CN203425784U - Reaction kettle device - Google Patents

Reaction kettle device Download PDF

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Publication number
CN203425784U
CN203425784U CN201320447472.2U CN201320447472U CN203425784U CN 203425784 U CN203425784 U CN 203425784U CN 201320447472 U CN201320447472 U CN 201320447472U CN 203425784 U CN203425784 U CN 203425784U
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CN
China
Prior art keywords
kettle
reactor
valve
magnetically
actuated
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Expired - Fee Related
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CN201320447472.2U
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Chinese (zh)
Inventor
宋花江
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WUXI YIKAI AUTOMATION TECHNOLOGY Co Ltd
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WUXI YIKAI AUTOMATION TECHNOLOGY Co Ltd
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Priority to CN201320447472.2U priority Critical patent/CN203425784U/en
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Publication of CN203425784U publication Critical patent/CN203425784U/en
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Abstract

The utility model discloses a reaction kettle device which comprises a magnetic driving reaction kettle, a heater, a heater sleeve, a kettle support and a reaction kettle stand, wherein the magnetic driving reaction kettle is arranged at one side of the reaction kettle stand, is fixedly connected with the top of the reaction kettle stand and comprises a magnetic stirring apparatus, a kettle body, a kettle cover, a stirring shaft, a stirring paddle and a cooling coiled pipe; the kettle body is in a circular barrel shape; the stirring paddle is arranged in the kettle body; the kettle cover is arranged at an opening of the kettle body; the kettle cover is connected with the kettle body in a sealing way; the magnetic stirring apparatus is fixed in the middle of the outer side of the kettle cover; one end of the stirring shaft is arranged in the middle of the inner side of the kettle cover, and the other end of the stirring shaft is provided with the stirring paddle and extends into the kettle body; the cooling coiled pipe is arranged on the stirring shaft extending into the kettle body in a sheathed manner; the heater is arranged at the outer side of the kettle body in a sheathed manner; the heater sleeve and the kettle support are respectively arranged under the magnetic driving reaction kettle and are respectively articulated with the reaction kettle stand. The reaction kettle device is simple and reasonable in structure; the magnetic driving reaction kettle with good effects is adopted by the reaction kettle device, and the efficacy of the magnetic driving reaction kettle can be fully exerted.

