CN203425818U - Cooling device of parallel reactor - Google Patents
Cooling device of parallel reactor Download PDFInfo
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- CN203425818U CN203425818U CN201320447543.9U CN201320447543U CN203425818U CN 203425818 U CN203425818 U CN 203425818U CN 201320447543 U CN201320447543 U CN 201320447543U CN 203425818 U CN203425818 U CN 203425818U
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- cooling
- reactor
- kettle
- oil
- magnetically
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Abstract
The utility model discloses a cooling device of a parallel reactor. The cooling device comprises a magnetic stirring water-cooling machine and oil cooling machines for reaction kettles, wherein the magnetic stirring water-cooling machine comprises a cooling water inlet and a cooling water outlet, each oil cooling machine for the reaction kettles comprises a cooling oil inlet and a cooling oil outlet, the lower end of a cooling coil is communicated with the cooling oil outlet, the upper end of the cooling coil is communicated with the cooling oil inlet, an electronic control stop valve is arranged between the lower end of the cooling coil and the cooling oil outlet, and both the cooling water inlet and the cooling water outlet are communicated with a magnetic stirrer. The cooling device of the parallel reactor is used for cooling magnetic driving reaction kettles, each magnetic driving reaction kettle is provided with one oil cooling machine of the reaction kettle for cooling substances in the reaction kettles independently, and the on and off of the electronic control stop valve is utilized for controlling; one magnetic stirring water-cooling machine is arranged for cooling the magnetic stirrers uninterruptedly, therefore, compared with the prior art, the cooling device of the parallel reactor can preferably achieve the experimental purposes.
Description
Technical field
The utility model relates to a kind of cooling device of parallel reactor.
Background technology
Parallel reactor (full-automatic multi-functional combined high pressure polymerization reaction system) is a plurality of instruments that react platform of collection reaction system and computer control system and data processing one, is the powerful measure that efficient, low-cost resin is researched and developed.But the work compound ability of a plurality of reaction platforms of the parallel reactor of prior art a little less than, complicated operation, be difficult for to realize.According to requirement of experiment, the interior material of the cooling magnetically-actuated reactor of needs and incessantly cooling magnetic stirring apparatus.
Therefore, need a kind of cooling device of parallel reactor to address the above problem.
Utility model content
Utility model object: for problem and the defect of above-mentioned existence, the utility model provides a kind of cooling device that can better realize the cooling parallel reactor of each reaction platform.
Technical scheme: for reaching above-mentioned utility model object, the cooling device of parallel reactor of the present utility model by the following technical solutions:
A kind of cooling device of parallel reactor, described parallel reactor comprises a plurality of magnetically-actuated reactors, described in each, magnetically-actuated reactor includes a magnetic stirring apparatus and a cooling coil, described cooling coil is arranged in described magnetically-actuated reactor, described cooling device comprises magnetic agitation cooling-water machine and reactor Cool oil machine, described magnetic agitation cooling-water machine comprises cooling water intake and cooling water outlet, and described reactor Cool oil machine comprises cold oil oil-in and cold oil oil-out; The lower end of described cooling coil is communicated with described cold oil oil-out, and the upper end of described cooling coil is communicated with described cold oil oil-in, between the lower end of described cooling coil and described cold oil oil-out, is provided with electric-control stop valve; Described cooling water intake and cooling water outlet are all communicated with described magnetic stirring apparatus.
Further, described magnetically-actuated reactor comprises magnetic stirring apparatus, kettle, kettle cover, shaft, paddle and cooling coil, described kettle is drum-shaped, described paddle is arranged in described kettle, the opening part of described kettle is provided with described kettle cover, and described kettle cover and described kettle are tightly connected;
Described magnetic stirring apparatus is fixed on the outer middle side part of described kettle cover, one end of described shaft is arranged on the middle inside of described kettle cover, the other end of described shaft is provided with described paddle and stretches into described kettle, and stretching into cover on the described shaft of described kettle has described cooling coil.
Further, described magnetically-actuated reactor also comprises sleeve pipe, described magnetic stirring apparatus is connected by rotating shaft with kettle cover, described sleeve pipe is arranged between described magnetic stirring apparatus and kettle cover and is enclosed within described rotating shaft, one end side surface and the other end side of described sleeve pipe are respectively arranged with opening, and described cooling water intake is connected respectively two openings with cooling water outlet.
