method of a kind of efficient energy-saving automatically cleaning polyplant the present invention relates to, this device consists of shell and tube reactor and a kind of rotator type cleaning and heat-transfer enhancing device, shell and tube reactor is comprised of end socket 2, tubulation 4, cylindrical shell 5, deflection plate 13 and tube sheet 15, and adopts conventional project organization and assembly relation, cleaning and heat-transfer enhancing device mainly comprises rotor 6, intermediate support beam 7, backwater end suspension member 8, locating part 9 and suspension hook suspension member 12, the end facing water of tubulation is provided with suspension hook suspension member 12, tubulation backwater end is provided with backwater end suspension member 8, rotating shaft 14 two ends are fixedly supported on suspension member by locating part 9, rotating shaft 14 is by the axis hole of rotor 6, the hollow shaft 7-2 axis hole of intermediate support beam 7 and the axis hole of locating part 9, a plurality of rotors 6 of the interior placement of tubulation 4, rotor 6 is arranged in groups and is enclosed within rotating shaft 14, intermediate support beam 7 is between every group of last rotor 6 and locating part 9, rotor 6 ends coordinate with intermediate support beam 7 front ends, locating part 9 front ends coordinate with intermediate support beam 7 ends, the blade 7-1 external diameter of intermediate support beam 7 is less than tubulation 4 internal diameters but is greater than rotor 6 external diameters, be used for supporting every section of rotor string, strengthen the rigidity of rotating shaft 14 and rotor 6 from centering effect, thereby the service life of the even whole device of Extending Rotor 6, the stopper slot 12-2 of suspension hook suspension member 12 coordinates with tubulation 4 ends, thereby plays the fixedly effect of suspension member for limiting moving radially of suspension member, plays the effect that axially fastens cleaning and heat-transfer enhancing device simultaneously, the alignment pin 12-1 of suspension hook suspension member 12 matches with the locating hole 12-6 of adjacent suspension hook suspension member 12, the suspension hook suspension member 12 that guarantees many tubulation 4 ends presents Integral connection structure, strengthen the axial tensile strength of single suspension hook suspension member 12, further limit in addition moving radially and circumferentially rotating of suspension hook suspension member 12.The positioning concave stations 12-5 of suspension hook suspension member 12 matches with the end of locating part 9, and the axial limiting of being convenient to locating part 9 is fixed, and reduces the contact-making surface between locating part 9 and fluid, reduces fluid resistance; Suspension hook 12-3, hollow shaft 12-4 and the positioning concave stations 12-5 of suspension hook suspension member 12 are positioned at tubulation, can reduce the impact to tubulation porch fluid, thereby greatly reduce fluid resistance.
In the present invention, reaction mass enters tube side through tube side entrance 1, and the product of polymerisation enters next step operation through tube side outlet 10; The fluid thrust of reaction mass can be rotated by rotor driven 6, and rotatablely moving of rotor 6 can be accelerated the even mixing of each reaction mass, makes polymerisation more thorough, improves the reaction efficiency of polymerisation; And the augmentation of heat transfer effect through cleaning and heat-transfer enhancing device, before polymerisation, can absorb fast the hot fluid heat of shell side entrance 11 inflows to reaction temperature, the cold fluid that after reaction, shell side entrance 11 flows into absorbs the heat of polymerisation fast, the cold fluid absorbing after heat flows out through shell side outlet 3, is convenient to proceeding of reaction.Due to the automatic cleaning action of cleaning and heat-transfer enhancing device, fluid is no longer sticked on tube wall, but along with the screw of fluid constantly moves ahead, thereby solved the sticky still problem of traditional handicraft.
Claims (9)
1. an efficient energy-saving automatically cleaning polyplant, by shell and tube reactor and a kind of cleaning and heat-transfer enhancing device, formed, it is characterized in that: shell and tube reactor is comprised of end socket, tubulation, cylindrical shell, deflection plate and tube sheet, and adopt conventional project organization and assembly relation, cleaning and heat-transfer enhancing device mainly comprises rotor, intermediate support beam, backwater end suspension member, locating part and suspension hook suspension member, the end facing water of tubulation is provided with suspension hook suspension member, tubulation backwater end is provided with backwater end suspension member, rotating shaft two ends are fixedly supported on suspension member by locating part, rotating shaft is by the axis hole of rotor, the hollow shaft axis hole of intermediate support beam and the axis hole of locating part, in tubulation, place a plurality of rotors, rotor is arranged in groups and is enclosed within rotating shaft, intermediate support beam is between every group of last rotor and locating part, Rotor terminal coordinates with intermediate support beam front end, locating part front end coordinates with intermediate support beam end, the maximum outside diameter of intermediate support beam is less than heat exchanger tube internal diameter but is greater than rotor diameter, the stopper slot of suspension hook suspension member coordinates with tubulation end, the alignment pin of suspension hook suspension member matches with the locating hole of adjacent suspension hook suspension member, the positioning concave stations of suspension hook suspension member matches with the end of locating part, and the suspension hook of suspension hook suspension member, hollow shaft and positioning concave stations are positioned at tubulation.
2. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: rotor is helical-blade rotor, fluting helical-blade rotor or the crossed combined rotor of blade rotation direction.
3. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: the blade number that intermediate support beam distributes along hollow shaft circumferencial direction is a plurality of.
4. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: backwater end suspension member is suspension hook suspension member, twisted strip type suspension member, open-type hanging part or low flow-resistance quick-mounting hanger.
5. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: suspension hook suspension member is a plurality of along the equally distributed suspension hook number of hollow shaft circumferencial direction.
6. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: the alignment pin of suspension hook suspension member and locating hole cross sectional shape are circular, ellipse or polygon.
7. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: the hollow shaft two ends of described rotor are provided with coaxial configuration, the coaxial configuration head and the tail combination of two adjacent rotor, has realized the axial location between rotor; The hollow shaft coaxial configuration of rotor can be ball-and-socket mode, circular cone mode, buckle mode or universal joint mode.
8. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: the rotor whole string that can join end to end is threaded onto in rotating shaft, the pole of rotating shaft rigidity, or flexible tightrope; Or be divided into identical or different some groups of rotor quantity by locating part.
9. according to a kind of efficient energy-saving automatically cleaning polyplant described in claim 1 time, it is characterized in that: rotor, intermediate support beam, backwater end suspension member, locating part and suspension hook suspension member are by macromolecular material, polymer-based composite, metal or ceramic material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320524974.0U CN203448113U (en) | 2013-08-27 | 2013-08-27 | Energy-saving efficient self-cleaning polymerization device |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201320524974.0U CN203448113U (en) | 2013-08-27 | 2013-08-27 | Energy-saving efficient self-cleaning polymerization device |
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| CN203448113U true CN203448113U (en) | 2014-02-26 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103406087A (en) * | 2013-08-27 | 2013-11-27 | 北京化工大学 | Energy-saving and high-efficiency self-cleaning polymerization process and device |
| CN103432981A (en) * | 2013-08-27 | 2013-12-11 | 北京化工大学 | Energy-saving high-efficiency self-cleaning polymerizing device |
| CN104154810A (en) * | 2014-08-07 | 2014-11-19 | 北京化工大学 | Built-in self-pre-tightening hanging piece of heat exchange tube |
| CN115449011A (en) * | 2022-10-09 | 2022-12-09 | 河北昊泽化工有限公司 | Synthesis method and synthesis equipment of high-solid cement modified acrylic emulsion |
-
2013
- 2013-08-27 CN CN201320524974.0U patent/CN203448113U/en not_active Withdrawn - After Issue
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103406087A (en) * | 2013-08-27 | 2013-11-27 | 北京化工大学 | Energy-saving and high-efficiency self-cleaning polymerization process and device |
| CN103432981A (en) * | 2013-08-27 | 2013-12-11 | 北京化工大学 | Energy-saving high-efficiency self-cleaning polymerizing device |
| WO2015027613A1 (en) * | 2013-08-27 | 2015-03-05 | 北京化工大学 | Self-cleaning polymerization apparatus and process |
| CN103432981B (en) * | 2013-08-27 | 2015-05-27 | 北京化工大学 | Energy-saving high-efficiency self-cleaning polymerizing device |
| CN104154810A (en) * | 2014-08-07 | 2014-11-19 | 北京化工大学 | Built-in self-pre-tightening hanging piece of heat exchange tube |
| CN115449011A (en) * | 2022-10-09 | 2022-12-09 | 河北昊泽化工有限公司 | Synthesis method and synthesis equipment of high-solid cement modified acrylic emulsion |
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Granted publication date: 20140226 Effective date of abandoning: 20150527 |
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