Description

A kind of reactor device
Technical field
The utility model relates to a kind of reactor device.
Background technology
Existing reactor device, comprises magnetically-actuated reactor, and the core component magnetic driving equipment of magnetically-actuated reactor is a kind of transmission device that utilizes permanent-magnet material to carry out magnetic driver.Magnetic coupling utilizes magnet steel to see through the principle that stainless steel still can attract each other, and makes a capping and is fixedly connected with kettle, forms static seal chamber, effectively Leakage prevention.Magnet steel brick that a use permanent-magnet material is made is respectively established in seal closure inside and outside, and rotor shapes resembles a horseshoe magnet, and magnet projection two ends are respectively N, the S utmost point of magnet steel.Because magnet steel has, there is a natural attraction between the sexes, the characteristic of two like magnetic poles repel each other, and internal-external magnetic steel is located in direction of rotation mutually by magneticaction.When driven by motor outer steel rotor, interior magnetic steel rotor is followed and is made synchronous rotary together with mixing component, has realized stirring object.It is that by the structure of packing seal shaft that magnetic coupling has been abandoned gland sealed, adopt inside and outside magnet rotor with magnetic force, to see through the brand-new kind of drive of capping transmitting torque, in still, mixing component is completely at kettle static seal chamber internal rotating, do not stretch out kettle outside, thoroughly solved the leakage problem that packing seal cannot overcome, make in the state of reaction medium in absolute sealing, without any leakage and pollution.But the magnetically-actuated reactor layout of prior art is reasonable not, complex structure, cooling effect is also undesirable.
Therefore, need a kind of new reactor device.
Utility model content
Utility model object: for problem and the defect of above-mentioned existence, the utility model provides a kind of reactor device.
Technical scheme: for reaching above-mentioned utility model object, the utility model by the following technical solutions:
A kind of reactor device, comprise magnetically-actuated reactor, heater, heaters set, still holder and reactor frame, described magnetically-actuated reactor is arranged on a side of described reactor frame, and described magnetically-actuated reactor is fixedly connected with the top of described reactor frame
Described magnetically-actuated reactor comprises magnetic stirring apparatus, kettle, kettle cover, shaft, paddle and cooling coil, described kettle is drum-shaped, described paddle is arranged in described kettle, and the opening part of described kettle is provided with described kettle cover, and described kettle cover and described kettle are tightly connected;
Described magnetic stirring apparatus is fixed on the outer middle side part of described kettle cover, one end of described shaft is arranged on the middle inside of described kettle cover, the other end of described shaft is provided with described paddle and stretches into described kettle, and stretching into cover on the described shaft of described kettle has described cooling coil;
The outside cover of described kettle has described heater, and described heaters set and described still drag the below that is all arranged on described magnetically-actuated reactor, and described heaters set and still holder are all hinged with described reactor frame.
Further, described magnetically-actuated reactor also comprises sleeve pipe, described magnetic stirring apparatus is connected by rotating shaft with kettle cover, and described sleeve pipe is arranged between described magnetic stirring apparatus and kettle cover and is enclosed within described rotating shaft, and an end side surface and the other end side of described sleeve pipe are respectively arranged with opening.
Further, described magnetically-actuated reactor also comprises cooling liquid inlet and cooling liquid outlet, described cooling liquid inlet and cooling liquid outlet are all arranged on described kettle cover, described cooling liquid inlet and cooling liquid outlet are connected respectively the two ends of described cooling coil, described cooling liquid outlet place is provided with coolant return line, described cooling liquid inlet place is provided with cooling fluid inlet pipe, and described cooling fluid inlet pipe and coolant return line are all arranged in described reactor frame.
Further, described magnetically-actuated reactor also comprises dilution tunnel, sampling needle valve and sample tap, in described kettle, be provided with described dilution tunnel, one end of described dilution tunnel is fixed on described kettle cover, and the other end of described dilution tunnel stretches into described kettle; Described sample tap is arranged on the upper of described kettle cover, described sample tap and described dilution tunnel UNICOM, and described sample tap place is provided with described sampling needle valve.
Further, also comprise gas discharge tube and air release magnetic valve, described gas discharge tube and air release magnetic valve are all arranged in described reactor frame, described magnetically-actuated reactor also comprises air release mouth and air release needle valve, described air release mouth is arranged on described kettle cover, described air release mouth and described kettle UNICOM, described air release mouth place is provided with described air release needle valve, one end of described gas discharge tube connects described air release needle valve, and the other end of described gas discharge tube connects described air release magnetic valve.