Further, described magnetically-actuated reactor also comprises cooling liquid inlet and cooling liquid outlet, and described cooling liquid inlet and cooling liquid outlet are all arranged on described kettle cover, and described cooling liquid inlet and cooling liquid outlet are connected respectively the two ends of described cooling coil.
Beneficial effect: the cooling device of parallel reactor of the present utility model is for carrying out cooling to magnetically-actuated reactor, reactor Cool oil machine of each magnetically-actuated reactor outfit carries out cooling independently to material in reactor, utilize the through and off of electric-control stop valve to control; Be equipped with a magnetic agitation cooling-water machine and magnetic stirring apparatus carried out incessantly cooling, with respect to prior art, can have and better complete experiment purpose.
Accompanying drawing explanation
Fig. 1 is the structural representation of parallel reactor;
Fig. 2 is the structural representation of the cooling device of parallel reactor of the present utility model;
Fig. 3 is the stereogram of magnetically-actuated reactor;
Fig. 4 is the stereogram of magnetically-actuated reactor;
Fig. 5 is the cutaway view of magnetically-actuated reactor.
The specific embodiment
Below in conjunction with the drawings and specific embodiments, further illustrate the utility model, should understand these embodiment and only for the utility model is described, be not used in restriction scope of the present utility model, after having read the utility model, those skilled in the art all fall within the application's claims limited range to the modification of the various equivalent form of values of the present utility model.
Refer to shown in Fig. 1, the utility model discloses a kind of cooling device of parallel reactor, wherein, parallel reactor comprises a plurality of reactors, control and data processing equipment and servicing unit, each reactor includes cooling device, nitrogen pressure device and the cooling device of reactor device, parallel reactor, control with data processing equipment and comprise data processing equipment and Reaction Control Assembly, servicing unit comprises reactor table and computer table, and reactor and control and data processing equipment are separately positioned on reactor table and computer table.Preferably, the quantity of reactor device is 6.Six reactor devices are tested simultaneously.Wherein, reactor device comprises magnetically-actuated reactor.
Compared with prior art, parallel reactor of the present utility model has the following advantages: each reactor is tested simultaneously, every reactor is furnished with independent heating, stirring, pressure assembly, guarantee that each reaction independently carries out in similar and different temperature, pressure, mixing speed, accelerate the screening of experimental condition, the optimization of reaction condition.
Refer to shown in Fig. 2, the cooling device of parallel reactor of the present utility model, parallel reactor comprises a plurality of magnetically-actuated reactors, the quantity of preferred magnetically-actuated reactor is 6.Each magnetically-actuated reactor includes a magnetic stirring apparatus 102 and a cooling coil 106, and cooling coil 106 is arranged in magnetically-actuated reactor.Wherein, cooling device comprises magnetic agitation cooling-water machine and reactor Cool oil machine.Wherein, the model of magnetic agitation cooling-water machine is AC-0.6, and it is 20-30 ℃ that coolant temperature is set, and once setting, does not need to go adjusting again; Reactor Cool oil machine model is AJO-2, cold oil medium: WD-320 mineral type high temperature heat conductive oil, need to carry out temperature setting to cooling medium according to experiment.
Magnetic agitation cooling-water machine comprises cooling water intake and cooling water outlet, and reactor Cool oil machine comprises cold oil oil-in and cold oil oil-out; The lower end of cooling coil 106 is communicated with cold oil oil-out, and the upper end of cooling coil 106 is communicated with cold oil oil-in, between the lower end of cooling coil 106 and cold oil oil-out, is provided with electric-control stop valve 610; Cooling water intake and cooling water outlet are all communicated with magnetic stirring apparatus 102.
The cooling device of parallel reactor of the present utility model is cooling for magnetically-actuated reactor is carried out, and reactor Cool oil machine of each magnetically-actuated reactor outfit carries out cooling independently to material in reactor, utilize the through and off of electric-control stop valve to control; Be equipped with a magnetic agitation cooling-water machine and magnetic stirring apparatus carried out incessantly cooling, with respect to prior art, can have and better complete experiment purpose.
