CN203385589U - Liquid sampler in reaction kettle - Google Patents
Liquid sampler in reaction kettle Download PDFInfo
- Publication number
- CN203385589U CN203385589U CN201320535827.3U CN201320535827U CN203385589U CN 203385589 U CN203385589 U CN 203385589U CN 201320535827 U CN201320535827 U CN 201320535827U CN 203385589 U CN203385589 U CN 203385589U
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- sampler
- sampling
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- thermometric
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Abstract
The utility model provides a technical scheme of a liquid sampler in a reaction kettle. According to the scheme, the liquid sampler comprises a hollow sampler body which comprises a sampling section and a temperature measuring section which are hollow cylinders, wherein the cross-section diameter of the sampling section is greater than that of the temperature measuring section; a through hole is formed in the top surface of the temperature measuring section; a thermometer is fixed inside the temperature measuring section; a transparent observation window for conveniently observing scales of the thermometer is arranged on the inner wall of the temperature measuring section; an annular table is arranged on the bottom of the sampling section; a sampling hole is formed in the center of the annular table; a rubber plug matched with the sampling hole is hinged on the upper part of the annular table. The liquid sampler in the reaction kettle disclosed by the utility model is simple in structure and accurate in sampling, is capable of ensuring sampling accuracy by increasing length of the sampler body and capable of measuring the temperature of liquid in the reaction kettle in real time by virtue of the thermometer in the sampler, and has very high popularization and use value.
Description
Technical field
The utility model relates to a kind of sampler, liquid sampler in especially a kind of reactor.
Background technology
As everyone knows, utilizing reactor to carry out chemical industry when synthetic, in order to adjust in time the parameter of controlling material in reactor, often need the reaction process of material in timely observing response still, sometimes also need to take out material in reactor and carry out sample analysis.Due to reactor, chemical industry normally carries out when synthetic under closed state material is carried out, therefore when sampling, need operating personnel first to dismantle nut, the bolt on the cover plate for manhole be connected with reactor, open the cover plate for manhole of reactor, then stopple coupon is deep under the liquid level in reactor and is sampled, in order to guarantee the homogeneity of sampling, need to all be sampled at the bottom of the still of reactor and still middle part, but reactor is deep, more difficult to when sampling at the bottom of still; And current most of sampler adopts the principle of piston to be sampled, install more complicatedly, to manufacture difficultly, production cost is higher.
In prior art, when preparing thiol methyl tin, material need to be put into to reactor and be stirred.In whole course of reaction, all need to carry out temperature detection, guarantee that temperature can not be higher than 50 degrees centigrade, and be to insert a thermometer from reactor in reactor to the detection mode of reactor temperature, be provided with the thermometer storehouse in reactor, material and thermometer are separated., there is certain inaccuracy in this temperature detection mode, across one deck thermometer storehouse, can not measure very accurately the temperature in reactor.And reactor is when stirring, puddler easily touches thermometer, causes the thermometer fracture, affects productivity effect.These are all the existing weak points of prior art.
Summary of the invention
Technical problem to be solved in the utility model, be exactly for the existing deficiency of prior art, and the technical scheme of liquid sampler in a kind of reactor is provided, this scheme is simple in structure, sampling is convenient, can guarantee the accuracy of sampling by the length that increases the sampler body; Can measure in real time the fluid temperature in reactor, there is very strong popularizing value simultaneously.
This programme is achieved by the following technical measures: liquid sampler in a kind of reactor, the sampler body that comprises hollow, the characteristics of this programme are: described sampler body comprises sampling section and thermometric section, described sampling section and thermometric section are hollow circular cylinder, and the cross-sectional diameter of sampling section is greater than the cross-sectional diameter of described thermometric section; The end face of described thermometric section is provided with through hole, and the thermometric intersegmental part is fixed with thermometer, and the inwall of thermometric section is provided with the convenient transparent windows of observing the thermometer registration; The bottom of described sampling section is provided with a ring platform, and the central authorities of ring platform are provided with a thief hole, and the upper articulation of ring platform has one and the rubber plug that matches of thief hole.
The concrete characteristics of this programme are: the length of described sampling section is 200mm.
The length 1500mm of described thermometric section.
The material of described sampler body is stainless steel.
Between described rubber plug and thief hole, cooperation place is provided with seal.
The end of described thermometric section is provided with the convenient handle gripped.
Described thief hole is bellmouth.
Described rubber plug is conical plug.
The beneficial effect of this programme can be learnt according to the narration to such scheme, owing to comprising the sampler body of hollow in this scheme, described sampler body comprises sampling section and thermometric section, described sampling section and thermometric section are hollow circular cylinder, and the cross-sectional diameter of sampling section is greater than the cross-sectional diameter of described thermometric section; The end face of described thermometric section is provided with through hole, the thermometric intersegmental part is fixed with thermometer, the inwall of thermometric section is provided with the convenient transparent windows of observing the thermometer registration, can not only be sampled easily, can also measure in real time and be reflected on thermometer reactor temperature, avoid in the prior art fluid temperature in reactor to measure inaccurate and thermometer and held flimsy problem; The bottom of described sampling section is provided with a ring platform, the central authorities of ring platform are provided with a thief hole, the upper articulation of ring platform has one and the rubber plug that matches of thief hole, rubber plug can rotate up while touching the interior liquid of reactor automatically, motion nimbly and freely, thereby can complete fast sampling operation, high efficiency.The utility model is simple in structure, and sampling is convenient, can guarantee the accuracy of sampling by the length that increases the sampler body; Can measure in real time the fluid temperature in reactor, there is very strong popularizing value simultaneously.As can be seen here, the utility model compared with prior art, has substantive distinguishing features and progress, and the beneficial effect of its enforcement is also apparent.