Further, also comprise vacuum-pumping tube and vacuumize magnetic valve, described vacuum-pumping tube and vacuumize magnetic valve and be all arranged in described reactor frame, also comprise vacuum orifice and vacuumize aciculiform valve, described vacuum orifice is arranged on described kettle cover, described vacuum orifice and described kettle UNICOM, vacuumize aciculiform valve described in described vacuum orifice place is provided with, and vacuumizes aciculiform valve and vacuumize magnetic valve described in the two ends of described vacuum-pumping tube connect respectively.
Further, also comprise pressure regulation tube, add pressure electromagnetic valve, pressure electromagnetic valve for adjusting, pressurization reset valve and pressure reset valve, described pressure regulation tube, add pressure electromagnetic valve, pressure electromagnetic valve for adjusting, pressurization reset valve and pressure reset valve are all arranged in described reactor frame, described magnetically-actuated reactor also comprises gas pressurized mouth, described gas pressurized mouth is arranged on described vacuum orifice and vacuumizes between aciculiform valve, described pressure regulation tube is three-way pipe, three openings of described pressure regulation tube connect respectively described gas pressurized mouth, add pressure electromagnetic valve and pressure electromagnetic valve for adjusting, described adding described in being provided with between pressure electromagnetic valve and described pressure regulation tube, adds pressure electromagnetic valve, between described pressure electromagnetic valve for adjusting and described pressure regulation tube, be provided with described pressure reset valve.
Further, described magnetically-actuated reactor also comprises filter, and described filter is arranged between described vacuum orifice and described gas pressurized mouth.
Further, also comprise that explosion discharges connecting leg, described explosion discharges connecting leg and is arranged in described reactor frame, described magnetically-actuated reactor also comprises safety blasting sheet and Pressure gauge, described Pressure gauge be arranged on described kettle cover and with described kettle UNICOM, described safety blasting sheet and described Pressure gauge UNICOM, described explosion discharges connecting leg and connects described explosion releasing piece.Safety blasting sheet plays safety effect, and when reacting kettle inner pressure surpasses the threshold value of safety blasting sheet, rupture disk meeting explosion, discharges still internal pressure.
Further, also comprise safety valve connecting leg, described safety valve connecting leg is arranged in described reactor frame, described magnetically-actuated reactor also comprises relief valve connection, described relief valve connection be arranged on described kettle cover and with described kettle UNICOM, described safety valve connecting leg connects described safety valve and relief valve connection.Safety valve plays safety effect, when reacting kettle inner pressure is excessive, discharges unnecessary gas.
Beneficial effect: compared with prior art, the utlity model has following advantage: reactor apparatus structure of the present utility model is simple, rationally, adopts the good magnetically-actuated reactor of effect, can give full play to the usefulness of magnetically-actuated reactor.
Accompanying drawing explanation
Fig. 1 is the first stereogram of reactor device of the present utility model;
Fig. 2 is the second stereogram of reactor device of the present utility model;
Fig. 3 is the 3rd stereogram of reactor device of the present utility model;
Fig. 4 is the first stereogram of magnetically-actuated reactor;
Fig. 5 is the second stereogram of magnetically-actuated reactor;
Fig. 6 is the 3rd stereogram of magnetically-actuated reactor.
The specific embodiment
Below in conjunction with the drawings and specific embodiments, further illustrate the utility model, should understand these embodiment and only for the utility model is described, be not used in restriction scope of the present utility model, after having read the utility model, those skilled in the art all fall within the application's claims limited range to the modification of the various equivalent form of values of the present utility model.
Refer to shown in Fig. 1, Fig. 2, Fig. 3, Fig. 4, Fig. 5 and Fig. 6, reactor device of the present utility model, comprise magnetically-actuated reactor 1, heater, heaters set 2, still holder 3 and reactor frame 4, magnetically-actuated reactor 1 is arranged on a side of reactor frame 4, magnetically-actuated reactor 1 is fixedly connected with the top of reactor frame 4
Magnetically-actuated reactor 1 comprises magnetic stirring apparatus 101, kettle 102, kettle cover 103, shaft 104, paddle 105 and cooling coil 106, kettle 102 is drum-shaped, paddle 105 is arranged in kettle 102, the opening part of kettle 102 is provided with kettle cover 103, and kettle cover 103 is tightly connected with kettle 102;
Magnetic stirring apparatus 101 is fixed on the outer middle side part of kettle cover 103, one end of shaft 104 is arranged on the middle inside of kettle cover 103, the other end of shaft 104 is provided with paddle 105 and stretches into kettle 102, and stretching into cover on the shaft 104 of kettle 102 has cooling coil 106.
Magnetically-actuated reactor of the present utility model, simple in structure, reaction effect is good, especially adopts cooling coil cooling to carrying out in reactor, and cooling effect is better.