Wherein, the technical parameter of magnetically-actuated reactor:
| Project | Parameter |
| Volume | 1000ml |
| Design pressure | 20MPa |
| Operating pressure | 10Mpa |
| Design temperature | 350℃ |
| Operating temperature | 250℃ |
| Stirring motor power | 0.37KW/380V |
| Mixing speed | 0-600r/min is stepless adjustable |
| Temperature control precision | ±0.5℃ |
| Pressure controling precision | ±0.5％Fs |
| Velocity control accuracy | ±0.5％n N |
| Heating power | 2.5KW |
| Heater voltage | 220V |
Wherein, Fs refers to the full value journey of pressure sensor; n
nfor motor rated speed value.
The important technological parameters of parallel reactor (uniformity):
Wherein, Fs refers to the full value journey of pressure sensor; n
nfor motor rated speed value.
Refer to shown in Fig. 3, Fig. 4 and Fig. 5, magnetically-actuated reactor of the present utility model, comprise magnetic stirring apparatus 101, kettle 102, kettle cover 103, shaft 104, paddle 105 and cooling coil 106, kettle 102 is drum-shaped, paddle 105 is arranged in kettle 102, the opening part of kettle 102 is provided with kettle cover 103, and kettle cover 103 is tightly connected with kettle 102; Magnetic stirring apparatus 101 is fixed on the outer middle side part of kettle cover 103, one end of shaft 104 is arranged on the middle inside of kettle cover 103, the other end of shaft 104 is provided with paddle 105 and stretches into kettle 102, stretch into cover on the shaft 104 of kettle 102 and have cooling coil 106, the lower end of cooling coil 106 is import, and upper end is outlet.
Also comprise sleeve pipe 116, magnetic stirring apparatus 101 is connected by rotating shaft with kettle cover 103, and sleeve pipe 116 is arranged between magnetic stirring apparatus 101 and kettle cover 103 and is enclosed within rotating shaft, and an end side surface and the other end side of sleeve pipe 116 are respectively arranged with opening.
Kettle cover 103 is with bolts with kettle 102, and adopts metallic graphite carbon wound gasket to seal.Whipped form is that high moment of torsion magnetic couple stirs.Paddle 105 is folding oar, and blade is two of individual layers.
Also comprise cooling liquid inlet 161 and cooling liquid outlet 162, cooling liquid inlet 161 and cooling liquid outlet 162 are all arranged on kettle cover 103, and cooling liquid inlet 161 and cooling liquid outlet 162 are connected respectively the two ends of cooling coil 106.Preferably, cooling liquid inlet 161 connects the lower end of cooling coil 106, and cooling liquid outlet 162 connects the upper end of cooling coil 106, makes cooling fluid flow to upper end from the lower end of cooling coil 106, and cooling effect is better.
Also comprise dilution tunnel 107, sampling needle valve 171 and sample tap, be provided with dilution tunnel 107 in kettle 102, one end of dilution tunnel 107 is fixed on kettle cover 103, and the other end of dilution tunnel 107 stretches into kettle 102; Sample tap is arranged on the upper of kettle cover 103, sample tap and dilution tunnel 107 UNICOMs, and sample tap place is provided with sampling needle valve 171.
Also comprise air release mouth and air release needle valve 109, air release mouth is arranged on kettle cover 103, air release mouth and kettle 102 UNICOMs, and air release mouth place is provided with air release needle valve 109.
Also comprise vacuum orifice and vacuumize aciculiform valve 110, vacuum orifice is arranged on kettle cover 103, vacuum orifice and kettle 102 UNICOMs, and vacuum orifice place is provided with and vacuumizes aciculiform valve 110.
Also comprise filter 111, filter 111 is arranged between vacuum orifice and gas pressurized mouth 113.
Also comprise temperature transmitter 112, be provided with temperature transmitter 112 on kettle cover 103, the temperature element of temperature transmitter 112 is arranged in kettle 102.
Also comprise gas pressurized mouth 113, gas pressurized mouth 113 is arranged on vacuum orifice and vacuumizes between aciculiform valve 110.