The accompanying drawing explanation
The structural representation that Fig. 1 is the utility model embodiment.
Fig. 2 is the utility model complete structural representation of sampling.
In figure, 1 is through hole, and 2 is handle, and 3 is transparent windows, and 4 is rubber plug, and 5 is the ring platform, and 6 is the sampling section, and 7 is the thermometric section, and 8 is thermometer, and 9 is thief hole, and 10 is seal.
Embodiment
For clearly demonstrating the technical characterstic of this programme, below by an embodiment, and, in conjunction with its accompanying drawing, this programme is set forth.
By accompanying drawing, can find out, liquid sampler in a kind of reactor of this programme, the sampler body that comprises hollow, the material of sampler body is stainless steel, and described sampler body comprises sampling section 6 and thermometric section 7, and the length of sampling section 6 is 200 mm, the length of thermometric section 7 is 1500mm, the length of sampler body is longer, can easily gather to the liquid of differing heights in reactor sampling, has guaranteed the accuracy of sampling result; Described sampling section 6 and thermometric section 7 are hollow circular cylinder, and the cross-sectional diameter of sampling section 6 is greater than the cross-sectional diameter of described thermometric section 7; The end face of described thermometric section 7 is provided with through hole 1, thermometric section 7 inside are fixed with thermometer 8, the inwall of thermometric section 7 is provided with the convenient transparent windows 3 of observing the thermometer registration, the material of transparent windows 3 can adopting quartz glass, can observe clearly the registration on thermometer, also prevent the corrosion and damage of reactant liquor to sampler.
The bottom of described sampling section 6 is provided with a ring platform 5, and the central authorities of ring platform 5 are provided with a thief hole 9, and the upper articulation of ring platform 5 has one and the rubber plug 4 that matches of thief hole 9, thief hole 9 is bellmouth, rubber plug 4 is conical plug, guarantees that liquid can only flow into sampler from reactor, and can not flow backwards; After sampler is put into to reactor, rubber plug 4 is understood automatic rotation after touching liquid, and liquid is entered in sampler.Between described rubber plug 4 and thief hole 9, cooperation place is provided with seal 10, after having sampled, sampler is taken out, and seal 10 can guarantee good sealing, prevents that the liquid in sampler from revealing.
In actual mechanical process, hand-held handle 2 is put into the reactor kettle by sampler, when rubber plug 4 touches liquid, rubber plug 4 can enter sampler by the interior liquid of automatic rotation while kettle, thermometer is measured fluid temperature in sampler, sees through transparent windows 3 and can observe the temperature registration; After having sampled, take out sampler, rubber plug 4 stops up thief hole 9, completes sampling process.
The utility model can pass through or adopt existing techniques in realizing without the technical characterictic of describing; do not repeat them here; certainly; above-mentioned explanation is not to restriction of the present utility model; the utility model also is not limited in above-mentioned giving an example; the variation that those skilled in the art make in essential scope of the present invention, remodeling, interpolation or replacement, also should belong to protection domain of the present utility model.
Claims (8)
1. liquid sampler in a reactor, the sampler body that comprises hollow, it is characterized in that: described sampler body comprises sampling section and thermometric section, and described sampling section and thermometric section are hollow circular cylinder, and the cross-sectional diameter of sampling section is greater than the cross-sectional diameter of described thermometric section; The end face of described thermometric section is provided with through hole, and the thermometric intersegmental part is fixed with thermometer, and the inwall of thermometric section is provided with the convenient transparent windows of observing the thermometer registration; The bottom of described sampling section is provided with a ring platform, and the central authorities of ring platform are provided with a thief hole, and the upper articulation of ring platform has one and the rubber plug that matches of thief hole.
2. liquid sampler in reactor according to claim 1, is characterized in that: the length 200mm of described sampling section.
3. liquid sampler in reactor according to claim 1, is characterized in that: the length 1500mm of described thermometric section.
4. liquid sampler in reactor according to claim 1, it is characterized in that: the material of described sampler body is stainless steel.
5. liquid sampler in reactor according to claim 1, it is characterized in that: between described rubber plug and thief hole, cooperation place is provided with seal.
6. according to liquid sampler in the described reactor of claim 1 or 3, it is characterized in that: the end of described thermometric section is provided with the convenient handle gripped.
7. liquid sampler in reactor according to claim 1, it is characterized in that: described thief hole is bellmouth.
8. liquid sampler in reactor according to claim 1, it is characterized in that: described rubber plug is conical plug.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320535827.3U CN203385589U (en) | 2013-08-30 | 2013-08-30 | Liquid sampler in reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320535827.3U CN203385589U (en) | 2013-08-30 | 2013-08-30 | Liquid sampler in reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203385589U true CN203385589U (en) | 2014-01-08 |
Family
ID=49874067
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320535827.3U Expired - Fee Related CN203385589U (en) | 2013-08-30 | 2013-08-30 | Liquid sampler in reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203385589U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109173786A (en) * | 2018-09-18 | 2019-01-11 | 安庆市睿霞机械有限公司 | A kind of chemical industry processing unit (plant) |
-
2013
- 2013-08-30 CN CN201320535827.3U patent/CN203385589U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109173786A (en) * | 2018-09-18 | 2019-01-11 | 安庆市睿霞机械有限公司 | A kind of chemical industry processing unit (plant) |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140108 Termination date: 20150830 |
|
| EXPY | Termination of patent right or utility model |