The outside cover having heaters of kettle 102, heaters set 2 and still drag 3 belows that are all arranged on magnetically-actuated reactor 1, and heaters set 2 and still holder 3 are all hinged with reactor frame 4.
Magnetically-actuated reactor 1 also comprises sleeve pipe 116, and sleeve pipe 116 is arranged between magnetic stirring apparatus 101 and kettle cover 103 and is enclosed within on shaft 104, and an end side surface and the other end side of sleeve pipe 116 are respectively arranged with opening.
Magnetically-actuated reactor 1 also comprises cooling liquid inlet 161 and cooling liquid outlet 162, cooling liquid inlet 161 and cooling liquid outlet 162 are all arranged on kettle cover 103, cooling liquid inlet 161 and cooling liquid outlet 162 are connected respectively the two ends of cooling coil 106, cooling liquid outlet 162 places are provided with coolant return line 504, cooling liquid inlet 161 places are provided with cooling fluid inlet pipe, and cooling fluid inlet pipe and coolant return line 504 are all arranged in reactor frame 4.
Magnetically-actuated reactor 1 also comprises dilution tunnel 107, sampling needle valve 171 and sample tap, is provided with dilution tunnel 107 in kettle 102, and one end of dilution tunnel 107 is fixed on kettle cover 103, and the other end of dilution tunnel 107 stretches into kettle 102; Sample tap is arranged on the upper of kettle cover 103, sample tap and dilution tunnel 107 UNICOMs, and sample tap place is provided with sampling needle valve 171.
Also comprise gas discharge tube 502 and air release magnetic valve 602, gas discharge tube 502 and air release magnetic valve 602 are all arranged in reactor frame 4, magnetically-actuated reactor 1 also comprises air release mouth and air release needle valve 109, air release mouth is arranged on kettle cover 103, air release mouth and kettle 102 UNICOMs, air release mouth place is provided with air release needle valve 109, one end of gas discharge tube 502 connects air release needle valve 109, and the other end of gas discharge tube 502 connects air release magnetic valve 602.
Also comprise vacuum-pumping tube 506 and vacuumize magnetic valve 603, vacuum-pumping tube 506 and vacuumize magnetic valve 603 and be all arranged in reactor frame 4, also comprise vacuum orifice and vacuumize aciculiform valve 110, vacuum orifice is arranged on kettle cover 103, vacuum orifice and kettle 102 UNICOMs, vacuum orifice place is provided with and vacuumizes aciculiform valve 110, and the two ends of vacuum-pumping tube 506 connect respectively and vacuumize aciculiform valve 110 and vacuumize magnetic valve 603.
Also comprise pressure regulation tube 505, add pressure electromagnetic valve 605, pressure electromagnetic valve for adjusting 606, pressurization reset valve 608 and pressure reset valve 609, pressure regulation tube 505, add pressure electromagnetic valve 605, pressure electromagnetic valve for adjusting 606, pressurization reset valve 608 and pressure reset valve 609 are all arranged in reactor frame 4, magnetically-actuated reactor 1 also comprises gas pressurized mouth 113, gas pressurized mouth 113 is arranged on vacuum orifice and vacuumizes between aciculiform valve 110, pressure regulation tube 505 is three-way pipe, three openings of pressure regulation tube 505 connect respectively gas pressurized mouth 113, add pressure electromagnetic valve 605 and pressure electromagnetic valve for adjusting 606, add and between pressure electromagnetic valve 605 and pressure regulation tube 505, be provided with pressurization reset valve 608, between pressure electromagnetic valve for adjusting 606 and pressure regulation tube 505, be provided with pressure reset valve 609.
Magnetically-actuated reactor 1 also comprises filter 111, and filter 111 is arranged between vacuum orifice and gas pressurized mouth 113.
Magnetically-actuated reactor 1 also comprises temperature transmitter 112, is provided with temperature transmitter 112 on kettle cover 103, and the temperature element of temperature transmitter 112 is arranged in kettle 102.
Also comprise that explosion discharges connecting leg 501, explosion discharges connecting leg 501 and is arranged in reactor frame 4, magnetically-actuated reactor 1 also comprises safety blasting sheet 114 and Pressure gauge 115, Pressure gauge 115 be arranged on kettle cover 103 and with kettle 102 UNICOMs, safety blasting sheet 114 and Pressure gauge 115 UNICOMs, explosion discharges connecting leg 501 and connects explosion releasing piece 114.Safety blasting sheet plays safety effect, and when reacting kettle inner pressure surpasses the threshold value of safety blasting sheet, rupture disk meeting explosion, discharges still internal pressure.
Also comprise safety valve connecting leg 503, described safety valve connecting leg 503 is arranged in described reactor frame 4, magnetically-actuated reactor 1 also comprises relief valve connection 117, relief valve connection 117 be arranged on kettle cover 103 and with kettle 102 UNICOMs, safety valve connecting leg 503 connection safety valves 601 and relief valve connection 117.Safety valve plays safety effect, when reacting kettle inner pressure is excessive, discharges unnecessary gas.Safety blasting sheet and safety valve play double shield effect, the safety of effective guarantee reactor.
Reactor device of the present utility model, rational in infrastructure, reaction effect is good.Reactor apparatus structure of the present utility model is simple, rationally, adopts the good magnetically-actuated reactor of effect, can give full play to the usefulness of magnetically-actuated reactor.