Also comprise safety blasting sheet 114 and Pressure gauge 115, Pressure gauge 115 be arranged on kettle cover 103 and with kettle 102 UNICOMs, safety blasting sheet 114 and Pressure gauge 115 UNICOMs.
Described magnetically-actuated reactor also comprises relief valve connection 117, described relief valve connection 117 be arranged on described kettle cover 103 and with described kettle 102 UNICOMs.
Magnetically-actuated reactor of the present utility model, simple in structure, reaction effect is good, especially adopts cooling coil cooling to carrying out in reactor, and cooling effect is better.
Claims (4)
1. the cooling device of a parallel reactor, it is characterized in that: described parallel reactor comprises a plurality of magnetically-actuated reactors, described in each, magnetically-actuated reactor includes a magnetic stirring apparatus (102) and a cooling coil (106), described cooling coil (106) is arranged in described magnetically-actuated reactor, described cooling device comprises magnetic agitation cooling-water machine and reactor Cool oil machine, described magnetic agitation cooling-water machine comprises cooling water intake and cooling water outlet, and described reactor Cool oil machine comprises cold oil oil-in and cold oil oil-out; The lower end of described cooling coil (106) is communicated with described cold oil oil-out, the upper end of described cooling coil (106) is communicated with described cold oil oil-in, between the lower end of described cooling coil (106) and described cold oil oil-out, is provided with electric-control stop valve (610); Described cooling water intake and cooling water outlet are all communicated with described magnetic stirring apparatus (102).
2. the cooling device of parallel reactor as claimed in claim 1, it is characterized in that, described magnetically-actuated reactor comprises magnetic stirring apparatus (101), kettle (102), kettle cover (103), shaft (104), paddle (105) and cooling coil (106), described kettle (102) is drum-shaped, described paddle (105) is arranged in described kettle (102), the opening part of described kettle (102) is provided with described kettle cover (103), and described kettle cover (103) is tightly connected with described kettle (102);
Described magnetic stirring apparatus (101) is fixed on the outer middle side part of described kettle cover (103), one end of described shaft (104) is arranged on the middle inside of described kettle cover (103), the other end of described shaft (104) is provided with described paddle (105) and stretches into described kettle (102), and the upper cover of described shaft (104) that stretches into described kettle (102) has described cooling coil (106).
3. the cooling device of parallel reactor as claimed in claim 2, it is characterized in that, described magnetically-actuated reactor also comprises sleeve pipe (116), described magnetic stirring apparatus (101) is connected by rotating shaft with kettle cover (103), described sleeve pipe (116) is arranged between described magnetic stirring apparatus (101) and kettle cover (103) and is enclosed within described rotating shaft, one end side surface and the other end side of described sleeve pipe (116) are respectively arranged with opening, and described cooling water intake is connected respectively two openings with cooling water outlet.
4. the cooling device of parallel reactor as claimed in claim 2, it is characterized in that, described magnetically-actuated reactor also comprises cooling liquid inlet (161) and cooling liquid outlet (162), it is upper that described cooling liquid inlet (161) and cooling liquid outlet (162) are all arranged on described kettle cover (103), and described cooling liquid inlet (161) and cooling liquid outlet (162) are connected respectively the two ends of described cooling coil (106).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320447543.9U CN203425818U (en) | 2013-07-25 | 2013-07-25 | Cooling device of parallel reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320447543.9U CN203425818U (en) | 2013-07-25 | 2013-07-25 | Cooling device of parallel reactor |
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| Publication Number | Publication Date |
|---|---|
| CN203425818U true CN203425818U (en) | 2014-02-12 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320447543.9U Expired - Fee Related CN203425818U (en) | 2013-07-25 | 2013-07-25 | Cooling device of parallel reactor |
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|---|---|
| CN (1) | CN203425818U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103432979A (en) * | 2013-07-25 | 2013-12-11 | 无锡意凯自动化技术有限公司 | Cooling device of parallel reactor |
-
2013
- 2013-07-25 CN CN201320447543.9U patent/CN203425818U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103432979A (en) * | 2013-07-25 | 2013-12-11 | 无锡意凯自动化技术有限公司 | Cooling device of parallel reactor |
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| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140212 Termination date: 20150725 |
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| EXPY | Termination of patent right or utility model |