Claims (10)

1. a reactor device, it is characterized in that, comprise magnetically-actuated reactor (1), heater, heaters set (2), still holder (3) and reactor frame (4), described magnetically-actuated reactor (1) is arranged on a side of described reactor frame (4), described magnetically-actuated reactor (1) is fixedly connected with the top of described reactor frame (4)
Described magnetically-actuated reactor (1) comprises magnetic stirring apparatus (101), kettle (102), kettle cover (103), shaft (104), paddle (105) and cooling coil (106), described kettle (102) is drum-shaped, described paddle (105) is arranged in described kettle (102), the opening part of described kettle (102) is provided with described kettle cover (103), and described kettle cover (103) is tightly connected with described kettle (102);
Described magnetic stirring apparatus (101) is fixed on the outer middle side part of described kettle cover (103), one end of described shaft (104) is arranged on the middle inside of described kettle cover (103), the other end of described shaft (104) is provided with described paddle (105) and stretches into described kettle (102), and the upper cover of described shaft (104) that stretches into described kettle (102) has described cooling coil (106);
The outside cover of described kettle (102) has described heater, described heaters set (2) and described still drag (3) to be all arranged on the below of described magnetically-actuated reactor (1), and described heaters set (2) and still holder (3) are all hinged with described reactor frame (4).
2. reactor device as claimed in claim 1, it is characterized in that: described magnetically-actuated reactor (1) also comprises sleeve pipe (116), described magnetic stirring apparatus (101) is connected by rotating shaft with kettle cover (103), described sleeve pipe (116) is arranged between described magnetic stirring apparatus (101) and kettle cover (103) and is enclosed within described rotating shaft, and an end side surface and the other end side of described sleeve pipe (116) are respectively arranged with opening.
3. reactor device as claimed in claim 1, it is characterized in that: described magnetically-actuated reactor (1) also comprises cooling liquid inlet (161) and cooling liquid outlet (162), described cooling liquid inlet (161) and cooling liquid outlet (162) are all arranged on described kettle cover (103), described cooling liquid inlet (161) and cooling liquid outlet (162) are connected respectively the two ends of described cooling coil (106), described cooling liquid outlet (162) locates to be provided with coolant return line (504), described cooling liquid inlet (161) locates to be provided with cooling fluid inlet pipe, described cooling fluid inlet pipe and coolant return line (504) are all arranged in described reactor frame (4).
4. reactor device as claimed in claim 1, it is characterized in that: described magnetically-actuated reactor (1) also comprises dilution tunnel (107), sampling needle valve (171) and sample tap, in described kettle (102), be provided with described dilution tunnel (107), it is upper that one end of described dilution tunnel (107) is fixed on described kettle cover (103), and the other end of described dilution tunnel (107) stretches into described kettle (102); Described sample tap is arranged on the upper of described kettle cover (103), described sample tap and described dilution tunnel (107) UNICOM, and described sample tap place is provided with described sampling needle valve (171).
5. reactor device as claimed in claim 1, it is characterized in that: also comprise gas discharge tube (502) and air release magnetic valve (602), described gas discharge tube (502) and air release magnetic valve (602) are all arranged in described reactor frame (4), described magnetically-actuated reactor (1) also comprises air release mouth and air release needle valve (109), described air release mouth is arranged on described kettle cover (103), described air release mouth and described kettle (102) UNICOM, described air release mouth place is provided with described air release needle valve (109), one end of described gas discharge tube (502) connects described air release needle valve (109), the other end of described gas discharge tube (502) connects described air release magnetic valve (602).
6. reactor device as claimed in claim 1, it is characterized in that: also comprise vacuum-pumping tube (506) and vacuumize magnetic valve (603), described vacuum-pumping tube (506) and vacuumize magnetic valve (603) and be all arranged in described reactor frame (4), also comprise vacuum orifice and vacuumize aciculiform valve (110), described vacuum orifice is arranged on described kettle cover (103), described vacuum orifice and described kettle (102) UNICOM, described in being provided with, described vacuum orifice place vacuumizes aciculiform valve (110), described in the two ends of described vacuum-pumping tube (506) connect respectively, vacuumize aciculiform valve (110) and vacuumize magnetic valve (603).
7. reactor device as claimed in claim 6, it is characterized in that, also comprise pressure regulation tube (505), add pressure electromagnetic valve (605), pressure electromagnetic valve for adjusting (606), pressurization reset valve (608) and pressure reset valve (609), described pressure regulation tube (505), add pressure electromagnetic valve (605), pressure electromagnetic valve for adjusting (606), pressurization reset valve (608) and pressure reset valve (609) are all arranged in described reactor frame (4), described magnetically-actuated reactor (1) also comprises gas pressurized mouth (113), described gas pressurized mouth (113) is arranged on described vacuum orifice and vacuumizes between aciculiform valve (110), described pressure regulation tube (505) is three-way pipe, three openings of described pressure regulation tube (505) connect respectively described gas pressurized mouth (113), add pressure electromagnetic valve (605) and pressure electromagnetic valve for adjusting (606), described adding between pressure electromagnetic valve (605) and described pressure regulation tube (505), is provided with described pressurization reset valve (608), between described pressure electromagnetic valve for adjusting (606) and described pressure regulation tube (505), be provided with described pressure reset valve (609).
8. reactor device as claimed in claim 7, is characterized in that, described magnetically-actuated reactor (1) also comprises filter (111), and described filter (111) is arranged between described vacuum orifice and described gas pressurized mouth (113).
9. reactor device as claimed in claim 1, it is characterized in that, also comprise that explosion discharges connecting leg (501), described explosion discharges connecting leg (501) and is arranged in described reactor frame (4), described magnetically-actuated reactor (1) also comprises safety blasting sheet (114) and Pressure gauge (115), described Pressure gauge (115) be arranged on described kettle cover (103) upper and with described kettle (102) UNICOM, described safety blasting sheet (114) and described Pressure gauge (115) UNICOM, described explosion discharges connecting leg (501) and connects described explosion releasing piece (114).
10. reactor device as claimed in claim 1, it is characterized in that, also comprise safety valve connecting leg (503), described safety valve connecting leg (503) is arranged in described reactor frame (4), described magnetically-actuated reactor (1) also comprises relief valve connection (117), described relief valve connection (117) be arranged on described kettle cover (103) upper and with described kettle (102) UNICOM, described safety valve connecting leg (503) connects described safety valve (601) and relief valve connection (117).
CN201320447472.2U 2013-07-25 2013-07-25 Reaction kettle device Expired - Fee Related CN203425784U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201320447472.2U CN203425784U (en) 2013-07-25 2013-07-25 Reaction kettle device

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Application Number Priority Date Filing Date Title
CN201320447472.2U CN203425784U (en) 2013-07-25 2013-07-25 Reaction kettle device

Publications (1)

Publication Number Publication Date
CN203425784U true CN203425784U (en) 2014-02-12

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CN201320447472.2U Expired - Fee Related CN203425784U (en) 2013-07-25 2013-07-25 Reaction kettle device

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CN (1) CN203425784U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104190323A (en) * 2014-09-10 2014-12-10 四川天齐锂业股份有限公司 Rapid vacuum dispersion reaction kettle
CN107670609A (en) * 2016-09-30 2018-02-09 青岛大学 A kind of chemical mechanical system using electromagnetic drive reactor

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104190323A (en) * 2014-09-10 2014-12-10 四川天齐锂业股份有限公司 Rapid vacuum dispersion reaction kettle
CN107670609A (en) * 2016-09-30 2018-02-09 青岛大学 A kind of chemical mechanical system using electromagnetic drive reactor

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Granted publication date: 20140212

Termination date: 20150725

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